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Development and Applications of Nanostructured Soft Magnetic Cores with Extremely Low Loss and Controlled Permeability

Research Project

Project/Area Number 15360170
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Electronic materials/Electric materials
Research InstitutionNAGASAKI UNIVERSITY

Principal Investigator

FUKUNAGA Hirotoshi  Nagasaki University, Faculty of Engineering, Professor, 工学部, 教授 (10136533)

Co-Investigator(Kenkyū-buntansha) NAKANO Masaki  Nagasaki University, Faculty of Engineering, Associate Professor, 工学部, 助教授 (20274623)
YANAI Takeshi  Nagasaki University, Faculty of Engineering, Research Associate, 工学部, 助手 (30404239)
吉沢 克仁  日立金属(株), 先端エレクトロニクス研究所, 主任研究員
掛橋 英典  松下電工(株), 照明R&Dセンター, 主査技師
金井 泰久  長崎大学, 工学部, 講師 (00264200)
Project Period (FY) 2003 – 2005
Project Status Completed (Fiscal Year 2005)
Budget Amount *help
¥15,200,000 (Direct Cost: ¥15,200,000)
Fiscal Year 2005: ¥2,000,000 (Direct Cost: ¥2,000,000)
Fiscal Year 2004: ¥6,100,000 (Direct Cost: ¥6,100,000)
Fiscal Year 2003: ¥7,100,000 (Direct Cost: ¥7,100,000)
KeywordsMagnetic loss / Nano-materials / Electronic Materials / Creep / Electronic Devices / Permeability / Magnetism / 誘導磁気異方性 / ナノ結晶材料 / 透磁率制御 / 応力下連続焼鈍 / 高周波特性 / PLD / 交換スプリング磁石 / ナノ結晶 / 最大エネルギー積 / 保磁力 / ND-Fe-B / 積層膜
Research Abstract

A new material with controllable permeability and extremely low magnetic loss was developed through this research project. The material was prepared by the crystallization of an amorphous Fe-Nb-Si-B ribbon under tensile stress. The crystallization under tensile stress induced magnetic anisotropy perpendicular to the ribbon axis, and resulted in the linear magnetization curve up to magnetic saturation. As the magnitude of the anisotropy was proportional to the stress value, the permeability was controlled easily by changing the magnitude of the applied stress.
The crystallization under tensile stress was achieved by several annealing methods. In the methods, the continuous crystallization of a moving amorphous ribbon by Joule-heating enabled us to prepare a ribbon with controlled permeability under the moving velocity exceeding 200cm/min. As the development of the anisotropy can be completed in an extremely short time less than 1 sec, the continuous crystallization under a faster moving velocity is expected by improving apparatus for crystallization.
Toroidal cores were obtained from a developed ribbon, and their magnetic properties were evaluated at the frequencies up to 2MHz. The prepared cores exhibited superior soft magnetic properties reflecting the magnetic properties of the ribbon, when their diameters were larger than a critical value which was determined from the saturation magnetostriction, Young modulus, and the thickness of the ribbon. Permeability of a core could be controlled at a value of a several hundreds and was constant up to 2MHz. Magnetic loss of the obtained cores was 1/3 of that of a ferrite core. The DC-bias filed applicable to the cores without deterioration of magnetic properties was 3 times as large as that of a ferrite core, which can be attributed to the large saturation magnetization of the developed material.

Report

(4 results)
  • 2005 Annual Research Report   Final Research Report Summary
  • 2004 Annual Research Report
  • 2003 Annual Research Report
  • Research Products

    (34 results)

All 2006 2005 2004 2003 Other

All Journal Article (29 results) Publications (5 results)

  • [Journal Article] Magnetic properties of Fe-based ribbons and toroidal cores prepared by continuous Joule heating under tensile stress2006

    • Author(s)
      T.Yanai, A.Shimada, K.Takahashi, M.Nakano, Y.Yoshizawa, H.Fukunaga
    • Journal Title

      IEEE Transaction on Magnetics Vol.42(To be published in a 2006)

      Pages: 7-12

    • NAID

      120006982391

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Magnetic properties of Fe-based ribbons and toroidal cores prepared by continuous Joule heating under tensile stress2006

    • Author(s)
      T.Yanai, A.Shimada, K.Takahashi, M.Nakano, Y.Yoshizawa, H.Fukunaga
    • Journal Title

