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Development of environmentally conscious cleaning method using cryogenic fine solid particles and its application to high density hydrogen storage

Research Project

Project/Area Number 15H03913
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Fluid engineering
Research InstitutionTohoku University

Principal Investigator

ISHIMOTO JUN  東北大学, 流体科学研究所, 教授 (10282005)

Co-Investigator(Kenkyū-buntansha) 堀邊 英夫  大阪市立大学, 大学院工学研究科, 教授 (00372243)
松浦 一雄  愛媛大学, 大学院理工学研究科, 准教授 (20423577)
真田 俊之  静岡大学, 大学院総合科学技術研究科, 准教授 (50403978)
Co-Investigator(Renkei-kenkyūsha) OCHIAI NAOYA  東北大学, 流体科学研究所, 助教 (40614508)
Research Collaborator Combescure Alain  INSA de Lyon, LaMCoS, 教授
Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥17,030,000 (Direct Cost: ¥13,100,000、Indirect Cost: ¥3,930,000)
Fiscal Year 2017: ¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Fiscal Year 2016: ¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2015: ¥10,140,000 (Direct Cost: ¥7,800,000、Indirect Cost: ¥2,340,000)
Keywords混相流 / 極低温 / 微粒化 / 流体解析 / 噴霧 / 半導体洗浄 / 超高熱流束 / 冷却 / ナノ洗浄
Outline of Final Research Achievements

The application of cryogenic high-speed spray of micro-solid nitrogen (SN2) to the non-aqueous resist-removal and ultra-cleaning system of semiconductor wafer is a focus of great interest.
In the present study, we have newly developed the new single-component micro-nano SN2 particle production method by using super adiabatic Laval nozzle (converging-diverging nozzle). The physical photo resist removal-cleaning performance using cryogenic particulate spray are investigated by a new type of integrated ToF-SIMS, XPS measurement coupled supercomputing technique. As a result, it has been clarified that the newly developed cryogenic spray cleaning method is effective particularly for the removal and cleaning process of novolac type resists.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Annual Research Report
  • 2015 Annual Research Report
  • Research Products

    (39 results)

All 2017 2016 2015 Other

All Int'l Joint Research (5 results) Journal Article (11 results) (of which Int'l Joint Research: 2 results,  Peer Reviewed: 11 results,  Acknowledgement Compliant: 5 results,  Open Access: 1 results) Presentation (22 results) (of which Int'l Joint Research: 17 results,  Invited: 8 results) Patent(Industrial Property Rights) (1 results)

  • [Int'l Joint Research] Wroclaw University of Sci. and Tech.(Poland)

    • Related Report
      2017 Annual Research Report
  • [Int'l Joint Research] INSA de Lyon(France)

    • Related Report
      2017 Annual Research Report
  • [Int'l Joint Research] Wroclaw University of Sci. and Tech.(Poland)

    • Related Report
      2016 Annual Research Report
  • [Int'l Joint Research] INSA de Lyon(France)

    • Related Report
      2016 Annual Research Report
  • [Int'l Joint Research] Wroclaw Univ. of Science and Technology(Poland)

    • Related Report
      2015 Annual Research Report
  • [Journal Article] Computational approach for hydrogen leakage with crack propagation of pressure vessel wall using coupled particle and Euler method2017

    • Author(s)
      Jun Ishimoto, Toshinori Sato, Alain Combescure
    • Journal Title

      International Journal of Hydrogen Energy

      Volume: 42 Issue: 15 Pages: 10656-10682

    • DOI

      10.1016/j.ijhydene.2017.01.161

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Numerical investigation of multiple-bubble behaviour and induced pressure in a megasonic field2017

    • Author(s)
      Naoya Ochiai and Jun Ishimoto
    • Journal Title

      Journal of Fluid Mechnics

      Volume: 印刷中 Pages: 562-594

    • DOI

      10.1017/jfm.2017.154

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Vitrification of Biological Cells Using a Cryogenic Fine Solid Particulate Spray2017

    • Author(s)
      Jun Ishimoto
    • Journal Title

      Interdisciplinary Information Sciences

      Volume: 23 Issue: 2 Pages: 167-170

    • DOI

      10.4036/iis.2017.S.01

    • NAID

      130006287943

    • ISSN
      1340-9050, 1347-6157
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Computational study for dynamic crack propagation in pressure vessel wall with hydrogen leakage using coupled particle and Euler method2017

    • Author(s)
      Jun Ishimoto, Toshinori Sato and Alain Combescure
    • Journal Title

      Proceedings of the Fifth International Conference on Computational Modeling of Fracture and Failure of Materials and Structures (CFRAC 2017)

      Volume: -

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Integrated Computational Study for Total Atomization Process of Primary Breakup to Spray Droplet Formation in Injector Nozzle2016

    • Author(s)
      Ochiai, N., Ishimoto, J., Arioka, A., Yamaguchi, N., Sasaki, Y., and Furukawa, N.
    • Journal Title

