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Evaluation of tribological properties of thin hard coatings by a slurry jet erosion test and its application to surface processing

Research Project

Project/Area Number 15360083
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Design engineering/Machine functional elements/Tribology
Research InstitutionUniversity of Fukui

Principal Investigator

IWAI Yoshiro  Univ.of Fukui, Mechanical Eng., Professor, 工学部, 教授 (40115291)

Co-Investigator(Kenkyū-buntansha) NOHDA Tomomi  Univ.of Fukui, Mechanical Eng., Associate Professor, 工学部, 助教授 (80251982)
Project Period (FY) 2003 – 2005
Project Status Completed (Fiscal Year 2005)
Budget Amount *help
¥11,500,000 (Direct Cost: ¥11,500,000)
Fiscal Year 2005: ¥1,800,000 (Direct Cost: ¥1,800,000)
Fiscal Year 2004: ¥2,800,000 (Direct Cost: ¥2,800,000)
Fiscal Year 2003: ¥6,900,000 (Direct Cost: ¥6,900,000)
KeywordsTribology / Wear test method / Evaluation / Slurry jet erosion test / MSE / PVD coating / Abrasion / Wear resistance / マイクロスラリージェットエロージョン / PVD膜 / スラリージェット / エロージョン / 微細加工
Research Abstract

We proposed slurry jet, a new type of solid particle erosion test, in order to quickly evaluate tribological properties of thin hard coatings. The slurry jet with 1μm alumina particles were impacted at high velocity perpendicular to thin PVD coatings.
(1) The TiN deposited under the highest substrate temperature proved to have the highest wear resistance although it had a relatively low hardness, The wear rate varies with the TiN grain orientation, i.e. the {111} orientation shows higher wear resistance than the {100}, which correlates to a correspondingly higher cleavage fracture resistance within each grains.
(2) The ranking of MSE wear resistance for CrN deposited by different conditions show good correlation to their ratio of micro hardness to elastic modulus (H/E).
(3) For the TiN/TiCN coating, the wear rate of TiN of the TiN/TiCN coating coincided to that of the singlelayerd TiN. However, TiN/TiCN coatings by the different deposition system showed discontinuous wear curves which were characterized by TiN, TiCN coatings and their interface. The differences in the wear properties between the coatings may be caused by the original surface morphology.
(4) We set up a new type of MSE test apparatus (pot type tests) which can obtain the wear volume per unit weight of erodent. As a result, it generates reproducible results.
(5) The ranking of wear resistance among the various coatings was compared with those obtained by other coating evaluation tests such as micro abrasion test.
As a result, our proposed micro slurry jet erosion (MSE) test proved to be very useful as a screening test when evaluating the properties of hard thin coatings. In addition, we tried to produce the surface textures of the glass surface by our MSE method and the possibility of processing was concluded.

Report

(4 results)
  • 2005 Annual Research Report   Final Research Report Summary
  • 2004 Annual Research Report
  • 2003 Annual Research Report
  • Research Products

    (15 results)

All 2006 2005 2004 Other

All Journal Article (7 results) Patent(Industrial Property Rights) (4 results) Publications (4 results)

  • [Journal Article] Evaluation of Erosive Wear Resistance of TiN Coatings by A Slurry Jet Impact Test2006

    • Author(s)
      Y.Iwai, et al.
    • Journal Title

      Wear (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Annual Research Report 2005 Final Research Report Summary
  • [Journal Article] Evaluation of Erosive Wear Resistance of TiN Coatings by A Slurry Jet Impact Test2006

    • Author(s)
      Y.Iwai, T.Miyajima, T.Honda, T.Matsubara, K.Kanda, S.Hogmark
    • Journal Title

      Wear (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Micro Slurry-jet Erosion Test(MSE) for Evaluation of Hard Thin Coatings2005

    • Author(s)
      Y.Iwai, et al.
    • Journal Title

      Book of Synopses ITC-KOBE

      Pages: 203-203

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Micro Slurry-jet Erosion Test (MSE) for Evaluation of Hard Thin Coatings2005

    • Author(s)
      Y.Iwai, et al.
    • Journal Title

      Book of Synopses ITC-KOBE

      Pages: 203-203

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Evaluation of Erosive Wear Resistance of TiN Coatings by A Slurry Jet Impact Test2004

    • Author(s)
      Y.Iwai, et al.
    • Journal Title

      Proc. of the 11th Nordic Symposium on Tribology, Tromso, Norway

      Pages: 197-206

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Evaluation of Erosive Wear Resistance of TiN Coatings by A Slurry Jet Impact Test2004

    • Author(s)
      Y.Iwai, T.Miyajima, T.Honda, T.Matsubara, K.Kanda, S.Hogmark
    • Journal Title

      Proc.of the 11th Nordic Symposium on Tribology, Tromso, Norway

      Pages: 197-206

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Micro Slurry-jet Erosion Test (MSE) for Evaluation of Hard Thin Coatings

    • Author(s)
      Y.Iwai, T.Miyajima, T.Honda
    • Journal Title

      Book of Synopses ITC-KOBE

      Pages: 203-203

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 皮膜の耐食性評価方法2005

    • Inventor(s)
      岩井善郎, 本田知己, 吉長重樹, 窪田佳彦
    • Industrial Property Rights Holder
      国立大学法人福井大学
    • Industrial Property Number
      2005-376279
    • Filing Date
      2005-12-27
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 皮膜評価試験機2004

    • Inventor(s)
      松原亨, 岩井善郎
    • Industrial Property Rights Holder
      マコー株式会社
    • Industrial Property Number
      2004-379835
    • Filing Date
      2004-12-28
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 商標「MSE」2004

    • Inventor(s)
      マコー株式会社, 岩井善郎
    • Industrial Property Rights Holder
      マコー株式会社, 岩井善郎
    • Filing Date
      2004-11-30
    • Acquisition Date
      2006-01-13
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 商標2004

    • Inventor(s)
      マコー株式会社, 岩井善郎
    • Industrial Property Rights Holder
      マコー株式会社, 岩井善郎
    • Filing Date
      2004-11-30
    • Related Report
      2004 Annual Research Report
  • [Publications] T.Yamaguchi, Y.Iwai, S.Inagaki, M.Ueda: "A method for detecting bearing wear in a drain pump utilizing an eddy-current displacement sensor"Measurement. 33. 205-211 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] Y.Iwai, S.Li: "Cavitation erosion in waters having different surface tensions"Wear. 254/1-2. 1-9 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] H.Kato, M.Takama, Y.Iwai, K.Washida, Y.Sasaki: "Wear and mechanical properties of sintered copper-tin composites containing graphite or molybdenum disulfide"Wear. 255. 573-578 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] M.Miyajima, Y.Iwai: "Effects of reinforcements on sliding wear behavior of aluminum matrix composites"Wear. 255. 606-616 (2003)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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