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Development of a compact low energy reactive gas ion gun for ultra high resolution depth profiling

Research Project

Project/Area Number 15560023
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Thin film/Surface and interfacial physical properties
Research InstitutionSetsunan University

Principal Investigator

INOUE Masahiko  Setsunan University, Asistant Professor, 工学部, 助教授 (60191889)

Co-Investigator(Kenkyū-buntansha) SHIMIZU Ryuichi  Osaka Institute of Technology, Professor, 情報科学部, 教授 (40029046)
Project Period (FY) 2003 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 2004: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 2003: ¥2,800,000 (Direct Cost: ¥2,800,000)
Keywordslow energy ion gun / Auger electron Spectroscopy / depth profiling / depth resolution / GaAs / AlAs / 低速イオンビーム / 酸素イオンビーム
Research Abstract

In the present study, AES depth profiling of GaAs/AlAs super lattice sample using the developed compact FLIG was performed with the ion energy ranging from 100 to 500eV. The practical etching rate of more than 1.5nm/min was attained in the energy region over 150eV. The high depth resolutions of 1.3,1.6,1.8 and 2.0nm (84-16%) were obtained with the sputtering energies of 100,150,200 and 300eV at the leading edge of Al-LVV depth profiles, respectively.
At the energy of 100eV, the best fit of the MRI calculation required different surface roughness of 0.4 and 1.2nm at the leading and trailing edges, leading to the remarkable improvement of the depth resolution at the leading edge (Δz_1=1.3nm) but followed by considerable deterioration at the trailing edge (Δz_1=2.7nm). Although this tendency is quite similar to the case of the ABS depth profiling with O_2^+ ion sputtering, probably due to the low sputtering yield of Al-oxides formed in AlAs layers by O_2^+ ion bombardment, any trace of oxygen adsorption onto a specimen surface could not be observed during the measurement. To investigate the origin of this phenomenon, we performed dynamic Monte-Carlo simulation.

Report

(3 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • Research Products

    (20 results)

All 2005 2003 Other

All Journal Article (14 results) Publications (6 results)

  • [Journal Article] High-Resolution Anger Depth Profiling by sub-keV Ion Sputlering2005

    • Author(s)
      M.Inoue, R.Shimizu, H.I.Lee, H.J.Kong
    • Journal Title

      Surf.& Interf.Anal. 37

      Pages: 167-170

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] High-resolution Auger Depth Profiling by Sub-KeV Ion Sputtering2005

    • Author(s)
      M.Inoue, R.Shimizu, H.I.Lee, H.J.Kang
    • Journal Title

      Surf.& Interf.Anal. Vol.37

      Pages: 167-170

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] High-resolution Auger Depth Profiling by sub-keV Ion Sputtering2005

    • Author(s)
      M.Inoue, R.Shimizu, H.I.Lee, H.J.Kang
    • Journal Title

      Surf.&Interf.Anal. 37

      Pages: 167-170

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Focusing and Positioning of Ion Beam for Sputter Depth Profiling using a Coaxicial Sample Stage and a Dual Nano-ammeter2003

    • Author(s)
      M.Inoue, K.Kurahashi, K.Kodama
    • Journal Title

      J.Surf.Anal. 10

      Pages: 197-202

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Application of a Low Energy Ion Gun for High Resolution Depth Profiling2003

    • Author(s)
      R.Shimizu, M.Inoue
    • Journal Title

      J.Surf.Anal. 10

      Pages: 154-157

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] A Novel Ultrahigh Vacuum Floating-type Low Energy Ion Gum for High Resolution Depth Profiling2003

    • Author(s)
      Y.Mizuhara, J.Kato, T.Nagatomi, Y.Takai, T.Aoyama, A.Yoshimoto, M.Inoue, R.Shimizu
    • Journal Title

      Surf.& Interf.Anal. 35

      Pages: 382-386

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] High Resolution Sputter Depth Profiling using Low Energy Ion Gum2003

