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Realisation of 3D In-situ Assessment of Local Crack Driving Forces via Ultra-high Resolution Synchrotron X-ray CT

Research Project

Project/Area Number 15560606
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionToyohashi University of Technology

Principal Investigator

TODA Hiroyuki  Toyohashi University of Technology, Associate Professor, 工学部, 助教授 (70293751)

Co-Investigator(Kenkyū-buntansha) KOBAYASHI Toshiro  Toyohashi University of Technology, Vice president, 副学長 (90023324)
Project Period (FY) 2003 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥2,200,000 (Direct Cost: ¥2,200,000)
Fiscal Year 2004: ¥800,000 (Direct Cost: ¥800,000)
Fiscal Year 2003: ¥1,400,000 (Direct Cost: ¥1,400,000)
KeywordsSynchrotron radiation / Micro-tomography / 3D observation / Crack driving force / Aluminum alloy / Damage / In-situ observation / Phase contrast / き列進展駆動力
Research Abstract

The procedure, by which real local crack driving forces (Modes I,II and III crack driving forced along crack front) can be measured in 3D, in-situ and in high density (at intervals less than 1 micron) via the sub-micrometer ultra-high resolution synchrotron radiation X-ray computed tomography (CT, hereinafter), has been developed in this study. This has been realized by microstructural tracking of several hundred features, and this can be further extended to several ten thousand features level. Measurements, which had been available only on specimen surface by the special material test procedures such as photoelasticity, Moire interferometry and caustics, have been readily applied to material interior. In general, the local crack driving forces are intricately and remarkably affected not only by macroscopic applied stress, but also by various crack shielding/anti-shielding effects, such as crack deflection, damage evolution and crack closure phenomenon, due to microstructures of the actual materials. The procedure developed has been applied to fatigue cracks propagating in aluminum alloys. The experiments were performed at the imaging beam lines BL20B2 and BL47XU of the SPring-8 and ID19 of the ESRF, and its feasibility was verified. By analyzing mechanisms of real local crack driving forces at each crack-tip point, the contributions by various crack shielding/anti-shielding effects, such as crack deflection, damage evolution and crack closure phenomenon, could be quantitatively clarified.
By doping Ga into nano-scopic structures such as grain boundaries, they could be visualized. The visualization of the grain boundary has been succeeded in casting materials, wrought materials and porous aluminum materials, which indicates the effectiveness of the technique developed.

Report

(3 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • Research Products

    (22 results)

All 2005 2004 2003 Other

All Journal Article (17 results) Publications (5 results)

  • [Journal Article] In-Situ High Resolution X-ray Tomography of Fracture Micromechanisms in Aluminium Foams2005

    • Author(s)
      H.Toda, T.Ohgaki, K.Uesugi
    • Journal Title

      Research Frontiers (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In-situ observation of fracture of aluminium foam using synchrotron X-ray microtomography2005

    • Author(s)
      H.Toda, T.Ohgaki, K.Uesugi, K.Makii, Y.Aruga, A.Toshikazu, M.Niinomi, T.Kobayashi
    • Journal Title

      Key Engng.Mater. (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] True-3D strain mapping for assessment of material deformation by synchrotron X-ray microtomography2005

    • Author(s)
      J.Ahn, H.Toda, M.Niinomi, T.Kobayashi
    • Journal Title

      Review of Progress in Quantitative NDE (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In-Situ High Resolution X-ray Tomography of Fracture Micromechanisms in Aluminium Foams2005

    • Author(s)
      H.Toda, T.Ohgaki, K.Uesugi
    • Journal Title

      Research Frontiers (In press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In-situ observation of fracture of aluminium foam using synchrotron X-ray microtomography2005

    • Author(s)
      H.Toda, T.Ohgaki, K.Uesugi, K.Makii, Y.Aruga, A.Toshikazu, M.Niinomi, T.Kobayashi
    • Journal Title

      Key Engng.Mater. (In press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In-Situ High Resolution X-ray Tomography of Fracture Micromechanisms in Aluminium Foams2005

    • Author(s)
      H.Toda, T.Ohgaki, K.Uesugi
    • Journal Title

      Research Frontiers 印刷中

    • Related Report
      2004 Annual Research Report
  • [Journal Article] In-situ observation of fracture of aluminium foam using synchrotron X-ray microtomography2005

    • Author(s)
      H.Toda, T.Ohgaki, K.Uesugi, K.Makii, Y.Aruga, A.Toshikazu, M.Niinomi, T.Kobayashi
    • Journal Title

      Key Engng.Mater. 印刷中

    • Related Report
      2004 Annual Research Report
  • [Journal Article] True-3D strain mapping for assessment of material deformation by synchrotron X-ray microtomography2005

