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Developments of Free Cutting Titanium Alloys for Dental CAD/CAM

Research Project

Project/Area Number 15390585
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field 補綴理工系歯学
Research InstitutionTohoku University

Principal Investigator

OKUNO Osamu  Tohoku University, Graduate School of Dentistry, Professor, 大学院・歯学研究科, 教授 (50014080)

Co-Investigator(Kenkyū-buntansha) KIMURA Kohei  Tohoku University, Graduate School of Dentistry, Professor, 大学院・歯学研究科, 教授 (40108551)
TAKADA Yukyo  Tohoku University, Graduate School of Dentistry, Associate Professor, 大学院・歯学研究科, 助教授 (10206766)
YODA Masanobu  Tohoku University, Graduate School of Dentistry, Associate Professor, 大学院・歯学研究科, 助教授 (70005073)
KIKUCHI Masafumi  Tohoku University, Graduate School of Dentistry, Assistant Professor, 大学院・歯学研究科, 助手 (50250791)
TAKAHASHI Masatoshi  Tohoku University, Graduate School of Dentistry, Assistant Professor, 大学院・歯学研究科, 助手 (50400255)
Project Period (FY) 2003 – 2005
Project Status Completed (Fiscal Year 2005)
Budget Amount *help
¥11,700,000 (Direct Cost: ¥11,700,000)
Fiscal Year 2005: ¥1,200,000 (Direct Cost: ¥1,200,000)
Fiscal Year 2004: ¥1,000,000 (Direct Cost: ¥1,000,000)
Fiscal Year 2003: ¥9,500,000 (Direct Cost: ¥9,500,000)
KeywordsTitanium Alloys / Dental Alloys / Free Cutting Titanium Alloys / Machinability / Grindability / CAD / CAM / Restoration / Prosthesis
Research Abstract

Free cutting titanium alloys for dental CAD/CAM, which have been dispersed fine brittle phase such as metastable α', α'', ω or intermetallic compound, were developed. β stabilizing elements of gold, silver, copper, niobium and hafnium were selected as alloying elements of titanium. Gold, silver and copper make eutectoid among titanium and these titanium compounds. Niobium or hafnium form complete solid solution with titanium. Machinability, mechanical properties and corrosion resistances of these titanium alloys were investigated.
Ti-30%Nb alloy showed significantly higher grinding rate at lower grinding speeds. Ti-20%Ag alloy and Ti-5%Cu alloys showed also significantly higher grinding rate at higher grinding speeds. Ti-30%Nb alloy, Ti-20%Ag alloy and Ti-5%Cu alloy had significantly higher tensile strength and Vickers hardness with reasonable elongations. Ti-30%Nb alloy may has good corrosion resistance because both of titanium and niobium have excellent corrosion resistance. Ti-20%Ag … More alloy and Ti-5%Cu alloy showed good corrosion resistance from the anodic porlaization curves and dissolution of ions equivalent to that of titanium. Then, machinability and mechanical properties of Ti-24%Nb-1%Cu alloy, Ti-18%Nb-2%Cu alloy and Ti-6%Nb-4%Cu alloy, which were mixed with Ti-5%Cu alloy and Ti-30%Nb alloy were investigated. Tensile strength of the experimental ternary titanium alloys were 700-860 MPa and significantly higher than those of CP titanium, Ti-5%Cu alloy and T-30%Nb alloy with about 4% elongation. The hardness of the experimental ternary titanium alloys were Hv 260-330. The grindability of Ti-6%Nb-4%Cu alloy increased with increasing grinding speed and became significantly larger than that of CP titanium above the grinding speed of 1250 m・min^<-1>. The garindability of Ti-18%Nb-2%Cu alloy was significantly higher than that of CP titanium at low grinding speed and became four times larger than that of CP titanium. The experimental Ti-Nb-Cu alloys may have good grindability and mechanical properties as CAD/CAM alloys for dental use. Less

Report

(4 results)
  • 2005 Annual Research Report   Final Research Report Summary
  • 2004 Annual Research Report
  • 2003 Annual Research Report
  • Research Products

    (32 results)

All 2006 2005 2004 2003 Other

All Journal Article (30 results) Publications (2 results)

  • [Journal Article] Elastic Moduli of Cast Ti-Au,Ti-Ag,and Ti-Cu Alloys2006

    • Author(s)
      M.Kikuchi, M.Takahashi, O.Okuno
    • Journal Title

      Dental Materials (in press)

      Pages: 1-6

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] CAD/CAM歯科用チタン合金の開発2006

    • Author(s)
      菊地聖史, 奥野 攻
    • Journal Title

      チタンと歯科臨床 4・1

      Pages: 1-6

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Elastic Moduli of Cast Ti-Au, Ti-Ag and Ti-Cu Alloys2006

