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Containerless Process for the Spherical Single Crystal Semiconductor Silicon by the Gas Jet Flow Type Electromagnetic Levitation.

Research Project

Project/Area Number 15560646
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Metal making engineering
Research InstitutionShibaura Institute of Technology

Principal Investigator

NAGAYAMA Katsuhisa  Shibaura Institute of Technology, Faculty of Engineering, Professor, 工学部, 教授 (80189167)

Project Period (FY) 2003 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥3,000,000 (Direct Cost: ¥3,000,000)
Fiscal Year 2006: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 2005: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 2004: ¥700,000 (Direct Cost: ¥700,000)
Fiscal Year 2003: ¥900,000 (Direct Cost: ¥900,000)
KeywordsContainerless process / Gas jet flow type electromagnetic levitation / Homogeneous nucleation / Spherical single crystal semiconductor Si / Undercoold Si melt / Nucleation / Undercooling / Crystal growth / 電磁溶融プロセス / ガスジェット浮遊 / ガスジェツト浮遊 / 高過冷度 / 低過冷度
Research Abstract

I researched and discussed the fabrication for the spherical single crystal semiconductor Si by using the gas jet flow type electromagnetic levitating process which is one of the containerless process. As with space, this levitating process can solidify metals and semiconductor without convection and container at ground level. Also, this process is new process which enables the high cooling rate and can detects the nucleation from undercooled Si melt. Furthermore, in view of the interaction between Si and high-frequency magnetic field, the sample for electromagnetic levitation is used the surface of high pure(99.999%) Si coated C or B by a high vaccum deposition apparatus. According to the results, this process enabels the containerless solidification for the B or C coated Si. Thereby, the validity of the new electromagnetic levitating process for B or C coated Si is clarified. Also, the undercooling ΔT is 150 K and 200 K for C or B coated Si, respectively. The cooling rate from the cooling start to the detection limit for pyrometer is 110 K/s and 300 K/s for C or B coated Si, respectively. Although crystal growth mode at lower undercoolings of C coated Si samples is faceted growth on the surface, the crystal growth mode of surface Si at higher undercoolings of samples is dendrite grown on the surface. Also, I obtained the a quantitative results about the relation between deposition time and solidification with undercooling of Si sample. From XRD measurements and SEM observation, the Si grain refinement with increasing the undercooling existed and the preferential growth orientation changes with increasing undercooling. As the results, I obtained the high validity of this process and the quantitative data.

Report

(5 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • 2004 Annual Research Report
  • 2003 Annual Research Report
  • Research Products

    (31 results)

All 2007 2006 2005 Other

All Journal Article (26 results) Publications (5 results)

  • [Journal Article] Undercooling Solidification Brehavior of C or B Coated Si by Electromagnetic Levitating Process2007

    • Author(s)
      Yusuke Sakuta, Shuji Azumo, Katsuhisa Nagayama
    • Journal Title

      Proc.of Third International Symposium on Physical Scence in Space 2007 3(in press)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Undercooling Solidification Behavior of C or B Coated Si by Electromagnetic Levitating Process.2007

    • Author(s)
      Yusuke Sakuta, Shuji Azumo, Katsuhisa Nagayama
    • Journal Title

      Proc.of Third International Symposium on Physical Science in Space 2007 (inpress)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Nd-Fe及びPr-Fe2元高保磁力非平衡相生成に対するガスジェット浮遊プロセスの効果2007

    • Author(s)
      米村 寛, 東雲 秀司, 永山 勝久
    • Journal Title

      日本金属学会2007年度140回春期講演大会概要(2007年3月27日) 140

      Pages: 532-532

    • Related Report
      2006 Annual Research Report
  • [Journal Article] 局在かつ遍歴電子間結合を利用した非平衡生成と構造及び磁性2007

    • Author(s)
      杉山 智瑛, 永山 勝久
    • Journal Title

      日本金属学会2007年度140回春期講演大会概要(2007年3月27日) 140

      Pages: 529-529

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Amorphous Formation and Magnetic Properties of Nd-Fe-Co-Al Alloys by Gas Flow Type Levitation2006

    • Author(s)
      Shuji Azumo, Seichi Utsuno, Katsuhisa Nagayama
    • Journal Title

      Materials Transaction, JIM 47

      Pages: 2842-2845

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Bulk Amorphous Formation and Magnetic Properties of Nd-Fe-Co-Al Alloys by the New Gas Jet Flow Type Levitating Process2006

    • Author(s)
      Shuji Azumo, Seichi Utsuno, Katsuhisa Nagayama
    • Journal Title