      IEEE Transaction on Magnetics (To be published in a 2006 issue)

    • NAID

      120006982391

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] A new fabrication process of Fe-based ribbon with creep-induced anisotropy2005

    • Author(s)
      T.Yanai, T.Ohya, K.Takahashi, M.Nakano, Y.Yoshizawa, H.Fukunaga
    • Journal Title

      Journal of Magnetism and Magnetic Materials Vol.290-291

      Pages: 1502-1505

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Annual Research Report 2005 Final Research Report Summary
  • [Journal Article] Origin of the magnetic anisotropy induced by stress annealing in Fe-based nanocrystalline alloy2005

    • Author(s)
      M.Ohnuma, K.Hono, T.Yanai, M.Nakano, H.Fukunaga, Y.Yoshizawa
    • Journal Title

      Applied Physics Letters Vol.86

    • NAID

      120006982345

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] A new fabrication process of Fe-based ribbon with creep-induced anisotropy2005

    • Author(s)
      T.Yanai, T.Ohya, K.Takahashi, M.Nakano, Y.Yoshizawa, H.Fukunaga
    • Journal Title

      J.Magn.Magn.Mater. Vol.290-291

      Pages: 1502-1505

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Origin of the magnetic anisotropy induced by stress annealing in Fe-based nanocrystalline alloy2005

    • Author(s)
      M.Ohnuma, K.Hono, T.Yanai, M.Nakano, H.Fukunaga, Y.Yoshizawa
    • Journal Title

      Appl.Phys.Lett. Vol.86

    • NAID

      120006982345

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Origin of the magnetic anisotropy induced by stress annealing it Fe-based nanocrystalline alloy2005

    • Author(s)
      M.Ohnuma, K.Hono, T.Yanai, M.Nakano, H.Fukunaga, Y.Yoshizawa
    • Journal Title

      Applied Physics Letters Vol.86

    • Related Report
      2005 Annual Research Report
  • [Journal Article] 応力下連続焼鈍で透磁率制御したFe系薄帯およびトロイダルコアの基礎特性2005

    • Author(s)
      島田視宏, 柳井武志, 高橋賢一郎, 中野正基, 福永博俊, 吉沢克仁
    • Journal Title

      電気学会マグネティクス研究会資料 MAG-05-39

      Pages: 7-12

    • NAID

      10016463489

    • Related Report
      2005 Annual Research Report
  • [Journal Article] 透磁率制御ナノ結晶薄帯の応力下熱暴露による異方性の変化2005

    • Author(s)
      柳井武志, 島田視宏, 高橋賢一郎, 中野正基, 福永博俊, 吉沢克仁
    • Journal Title

      第29回応用磁気学会学術講演会概要集

    • Related Report
      2005 Annual Research Report
  • [Journal Article] 応力下連続ジュール加熱法により作製した透磁率制御Fe系ナノ結晶薄帯の基礎特性2005

    • Author(s)
      島田視宏, 柳井武志, 高橋賢一郎, 中野正基, 福永博俊, 吉沢克仁
    • Journal Title

      第29回応用磁気学会学術講演会概要集

    • NAID

      120006980813

    • Related Report
      2005 Annual Research Report
  • [Journal Article] 応力下連続ジュール加熱法による透磁率制御Fe系薄帯の作製2005

    • Author(s)
      島田視宏, 柳井武志, 高橋賢一郎, 中野正基, 福永博俊, 吉沢克仁
    • Journal Title

      電気学会マグネティクス研究会資料 MAG-05-114

      Pages: 63-68

    • NAID

      10016966629

    • Related Report
      2005 Annual Research Report
  • [Journal Article] A new fabrication process of Fe-based ribbon with creep-induced anisotropy2005

    • Author(s)
      T.Yanai, T.Ohya, K.Takahashi, M.Nakano, H.Fukunaga
    • Journal Title

      Journal of Magnetism and Magnetic Materials In press

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Microstructure and Magnetic Relaxation in Amorphous and Nanocrystalline Fe_<42.7>Co_<42.7>Zr_<6.8-x>Nb_xB_<6.8>Cu_1 (X=0 or 1) Alloys2004

    • Author(s)
      J.Zbroszczyk, W.Ciurzyhska, H.Fukunaga, et al.
    • Journal Title