      SAE Technical Paper

      Volume: 2016-02-3303

    • DOI

      10.4271/2016-01-2202

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Micro-Solid Nitrogen Particulate Spray Cooling Characteristics and its Application to Wafer Cleaning Technology2016

    • Author(s)
      Jun Ishimoto
    • Journal Title

      Proceedings of 1st Asian ICMC and CSSJ 50th Anniversary Conference

      Volume: -

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] FSI Approach of Hydrogen Leakage Problems with Crack Propagation2016

    • Author(s)
      Jun Ishimoto, Toshinori Sato and Alain Combescure
    • Journal Title

      Proceedings of the TFC ELyT Workshop 2016

      Volume: -

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Development of Environmental Harmony Resist Removal System using Cryogenic Particulate Spray2015

    • Author(s)
      Jun Ishimoto and Hideo Horibe
    • Journal Title

      Journal of Photopolymer Science and Technology

      Volume: 28 Issue: 2 Pages: 285-288

    • DOI

      10.2494/photopolymer.28.285

    • NAID

      130005093859

    • ISSN
      0914-9244, 1349-6336
    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Computational prediction of cryogenic micro-nano solid nitrogen particle production using Laval nozzle for physical photo resist removal-cleaning technology2015

    • Author(s)
      Jun Ishimoto, Haruto Abe and Naoya Ochiai
    • Journal Title

      Physics Procedia

      Volume: 28 Pages: 607-612

    • DOI

      10.1016/j.phpro.2015.06.103

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Computational Study of the Dynamics of Two Interacting Bubbles in a Megasonic Field2015

    • Author(s)
      Naoya Ochiai and Jun Ishimoto
    • Journal Title

      Ultrasonics Sonochemistry

      Volume: 26 Pages: 351-360

    • DOI

      10.1016/j.ultsonch.2015.04.005

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Computational study of the dynamics of two interacting bubbles in a megasonic field2015

    • Author(s)
      Naoya Ochiai and Jun Ishimoto
    • Journal Title

      Ultrasonics Sonochemistry

      Volume: 26 Issue: 3 Pages: 351-360

    • DOI

      10.1016/j.cryobiol.2015.10.046

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Computationally Assisted Study for Cryogenic Fine Particulate Spray in Application to Photoresist-Removal Cleaning Technology2017

    • Author(s)
      Jun Ishimoto
    • Organizer
      The 26th Surface Cleaning Users Group Meeting, Cleaning Technology Symposium (KSCUGM), October 26 (2017) Hanyang University, ERICA Campus, Ansan, Korea
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Computational study for dynamic crack propagation in pressure vessel wall with hydrogen leakage using coupled particle and Euler method2017

    • Author(s)
      Jun Ishimoto, Toshinori Sato and Alain Combescure
    • Organizer
      Fifth International Conference on Computational Modeling of Fracture and Failure of Materials and Structures (CFRAC 2017), 14-16 June 2017, La Cite;, Nantes Events Center, Nantes, France
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Coupled Computing of Hydrogen Leakage with Crack Propagation Using Hybrid Particle and Euler Method2017

    • Author(s)
      Jun Ishimoto, Toshinori Sato and Alain Combescure
    • Organizer
      Fourth International Symposium on Smart Layered Materials and Structures for Energy Saving, Nov. 1, 2017, Sendai International Center, Sendai, Japan
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Coupled Analysis of High-Density Hydrogen Safety Management2017

    • Author(s)
      Jun Ishimoto and Alain Combescure
    • Organizer
      The 17th International Symposium on Advanced Fluid Information (AFI-2017), Nov. 2, 2017, Sendai International Center, Sendai, Japan
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Micro-Solid Nitrogen Particulate Spray Cooling Characteristics and its Application to Wafer Cleaning Technology2016

    • Author(s)
      Jun Ishimoto
    • Organizer
      1st Asian ICMC and CSSJ 50th Anniversary Conference, Nov. 8, 2016, Kanazawa Kageki-za, Kanazawa, Japan
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Supercomputing of Tsunami Damage Mitigation Using Offshore Mega-Floating Structure2016

    • Author(s)
      Jun Ishimoto
    • Organizer
      International Innovation Workshop on Tsunami, Snow Avalanche & Flash Flood Energy Dissipation, January 21-22, 2016, Maison Villemanzy in Lyon, France
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Integrated Computational Study for Total Atomization Process of Primary Breakup to Spray Droplet Formation in Injector Nozzle2016

    • Author(s)
      Naoya Ochiai
    • Organizer
      SAE 2016 International Powertrains, Fuels & Lubricants Meeting, October 24-26, 2016, Baltimore, Maryland, USA
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] FSI Approach of Hydrogen Leakage Problems with Crack Propagation2016

    • Author(s)
      Jun Ishimoto
    • Organizer
      TFC ELyT Workshop 2016, October 6-8, 2016, Miyagi Zao Royal Hotel, Japan
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Computational Study of Unsteady Cavitation in High-Speed Submerged Water Jet2016