      Materials Transaction, JIM 47

      Pages: 1568-1571

    • NAID

      10018160674

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] ガスジェット浮遊電磁溶融プロセスを用いた希土類-遷移金属-Al系バルクアモルファス生成とNd-Fe系非平衡相の高保磁力発現2006

    • Author(s)
      永山 勝久, 宇都野 正史, 東雲 秀司
    • Journal Title

      日本マイクログラビティ応用学会誌 23

      Pages: 8-14

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] ガスジェット浮遊型電磁溶融プロセスによって作製したLa-Cu-Ni-Co-AlおよびNd-Fe-Co-Al系バルク状近似アモルファス合金2006

    • Author(s)
      東雲 秀司, 宇都野 正史, 永山 勝久
    • Journal Title

      日本金属学会誌 70

      Pages: 138-141

    • NAID

      10017283570

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Amorphous Formation and Magnetic Properties of Nd-Fe-Co-Al Alloys by Gas Flow Type Levitation Process.2006

    • Author(s)
      Shuji Azumo, Katsuhisa Nagayama
    • Journal Title

      Materials Transactions., The Japn Institute of Metals 47

      Pages: 2842-2845

    • NAID

      10019277264

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Bulk Amorphous Formation and Magnetic Properties of Nd-Fe-Co-Al Alloys by the New Gas jet Flow Type Levitation Process.2006

    • Author(s)
      Shuji Azumo, Seichi Utsuno, Katsuhisa Nagayama
    • Journal Title

      Materials Transactions., The Japn Institute of Metals 47

      Pages: 1568-1571

    • NAID

      10018160674

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Bulk Amorphous Formation of LRE-TM-Al Systems and High Coecivity of Metastable Phase in Highly Undercooled Nd-Fe Systems by Using The New Gas Jet Flow Type Electromagnetic Levitation Process.2006

    • Author(s)
      Shuji Azumo, Seichi Utsuno, Katsuhisa Nagayama
    • Journal Title

      J.Japan Soc.Microgravity Appl. 23

      Pages: 8-14

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Bulk Approximate Amorphous Formation and Magnetic Properties of Nd-Fe-Co-Al Alloys by the New Gas Jet Type Levitating Process.2006

    • Author(s)
      Katsuhisa Nagayama, Seichi Utsuno, Shuji Azumo
    • Journal Title

      J.Japan Inst.Metals 70

      Pages: 138-141

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Amorphous Formation and Magnetic Properties of Nd-Fe-Co-Al Alloys by Gas Flow Typo Lovitation2006

    • Author(s)
      Shuji Azumo, Katsuhisa Nagayama
    • Journal Title

      Materials Transaction, JIM 47

      Pages: 2842-2845

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Bulk Amorphous Formation and Magnetic Properties of Nd-Fe-Co-Al Alloys by the New Gas Jet Flow Type Levitating Process2006

    • Author(s)
      Shuji Azumo, Seichi Utsuno, Katsuhisa Nagyama
    • Journal Title

      Materials Transaction, JIM 47

      Pages: 1568-1571

    • Related Report
      2006 Annual Research Report
  • [Journal Article] ガスジェット浮遊電磁溶融プロセスを用いた希土類-偏移金属-Al系バルクアモルファス生成とNd-Fe系非平衡相の高保磁力発現2006

    • Author(s)
      永山 勝久, 宇都野 正史, 東雲 秀司
    • Journal Title

      日本マイクログラビティ応用学会誌 23

      Pages: 8-14

    • Related Report
      2006 Annual Research Report
  • [Journal Article] ガスジェット浮遊型電磁溶融プロセスによって作成したLa-Cu-Ni-Co-AlおよびNd-Fe-Co-Al系バルク状近似アモルファス合金2006

    • Author(s)
      東雲 秀司, 宇都野 正史, 永山 勝久
    • Journal Title

      日本金属学会誌 70

      Pages: 138-141

    • Related Report
      2006 Annual Research Report
  • [Journal Article] ガスジェット浮遊型電磁溶融プロセスによって作製したLa-Cu-Ni-Co-AlおよびNd-Fe-Co-Al系バルク状近似アモルファス合金2006

    • Author(s)
      永山勝久, 東雲秀司, 宇都野正史
    • Journal Title

      日本金属学会誌 70巻・2号

      Pages: 138-141

    • NAID

      10017283570

    • Related Report
      2005 Annual Research Report
  • [Journal Article] ガスジェット浮遊電磁溶融プロセスを用いた軽希土類-遷移金属-Al系バルクアモルファス生成とNd-Fe系非平衡相の高保磁力発現2006