      Journal of Magnetism and Magnetic Materials Vol.272-276

      Pages: 1425-1426

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Nanocrystallization and Magnctic Properties of Fe_<85.4>Zr_<6.8-x>M_xB_<6.8>Cu_1 (X=0 or 1; M=Nb, Nd or Mo) A11oys2004

    • Author(s)
      J.Olszewski, H.Fuklmagab et al.
    • Journal Title

      Journal of Magnetism and Magnetic Materials Vol. 272-276

      Pages: 1433-1435

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Development of nanostructured magnetic cores with low permeability and low magnetic loss for next generation2004

    • Author(s)
      Y.Yanai, H.Tanaka, K.Takahashi, M.Nakano, H.Fukunaga
    • Journal Title

      Proc. 8^<th> Joint Sym. Cheju National Univ. & Nagasaki Univ. on Sci. & Tech.

      Pages: 75-78

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] High temperature magnetic properties of Fe-Cu-Nb-Si-B cores with creep-induced anisotropy2004

    • Author(s)
      T.Yanai, M.Yamasaki, K.Takahashi, M.Nakano, Y.Yoshizawa, H.Fukunaga
    • Journal Title

      IEEE Transaction in Magnetics Vol.40,No.4

      Pages: 2721-2723

    • NAID

      120006984980

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Investigation of Development Process of Creep-Induced Anisotropy in Nanocrystalline Fe_<73.5>Cu_1Nb_3Si_<15.5>B_7 Ribbon for Mass Production2004

    • Author(s)
      Y.Yanai, M.Yamasaki, K.Takahashi, M.Nakano, H.Fukunaga, Y.Yoshizawa
    • Journal Title

      Proc.SMM 16 Vol.1.2

      Pages: 737-741

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Microstructure and Magnetic Relaxation in Amorphous and Nanocrystalline Fe_<42.7>Co_<42.7>Zr_<6.8-X>Nb_XB_<6.8>Cu_1(X=0 or 1) Alloys2004

    • Author(s)
      J.Zbroszczyk, W.Ciurzynska, H.Fukunaga, J.Olszewski, A.Mlyneczyk, M.Piasecki, P.Bragiel, M.Hasiak, J.Lelatko
    • Journal Title

      J.Magn.Magn.Mater. Vol.272-276

      Pages: 1425-1426

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Nanocrystallization and Magnetic Properties of Fe_<85.4>Zr_<6.8-X>M_XB_<6.8>Cu_1 (X=0 or 1 ; M=Nb, Nd or Mo) Alloys2004

    • Author(s)
      J.Olszewski, H.Fukunaga, J.Zbroszczyk, W.Ciurzynska, K.Perduta, P.Bragiel, M.Piasecki, J.Lelatko, M.Hasiak
    • Journal Title

      J.Magn.Magn.Mater. Vol.272-276

      Pages: 1433-1435

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Development of nanostructured magnetic cores with low permeability and low magnetic loss for next generation2004

    • Author(s)
      Y.Yanai, H.Tanaka, K.Takahashi, M.Nakano, H.Fukunaga
    • Journal Title

      Proc.8^<th> Joint Sym.Cheju National Univ.& Nagasaki Univ.on Sci.& Tech.

      Pages: 75-78

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] High temperature magnetic properties of Fe-Cu-Nb-Si-B cores with creep-induced anisotropy2004

    • Author(s)
      T.Yanai, M.Yamasaki, K.Takahashi, M.Nakano, Y.Yoshizawa, H.Fukunaga
    • Journal Title

      IEEE Trans.Magn. Vol.40, No.4

      Pages: 2721-2723

    • NAID

      120006984980

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Investigation of Development Process of Creep-Induced Anisotropy in Nanocrystalline Fe_<73.5>Cu_1Nb_3Si_<15.5>B_7 Ribbon for Mass Production2004

    • Author(s)
      Y.Yanai, M.Yamasaki, K.Takahashi, M.Nakano, H.Fukunaga, Y.Yoshizawa
    • Journal Title

      Proc.SMM 16 Vol.2

      Pages: 737-741

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Development of nanostructured magnetic cores with low permeability and low magnetic loss for next generation2004

    • Author(s)
      T.Yanai, H.Tanaka, K.Takahashi, M.Nakano, H.Fukunaga
    • Journal Title

      JSST 2004/Special Issue of Conference Proceedings

      Pages: 75-78

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Investigation of development process of creep-induced anisotropy in nanocrystalline Fe_<73.5>Cu_1Nb_3S_<115.5>B_7 ribbon for mass production2004