    • Author(s)
      J.Ahn, H.Toda, M.Niinomi, T.Kobayashi
    • Journal Title

      Review of Progress in Quantitative NDE 印刷中

    • Related Report
      2004 Annual Research Report
  • [Journal Article] 高分解能X線CTによる可視化技術の進歩:材料内部の局所力学量のin-situ測定への応用2004

    • Author(s)
      戸田裕之, 小林俊郎, 大垣智巳
    • Journal Title

      材料試験技術 Vol.48

      Pages: 5-10

    • NAID

      80016412890

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] In-situ high resolution synchrotron X-ray tomography of crack closure micromechanisms2004

    • Author(s)
      K.H.Khor, H.Toda, J.-Y.Buffiere, W.Ludwig, H.S.Ubhi, P.J.Gregson, I.Sinclair
    • Journal Title

      Journal of Physics : Condensed Matter 16

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Proposal of 3D high-density measurement procedure of internal local crack driving forces by sub-micrometer resolution synchrotron X-ray microtomography2004

    • Author(s)
      H.Toda, I.Sinclair, J.-Y.Buffiere, E.Maire, K.H.Khor, P.Gregson, T.Kobayashi
    • Journal Title

      Acta Materialia 52

      Pages: 1305-1317

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Progress in visualization techniques via high-resolution X-ray CT : Application to in-situ measurement of local mechanical quantities inside materials2004

    • Author(s)
      H.Toda, T.Kobayashi, T.Ohgaki
    • Journal Title

      Materials testing techniques Vol.48 No.1

      Pages: 5-10

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] True-3D strain mapping for assessment of material deformation by synchrotron X-ray microtomography2004

    • Author(s)
      J.Ahn, H.Toda, M.Niinomi, T.Kobayashi
    • Journal Title

      Review of Progress Quantitative NDE (In press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] In-situ high resolution synchrotron X-ray tomography of crack closure micromechanisms2004

    • Author(s)
      K.H.Khor, H.Toda, J.-Y.Buffiere, W.Ludwig, H.S.Ubhi, P.J.Gregson I.Sinclair
    • Journal Title

      Journal Physics : Condensed Matter 16

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Proposal of 3D high-density measurement procedure of internal local crack driving forces by sub-micrometer resolution synchrotron X-ray microtomography2004

    • Author(s)
      H.Toda, I.Sinclair, J.-Y.Buffiere, E.Maire, K.H.Khor, P.Gregson, T.Kobayashi
    • Journal Title

      Acta Materialia Vol.52 No.5

      Pages: 1305-1317

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Assessment of fatigue crack closure phenomenon in damage tolerant aluminium alloy by in-situ high-resolution synchrotron X-ray microtomography2003

    • Author(s)
      H.Toda, I.Sinclair, J.-Y.Buffiere, E.Maire, T.Connolley, M.Joyce, K.H.Khor, P.Gregson
    • Journal Title

      Philosophical Magazine A 83

      Pages: 2429-2448

    • NAID

      120006309088

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Journal Article] Assessment of fatigue crack closure phenomenon in damage tolerant aluminium alloy by in-situ high-resolution synchrotron X-ray microtomography2003

    • Author(s)
      H.Toda, I.Sinclair, J.-Y.Buffiere, E.Maire, T.Connolley, M.Joyce, K.H.Khor, P.Gregson
    • Journal Title

      Philosophical Magazine A Vol.83 No.21

      Pages: 2429-2448

    • NAID

      120006309088

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Publications] 戸田裕之, 小林俊郎, 大垣智巳: "高分解能X線CTによる可視化技術の進歩:材料内部の局所力学量のin-situ測定への応用"材料試験技術. Vol.48 No.1. 5-10 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] K.H.Khor, H.Toda, J.-Y.Buffiere, W.Ludwig, H.S.Ubhi他: "In-situ high resolution synchrotron X-ray tomography of crack closure micromechanisms"Journal of Physics : Condensed Matter. (印刷中). (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] H.Toda, I.Sinclair, J.-Y.Buffiere, E.Maire, K.H.Khor, P.Gregson, T.Kobayshi: "Proposal of 3D high-density measurement procedure of internal local crack driving forces by sub-micrometer resolution synchrotron X-ray microtomography"Acta Materialia. Vol.52 No.5. 1305-1317 (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] K.H.Khor, M.Joyce, T.Connolley, H.Toda, I.Sinclair, E.Maire, J.-Y.Buffiere: "Synchrotron Microtomography of Fatigue Crack Closure"2002 ESRF Scientific Highlights. 79-80 (2003)

    • Related Report
      2003 Annual Research Report
  • [Publications] H.Toda, I.Sinclair, J.-Y.Buffiere, E.Maire, T.Connolley, M.Joyce他: "Assessment of fatigue crack closure phenomenon in damage tolerant aluminium alloy by in-situ high-resolution synchrotron X-ray microtomography"Philosophical Magazine A. Vol.83 No.21. 2429-2448 (2003)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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