    • Author(s)
      M.Inoue, R.Shimizu, K.Uta, T.Sato
    • Journal Title

      J.Surf.Anal. 10

      Pages: 31-41

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Focusing and Positioning of Ion Beam for Sputter Depth Profiling using a Coaxicial Sample Stage and a Dual Nano-ammter2003

    • Author(s)
      M.Inoue, K.Kurahashi, K.Kodama
    • Journal Title

      J.Surf.Anal. Vol.10

      Pages: 197-202

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Application of a Low Energy Ion Gun for High Resolution Depth Profiling2003

    • Author(s)
      R.Shimizu, M.Inoue
    • Journal Title

      J.Surf.Anal. Vol.10

      Pages: 154-157

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] A Novel Ultra high Vacuum Floating-type Low Energy Ion Gun for High Resolution Depth Profiling2003

    • Author(s)
      Y.Mizuhara, J.Kato, T.Nagatomi, Y.Takai, T.Aoyama, A.Yoshimoto, M.Inoue, R.Shimizu
    • Journal Title

      Surf.& Interf.Anal. Vol.35

      Pages: 382-386

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] High Resolution Sputter Depth Profiling using Low Energy Ion Gun2003

    • Author(s)
      M.Inoue, R.Shimizu, K.Uta, T.Sato
    • Journal Title

      J.Surf.Anal. Vol.10

      Pages: 31-41

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Focusing and Positioning of Ion Beam for Sputler-Depth Profiling using a Coaxcial Sample Stage and a Dual Nano-ammeter2003

    • Author(s)
      M.Inoue, K.Kurahashi, K.Kodama
    • Journal Title

      J.Surf.Anal. 10

      Pages: 197-202

    • Related Report
      2004 Annual Research Report
  • [Journal Article] A Novel Ultrahigh Vacuam Floating-type Low-Energy Ion Gun for High Resolution Depth Profiling2003

    • Author(s)
      Y.Mizuhara, J.Kato, T.Nagatomi, Y.Takai, T.Aoyama, A.Yoshimoto, M.Inoue, R.Shimizu
    • Journal Title

      Surf.&Interf.Anal. 35

      Pages: 382-386

    • Related Report
      2004 Annual Research Report
  • [Journal Article] High Resolution Sputler Depth Profiling using Low Energy Ion Gun2003

    • Author(s)
      M.Inoue, R.Shimizu, K.Uta, T.Sato
    • Journal Title

      J.Surf.Anal 10

      Pages: 31-41

    • Related Report
      2004 Annual Research Report
  • [Publications] 井上雅彦, 志水隆一, 宇多勝明, 佐藤達志: "低速イオン銃を用いた高分解能深さ方向分析"Journal of Surface Analysis. Vol.10,No.1. 31-41 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] R.Shimizu, M.Inoue: "Application of a Low Energy Ion Gun for High Resolution Depth Profiling"Journal of Surface Analysis. Vol.10,No.2. 154-157 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 井上雅彦, 倉橋和之, 児玉圭司: "同軸試料台と2連微小電流計を用いたスパッタ深さ方向分析用イオンビームの収束及び位置合わせ"Journal of Surface Analysis. Vol.10,No.3. 197-200 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] M.Inoue, R.Shimizu, H.I.Lee, H.J.Kang: "High Resolution Auger Depth Profiling by Sub-KeV Ion Sputtering"Abstract of 4th International Symposium on Atomic Level Characterizations for New Materials and Devices. 175-175 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 倉橋和之, 井上雅彦: "同軸試料台を用いたイオンビームの収束及び位置合わせ"2003年度実用表面分析講演会アブストラクト. 3-4 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] 天満真二, 倉橋和之, 井上雅彦, 志水隆一: "低エネルギーイオンスパッタリングによる高分解能AES深さ方向分析"2003年度実用表面分析講演会アブストラクト. 13-14 (2003)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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