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The measurements by the back surface laser flash method and the construction of the database on thermal conductivity of silicate melts.

Research Project

Project/Area Number 15560640
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Metal making engineering
Research InstitutionIbaraki University

Principal Investigator

OHTA Hiromichi  Ibaraki University, the College of Engineering, Associate professor, 工学部, 助教授 (70168946)

Project Period (FY) 2003 – 2004
Project Status Completed (Fiscal Year 2004)
Budget Amount *help
¥3,200,000 (Direct Cost: ¥3,200,000)
Fiscal Year 2004: ¥1,300,000 (Direct Cost: ¥1,300,000)
Fiscal Year 2003: ¥1,900,000 (Direct Cost: ¥1,900,000)
Keywordsthermal conductivity / thermal diffusivity / silicate melts / slag / structure of melts / laser flash method / high temperature / thermophysical properties / 熱移動 / 熱伝率導 / 高温融体 / シリケート
Research Abstract

In the metal refinement process, the request of environmental loading reduction has become intensified, and a grasp of the heat transfer phenomenon of the system is indispensable for the design. The measurement of the thermal property of silicate melt of the high temperature in the process is carried out in proportion to these requests. However, thermal conductivity thermal conductivity of the high-temperature region of the silicate melt which is one of the most important physical property in heat transfer of the refining process the measured value is greatly different by measuring method, and the value with the high reliability has not been obtained yet.
In this study, this problem is approached from two directions. One is to evaluate the values derived in the conventional study and stores them into database. The other is to establish the measuring method with the high reliability based on the new principle.
In this study, the thin platinum crucible is filled with the silicate melt sample, and the pulse heating is irradiated on the bottom surface of the crucible. The thermal conductivity of the alumina/silica/calcia system slag was measured by this technique from the temperature response of platinum crucible after irradiation. With the measured results and database, two models were examined. One is the model in which a heat propagates through the network of Si-O-Si of the silicate. The other is the model in which the heat transfer depends on the regularity of the structure in the melt.
The model in which a heat propagates through the network of Si-O-Si does not explain the experimental result well. While the model that thermal conductivity depends on the regularity of the structure is rather effective considering that higher thermal conductivity at liquid state is observed in the vicinity of the corresponding composition of the crystal phases in solid state.

Report

(3 results)
  • 2004 Annual Research Report   Final Research Report Summary
  • 2003 Annual Research Report
  • Research Products

    (9 results)

All 2006 2004 2003 Other

All Journal Article (6 results) Book (1 results) Publications (2 results)

  • [Journal Article] Thermal conductivity CaO-Al_2O_3-SiO_2 slag2006

    • Author(s)
      Hiromichi Ohta, Hiroyuki Shibata
    • Journal Title

      Metallurgical and Materials Transactions 37A(発表予定)

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Measurement of Physical Properties of Slag Formed Around The Raceway in The Working Blast Furnace2004

    • Author(s)
      Shinichi Inaba, Yoshio Kmura, Hiroyuki Shibata, Hiromichi Ohta
    • Journal Title

      ISIJ International 44

      Pages: 2120-2126

    • NAID

      10014239951

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Measurement of Physical Properties of Slag Formed Around The Raceway in The Working Blast Furnace2004

    • Author(s)
      Shinichi Inaba, Yoshio Kmura, Hiroyuki Shibata, Hiromichi Ohta
    • Journal Title

      ISIJ International 44-12

      Pages: 2120-2126

    • NAID

      10014239951

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Measurement of physical properties of slag formed around the raceway in the working blast furnace2004

    • Author(s)
      Shinichi Inaba, Yoshio Kmura, Hiroyuki Shibata, Hromichi Ohta
    • Journal Title

      ISIJ International 44[12]

      Pages: 2120-2126

    • NAID

      10014239951

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Measurement of Thermal Transport Properties for Molten Silicate Glasses at High Temperatures by means of a Novel Laser Flash Technique

    • Author(s)
      Hiroyuki Shibata, Atsushi Suzuki, Hiromichi Ohta
    • Journal Title

      Materials Transactions 46(印刷中)

    • NAID

      130004823918

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Journal Article] Measurement of Thermal Transport Properties for Molten Silicate Glasses at High Temperatures by means of a Novel Laser Flash Technique

    • Author(s)
      Hiroyuki Shibata, Atsushi Suzuki, Hiromichi Ohta
    • Journal Title

      Materials Transactions 46 (Printing)

    • NAID

      130004823918

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2004 Final Research Report Summary
  • [Book] 融体材料の熱拡散率測定(最新熱測定-基礎から応用まで-,八田一郎監修)2003

    • Author(s)
      太田弘道, 柴田浩幸, 早稲田嘉夫
    • Publisher
      アグネ技術センター
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2004 Annual Research Report 2004 Final Research Report Summary
  • [Publications] H.Ohta H.Shibata, Y.Waseda: "Thermal Conductivity and Diffusivity of Molten Slags by Laser Flash Method"Metallurgical and Materials Transactions A. 36A(発表予定). (2006)

    • Related Report
      2003 Annual Research Report
  • [Publications] 太田弘道, 柴田浩幸, 早稲田嘉夫 (分担執筆:八田一郎 監修・アルバック理工 編集): "融体材料の熱拡散率測定(最新熱測定-基礎から応用まで-)"アグネ技術センター. 11(392) (2003)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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