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TEM/3DAP study of nanocomposite alloys

Research Project

Project/Area Number 15560580
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionNational Institute for Materials Science

Principal Investigator

OHKUBO Tadakatsu  National Institute for Materials Science, Materials Engineering Laboratory, Senior Researcher, 材料研究所, 主任研究員 (00242462)

Co-Investigator(Kenkyū-buntansha) HONO Kazuhiro  National Institute for Materials Science, Fellow, フェロー (60229151)
Project Period (FY) 2003 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 2004: ¥1,600,000 (Direct Cost: ¥1,600,000)
Fiscal Year 2003: ¥2,100,000 (Direct Cost: ¥2,100,000)
KeywordsTEM / atom probe / nanocomposite / nanostructure / magnetic property / 熱伝導率 / 高強度鋼板
Research Abstract

In order to understand the relation between nanostructure and properties of nanocomposite alloys, detailed nanostructure analysis has been done by TEM and atom probe techniques.
1.Hard magnetic property and nanostructure of Nd-Fe-B nanocomposite magnets
The effect of Ti and C additions on the microstructures and the magnetic properties of Nd-Fe-B isotropic nanocomposite has been investigated by transmission electron microscopy and three-dimensional atom probe techniques. The grain size was substantially refined by the addition of Ti due to the formation of Ti-enriched amorphous grain boundary. Also, the formation of hard magnetic Nd_2Fe_<14>B phase was promoted. Further addition of C enhanced the enrichment of Ti in the grain boundary phase, which led to the increase of coercivity and maximum energy product.
2.Age hardening behavior and nanoprecipitation of Mg alloys
Mechanical properties of Mg alloy are improved by addition of small amount of elements and the anneal process. It is thought that formation of nanocomposite by precipitation and grain boundary segregation causes the improvement. In order to understand the relation between nanostructure and mechanical property, TEM and 3DAP analyses has been done. From the change of nanostructure and elemental distribution due to the growth of precipitates, the effect for mechanical property was discussed.

Report

(3 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • Research Products

    (10 results)

All 2005 2004 Other

All Journal Article (10 results)

  • [Journal Article] TEM and 3DAP characterization of an age-hardened Mg-Ca-Zn alloy2005

    • Author(s)
      J.C.Oh
    • Journal Title

      Scripta Mater. 53

      Pages: 675-679

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Phase separation in Cu_<43>Zr_<43>Al_7Ag_7 bulk metallic glass2005

    • Author(s)
      J.C.Oh
    • Journal Title

      Scripta Mater. 53

      Pages: 165-169

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Platelet microstructure and magnetic properties in rapidly solidified Sm_<20.8>Co_<63.4>Fe_<7.9>Cu_<2.4>Zr_<1.6>B_4 ribbons2005

    • Author(s)
      R.Gopalan
    • Journal Title

      Scripta Mater. 53

      Pages: 367-371

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Characterization of nanocrystal dispersed Cu_<60>Zr_<30>Ti_<10> metallic glass2005

    • Author(s)
      D.Nagahama
    • Journal Title

      Mater. Trans. 46

      Pages: 1264-1270

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Characterization of nanocrystal dispersed Cu_<60>Zr_<30>Ti_<10> metallic glass2005

    • Author(s)
      D.Nagahama
    • Journal Title

      Mater.Trans. 46

      Pages: 1264-1270

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Rapidly solidified(FePt)_<70>P_<30>alloy with high coercivity2004

    • Author(s)
      A.A.Kundig
    • Journal Title

      Appl.Phys.Lett. 85(5)

      Pages: 789-791

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Effects of C and Ti additions on the microstructure of Nd-Fe-B nanocomposite magnets

    • Author(s)
      T.Ohkubo
    • Journal Title

      Mater. Sci. Eng. A (in press.)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Effect of C and Ti additions on the microstructure of Nd-Fe-B nanocomposite magnets

    • Author(s)
      T.Ohkubo
    • Journal Title

      Mater.Sci.Eng.A (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Nanoscale microstructure and magnetic properties of melt-spun Sm(Co_<0.725>Fe_<0.1>Cu_<0.12>Zr_<0.04>B_<0.015>)_<7.4> ribbons

    • Author(s)
      R.Gopalan
    • Journal Title

      J.Mag.Mag.Mater. (In Press)

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Chemistry of nanoscale precipitates in Mg-2.1Gd-0.6Y-0.2Zr(at.%)alloy investigated by the atom probe technique

    • Author(s)
      T.Honma
    • Journal Title

      Mat.Sci.Eng.A (In Press)

    • Related Report
      2004 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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