    • Author(s)
      M.Kikuchi, M.Takahashi, O.Okuno
    • Journal Title

      Dental Materials (in press)

      Pages: 1-6

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Developments of Dental Free Cutting Titanium Alloys2006

    • Author(s)
      M.Kikuchi, O.Okuno
    • Journal Title

      Journal of Society for Titanium Alloys in Dentistry 4・1

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Mechanical Properties of Cast Ti-Hf Alloys2005

    • Author(s)
      H.Sato, M.Kkuchi, M.Komatsu, O.Okuno, T.Okabe
    • Journal Title

      Journal of Biomedical Materials Research, Part B : Applyed Biomaterials 72B・1

      Pages: 362-367

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Grindability of Cast Ti-Hf Alloys2005

    • Author(s)
      M.Kkuchi, M.Takahashi, H.Sato, O.Okuno, M.Nunn, T.Okabe
    • Journal Title

      Journal of Biomedical Materials Research, Part B : Applyed Biomaterials 77B・1

      Pages: 34-38

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Electrochemical Characterization of Cast Ti-Hf Binary Alloys2005

    • Author(s)
      Z.Cai, M.Koike, H.Sato, M.Brezner, Q.Guo, M.Komatsu, O.Okuno, T.Okabe
    • Journal Title

      Acta Biomaterialia 1

      Pages: 353-356

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Corrosion Characteristics of α-Ti and Ti_2Cu Composing Ti-Cu Alloys2005

    • Author(s)
      Y.Takada, O.Okuno
    • Journal Title

      Dental Materials Journal 24・4

      Pages: 610-616

    • NAID

      110003495348

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Annual Research Report 2005 Final Research Report Summary
  • [Journal Article] Evaluation of Ti-Cr-Cu Alloys for Dental Applications2005

    • Author(s)
      M.Koike, M.Itoh, O.Okuno, K.Kimura, O.Takeda, T.H.Okabe, T.Okabe
    • Journal Title

      Journal of Materials Engineering and Performance 14・6

      Pages: 778-783

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Mechanical Properties of Cast Ti-Hf Alloys2005

    • Author(s)
      H.Sato, M.Kikuchi, M.Komatsu, O.Okuno, T.Okabe
    • Journal Title

      Journal of Biomedical Materials Research, Part B : Applyed Biomaterials 72B・1

      Pages: 362-367

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Annual Research Report 2005 Final Research Report Summary
  • [Journal Article] Grindability of Cast Ti-Hf Alloys2005

    • Author(s)
      M.Kikuchi, M.Takahashi, H.Sato, O.Okuno, M.Nunn, T.Okabe
    • Journal Title

      Journal of Biomedical Materials Research, Part B : Applyed Biomaterials 77B・1

      Pages: 34-38

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Annual Research Report 2005 Final Research Report Summary
  • [Journal Article] Electrochemical Characterization of Cast Ti-Hf Binary Alloys2005

    • Author(s)
      Z.Cai, M.Koike, H.Sato, M.Brezner, Q.Guo, M.Komats, O.Okuno, T.Okabe
    • Journal Title

      Acta Biomaterialia 1

      Pages: 353-356

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Electrochemical characterization of cast Ti-Hf binary alloys2005

    • Author(s)
      Z.Cai, M.Koike, H.Sato, M.Brezner, Q.Guo, M.Komatsu, O.Okuno, T.Okabe
    • Journal Title

      Acta Biomaterialia 1

      Pages: 353-356

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Evaluation of Ti-Cr-Cu Alloys for Dental Applications2005

    • Author(s)
      M.Koike, M.Itoh, O.Okuno, K.Kimura, O.Takeda, T.H.Okabe, Toru Okabe
    • Journal Title

      Journal of Materials Engineering and Performance 14・6

      Pages: 778-783

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Elastic moduli of cast Ti-Au, Ti-Ag, and Ti-Cu alloys2005

    • Author(s)
      M.Kikuchi, M.Takahashi, O.Okuno
    • Journal Title

      Dental Materials (in press)

      Pages: 1-6

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Mechanical Properties of Cast Ti-Hf Alloys2005

    • Author(s)
      H.Sato, M.Kikuchi, M.Komatsu, O.Okuno, T.Okabe
    • Journal Title

      J Biomed Mater Res Part B : Appl Biomater 72B

      Pages: 362-367

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Improving Grindability and Wear Resistance of Ttanum Alloys2004