    • Author(s)
      永山勝久, 宇都野正史, 東雲秀司
    • Journal Title

      日本マイクログラビティ応用学会誌 Vol.23

      Pages: 8-14

    • NAID

      10017253772

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Bulk Amorphous Formation and Magnetic Properties of Nd-Fe-Co-Al Alloys by the New Gas Jet Flow Type Levitating Process2006

    • Author(s)
      Katsuhisa Nagayama, Shuji Azumo, Seishi Utsuno
    • Journal Title

      Materials Transaction, JIM (Accepted)

    • NAID

      10018160674

    • Related Report
      2005 Annual Research Report
  • [Journal Article] ガスジェット浮遊プロセスによるNd-Fe-CO-Al系アモルファス合金の構造と磁性2006

    • Author(s)
      永山勝久, 東雲秀司
    • Journal Title

      日本金属学会2006年度138回春期講演大会概要(2006年3月22日発表)

      Pages: 410-410

    • Related Report
      2005 Annual Research Report
  • [Journal Article] La55A125Cu10Ni5Co55 元SiCウイスカー添加合金の過冷凝固過程とバルクアモルファス生成2005

    • Author(s)
      東雲 秀司, 永山 勝久
    • Journal Title

      日本金属学会誌 69

      Pages: 399-401

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Undercooling solidification Behavior and Bulk Amorphous Formation of La_<55>Al_<25>Cu_<10>Ni5Co_5 Alloys with SiC Whisker Addition.2005

    • Author(s)
      Shuji Azumo, Katsuhisa Nagayama
    • Journal Title

      J.Japan Inst.Metals 69

      Pages: 399-401

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] ガスジェット型電磁浮遊炉を用いたNd-Fe系高保磁力強磁性非平衡相の過冷凝固過程と磁性2005

    • Author(s)
      永山勝久, 宇都野正史, 小田克郎
    • Journal Title

      第21回 宇宙利用シンポジウム プロシーディング(Proc. The Twenty-first Space Utilization Symposium) Vol.21

      Pages: 5-8

    • Related Report
      2005 Annual Research Report
  • [Journal Article] La_<55>Al_<25>Cu_<10>Ni_5Co_5 5元SiCウイスカー添加合金の過冷凝固過程とバルクアモルファス生成2005

    • Author(s)
      永山 勝久, 東雲 秀司
    • Journal Title

      日本金属学会誌 69巻・4号

      Pages: 399-401

    • NAID

      10015521175

    • Related Report
      2005 Annual Research Report
  • [Journal Article] ガスジェット型電磁浮遊炉を用いたNd-Fe系高保磁力強磁性非平衡相の過冷凝固過程と磁性2005

    • Author(s)
      永山勝久, 宇都野正史, 小田克郎
    • Journal Title

      第21回 宇宙利用シンポジウム プロシーディング(Proc.The Twenty-first Space Utilization Symposium) Vol.21

      Pages: 5-8

    • Related Report
      2004 Annual Research Report
  • [Journal Article] La_<55>Al_<25>Cu_<10>Ni_5Co_5 5次元SiCウイスカー添加合金の過冷凝固過程とバルクアモルファス生成2005

    • Author(s)
      永山 勝久, 東雲 秀司
    • Journal Title

      日本金属学会誌 69巻・4号(現在、製本中)

    • Related Report
      2004 Annual Research Report
  • [Publications] 永山 勝久, 糸井真司: "ガスジェット型電磁浮遊炉を用いた球状単結晶Si創製に対する無容器プロセシング"日本金属学会2004年度第134回春期講演大会概要. (2004年3月発表予定). (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 永山 勝久, 蓑輪 泉: "電磁溶融プロセスを用いたGe-Si半導体および,A1系偏晶合金の組織生成に対する冷却速度依存性"日本金属学会2004年度第134回春期講演大会概要. (2004年3月発表予定). (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 永山勝久, 堀越昭太郎: "Nd2Fe14B初晶面組成試料を用いたガスジェット浮遊溶融に伴う主相核生成と粒界相形成"日本金属学会2004年度第134回春期講演大会概要. (2004年3月発表予定). (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 永山 勝久, 東雲 秀司: "ガスジェット浮遊炉を用いたLa55Al25Cu10Ni5Co5 5元SiC添加試料の過冷凝固過程とバルクアモルファス生成"日本金属学会2004年度第134回春期講演大会概要. (2004年3月発表予定). (2004)

    • Related Report
      2003 Annual Research Report
  • [Publications] 永山 勝久, 本多 啓二: "軽希土類-遷移金属系合金の巨大過冷却発現に対する無容器プロセスの効果"日本金属学会2004年度第134回春期講演大会概要. (2004年3月発表予定). (2004)

    • Related Report
      2003 Annual Research Report

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Published: 2003-04-01   Modified: 2016-04-21  

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