    • Author(s)
      T.Yanai, M.Yamasaki, K.Takahashi, M.Nakano, H.Fukunaga, Y.Yoshizawa
    • Journal Title

      SMM 16/Special 16/Special Issue of Conference Proceedings 2

      Pages: 737-741

    • Related Report
      2004 Annual Research Report
  • [Journal Article] High temperature magnetic properties of Fe-Cu-Nb-Si-B cores with creep-induced anisotropy2004

    • Author(s)
      T.Yanai, M.Yamasaki, K.Takahashi, M.Nakano, Y.Yoshizawa, H.Fukunaga
    • Journal Title

      IEEE Transactions on Magnetics 40

      Pages: 2721-2723

    • NAID

      120006984980

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Microstructure and magnetic relaxation in amorphous and nanocrystalline Fe_<42.7>Co_<42.7>Zr_<6.8-x>Nb_xB_<6,8>Cu_1(X=0 or 1) alloys2004

    • Author(s)
      J.Zbroszczyk, W.Ciurzynska, H.Fukunaga, J.Olszewski, A.Mlyneczyk, M.Piasecki, P.Bragiel, M.Hasiak, J.Lelatko
    • Journal Title

      Journal of Magnetism and Magnetic Materials 272-276

      Pages: 1425-1426

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Nanocrystallization and magnetic properties of Fe_<85.4>Zr_<6.8-x>MxB_<6.8>Cu_1(X=0 or 1; M=Nb, Nd or Mo) alloys2004

    • Author(s)
      J.Olszewski, H.Fukunaga, J.Zbroszczyk, W.Ciurzynska, K.Perduta, P.Bragiel, M.Piasecki, J.Lelatko, M.Hasiak
    • Journal Title

      Journal of Magnetism and Magnetic Materials 272-276

      Pages: 1433-1435

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Direct evidence for structural origin of stress-induced magnetic anisotropy in Fe-Si-B-Nb-Cu nanocrystalline alloys2003

    • Author(s)
      M.Ohnuma, K.Hono, T.Yanai, H.Fukunaga, Y.Yoshizawa
    • Journal Title

      Applied. Physics Letters Vo1.83,No.14

      Pages: 2859-2861

    • NAID

      120006982346

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Direct evidence for structural origin of stress-induced magnetic anisotropy in Fe-Si-B-Nb-Cu nanocrystalline alloys2003

    • Author(s)
      M.Ohnuma, K.Hono, T.Yanai, H.Fukunaga, Y.Yoshizawa
    • Journal Title

      Appl.Phys Lett. Vol.83

      Pages: 2859-2861

    • NAID

      120006982346

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Publications] J.Olszewski, J.Zbroszczyk, W.Ciurznska, H.Fukunaga, 他6名: "Nanocrystallization studies of rapidly quenched Fe_<85.4-X>Co_XZr_<6.8-Y>Nb_yB_<6.8>Cu_1X=0 or 1)alloys"NUKLEONIKA. Vol.8 Supplement. 49-52 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] M.Ohnuma, K.Hono, T.Yanai, H.Fukunaga, Y.Yoshizawa: "Direct evidence for structural origin of stress-induced magnetic anisotropy in Fe-Si-B-Nb-Cu nanocrystalline alloys"Appl.Phys Lett.. Vol.83 No.14. 2859-2861 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] J.Zbroszczyk, W.Ciurzynska, H.Fukunaga, 他6名: "Microstructure and Magnetic Relaxation in Amorphous and Nanocrystalline Fe_<42.7>Co_<42.7>Zr_<6.8-X>Nb_XB_<6.8>Cu_1 (X=0 or 1) Alloys"J.Magn.Magn.Mater.. in press. (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] J.Olszewski, H.Fukunaga, 他7名: "Nanocrystallization and Magnetic Properties of Fe_<85.4>Zr_<6.8-X>M_XB_<6.8>Cu_1 (X=0 or 1;M=Nb, Nd or Mo) Alloys"J.Magn.Magn.Mater.. in press. (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] T.Yanai, M.Yamasaki, K.Takahashi, M.Nakano, Y.Yoshizawa, H.Fukunaga: "High temperature magnetic prorerties of Fe-Cu-Nb-Si-B cores with creep-induced"IEEE Trans.Magn.. in press. (2004)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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