    • Author(s)
      T.Okabe, M.Kikuchi, C.Ohkubo, M.Koike, O.Okuno, Y.Oda
    • Journal Title

      Cost-Affordable Titanium Symposium, Ed.by F.Froes, M.Imam and D.Fray, TMS(The Minerals,Metals & Materials Society)

      Pages: 177-181

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Machinability Evaluation of Titanium Alloys2004

    • Author(s)
      M.Kikuchi, O.Okuno
    • Journal Title

      Dental Materials Journal 23・1

      Pages: 37-45

    • NAID

      110002983618

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Machinability Evaluation of Titanium Alloys (Part 2) -Analyses of Cutting Force and Spindle Motor Current-2004

    • Author(s)
      M.Kikuchi, O.Okuno
    • Journal Title

      Dental Materials Journal 23・4

      Pages: 621-627

    • NAID

      110002983801

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] The Grindability and Wear of Ti-Cu Alloys for Dental Applications2004

    • Author(s)
      T.Okabe, M.Kikuchi, C.Ohkubo, M.Koike, O.Okuno, Y.Oda
    • Journal Title

      JOM

      Pages: 46-48

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Corrosion Behavior and Microstructures of Experimental Ti-Au Alloys2004

    • Author(s)
      M.Takahashi, M.Kikuchi, Y.Takada, O.Okuno, T.Okabe
    • Journal Title

      Dental Materials Journal 23・2

      Pages: 109-116

    • NAID

      110002983611

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Mechanical Properties and Grindability of Experimental Ti-Au Alloys2004

    • Author(s)
      M.Takahashi, M.Kikuchi, O.Okuno
    • Journal Title

      Dental Materials Journal 23・2

      Pages: 203-210

    • NAID

      110002983596

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Improving Grindability and Wear Resistance of Titanium Alloys2004

    • Author(s)
      T.Okabe, M.Kikuchi, C.Ohkubo, M.Koike, O.Okuno, Y.Oda
    • Journal Title

      Cost-Affordable Titamium Symposium, TMS (The Minerals, Metals & Materials Society)

      Pages: 177-181

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] The grindability and wear of Ti-Cu alloys for dental applications2004

    • Author(s)
      T.Okabe, M.Kikuchi, C.Ohkubo, M.Koike, O.Okuno, Y.Oda
    • Journal Title

      JOM

      Pages: 46-48

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Mechanical properties and microstructures of cast Ti-Cu alloys2003

    • Author(s)
      M.Kikuchi, Y.Takada, S.Kiyosue, M.Yoda, M.Woldu, Z.Cai, O.Okuno, T.Okabe
    • Journal Title

      Dental Materials 19・3

      Pages: 174-181

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Grindability of cast Ti-Cu alloys2003

    • Author(s)
      M.Kikuchi, Y.Takada, S.Kiyosue, M.Yoda, M.Woldu, Z.Cai, O.Okuno, T.Okabe
    • Journal Title

      Dental Materials 19・5

      Pages: 375-381

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Grindability of Dental Cast Ti-Ag and Ti-Cu Alloys2003

    • Author(s)
      M.Kikuchi, M.Takahashi, T.Okabe, O.Okuno
    • Journal Title

      Dental Materials Journal 22・2

      Pages: 191-205

    • NAID

      110002983665

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Mechanical Properties and Grindability of Dental Cast Ti-Nb Alloys2003

    • Author(s)
      M.Kikuchi, M.Takahashi, O.Okuno
    • Journal Title

      Dental Materials Journal 22・3

      Pages: 328-342

    • NAID

      110002983652

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Mechanical Properties and Microstructures of Cast Ti-Cu alloys2003

    • Author(s)
      M.Kikuchi, Y.Takada, S.Kiyosue, M.Yoda, M.Woldu, Z.Cai, O.Okuno, T.Okabe
    • Journal Title

      Dental Materials 19・3

      Pages: 174-181

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Grindability of Cast Ti-Cu Alloys2003

    • Author(s)
      M.Kikuchi, Y.Takada, S.Kiyosue, M.Yoda, M.Woldu, Z.Cai, O.Okuno, T.Okabe
    • Journal Title

      Dental Materials 19・5

      Pages: 375-381

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Publications] M.KIKUCHI, M.TAKAHASHI, T.OKABE, O.OKUNO: "Grindability of Dental Cast Ti-Ag and Ti-Cu Alloys"Dental Materials Journal. 22・2. 191-205 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] M.KIKUCHI, M.TAKAHASHI, O.OKUNO: "Mechanical Properties and Grindability of Dental Cast Ti-Nb Alloys"Dental Materials Journal. 22・3. 328-342 (2003)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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