    • Author(s)
      Naoya Ochiai
    • Organizer
      The Fourth International Symposium on Innovative Energy Research III, Multiphase Energy Science and Disaster Damage Mitigation Technology Related to FSI Analysis, Oct. 10, 2016, Sendai
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Numerical Model and Computing of Freezing Front Propagation of Biological Cell Suspension2016

    • Author(s)
      Przemyslaw Smakulski
    • Organizer
      The Fourth International Symposium on Innovative Energy Research III, Multiphase Energy Science and Disaster Damage Mitigation Technology Related to FSI Analysis, Oct. 10, 2016, Sendai
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Coupled Analysis of High-Density Hydrogen Safety Management2016

    • Author(s)
      Jun Ishimoto
    • Organizer
      13th International Conference on Flow Dynamics (ICFD2016), Oct. 10-12, 2016, Sendai International Center, Sendai, Japan
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Multiphase Fluid Dynamic Approach for Fire Whirl Risk Mitigation2016

    • Author(s)
      Jun Ishimoto
    • Organizer
      13th International Conference on Flow Dynamics (ICFD2016), Oct. 10-12, 2016, Sendai International Center, Sendai, Japan
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 極低温微細固体粒子噴霧を用いた各種細胞のガラス凍結2016

    • Author(s)
      石本淳
    • Organizer
      BioJapan 2016, October 12-14, 2016, Pacifico Yokohama, Japan
    • Related Report
      2016 Annual Research Report
    • Invited
  • [Presentation] ブリッジツールを用いたVOF-Lagrangeハイブリッド噴霧微粒化シミュレーション法の開発2016

    • Author(s)
      石本淳
    • Organizer
      ICSC 2016, CONVERGE Conference Day, 2016年11月17日(木), 横浜ベイホテル東急, Yokohama, Japan
    • Related Report
      2016 Annual Research Report
    • Invited
  • [Presentation] メガソニック場中の複数気泡並進運動メカニズムの数値的解明2016

    • Author(s)
      森 勇人
    • Organizer
      混相流シンポジウム2015 オーガナイズドセッション(OS-5 サステナブル異分野融合型混相流),2016年8月8日(月)~10日(水),同志社大学 今出川キャンパス(京都市)
    • Related Report
      2016 Annual Research Report
  • [Presentation] ラバルノズル内における固相変化を伴う極低温微粒化と粒子衝突挙動に関する数値予測2016

    • Author(s)
      関田健雄
    • Organizer
      日本機械学会流体工学部門講演会,2016年11月12日~13日,山口大学(宇部市)
    • Related Report
      2016 Annual Research Report
  • [Presentation] Supercomputing of Multiscale Multiphase Flow Related to Industrial Field and Natural Disaster Problems2015

    • Author(s)
      Jun Ishimoto
    • Organizer
      11th Korea-Japan CFD Workshop (KJCFD2015)
    • Place of Presentation
      Kyushu University, Fukuoka, Japan
    • Year and Date
      2015-12-16
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] ラバルノズル内における固相変化を伴う極低温混相流動特性に関する数値解析2015

    • Author(s)
      阿部開史,石本 淳,落合直哉
    • Organizer
      日本機械学会 第93期 流体工学部門 講演会
    • Place of Presentation
      東京理科大学 葛飾キャンパス(東京都葛飾区)
    • Year and Date
      2015-11-07
    • Related Report
      2015 Annual Research Report
  • [Presentation] Coupled Analysis of High-Density Hydrogen Safety Management2015

    • Author(s)
      Jun Ishimoto and Alain Combescure
    • Organizer
      12th International Conference on Flow Dynamics (ICFD2015)
    • Place of Presentation
      Sendai International Center, Sendai, Japan
    • Year and Date
      2015-10-27
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Innovative glass freezing technologies of biological cell using cryogenic solid particulate spray2015

    • Author(s)
      Jun Ishimoto
    • Organizer
      CRYO2015 - the 52nd Annual Meeting of the Society for Cryobiology
    • Place of Presentation
      Clarion Congress Hotel Ostrava, Ostrava-Zabreh, Czech Republic
    • Year and Date
      2015-07-26
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Development of environmental harmony resist removal system using cryogenic particulate spray2015

    • Author(s)
      Jun Ishimoto
    • Organizer
      The 32nd International Conference of Photopolymer Science and Technology, Materials & Processes for Advanced Microlithography, Nanotechnology and Phototechnology (ICPST-32)
    • Place of Presentation
      Makuhari Messe, Chiba, Japan
    • Year and Date
      2015-06-26
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Cryogenic solid nitrogen particle production through Laval nozzle and its impingement behavior with phase change2015

    • Author(s)
      Jun Ishimoto
    • Organizer
      EMN Meeting on Droplets 2015
    • Place of Presentation
      Holiday Inn Resort Phuket, Phuket, Thailand
    • Year and Date
      2015-05-08
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Patent(Industrial Property Rights)] 凍結装置、凍結方法2016

    • Inventor(s)
      石本淳
    • Industrial Property Rights Holder
      石本淳
    • Industrial Property Rights Type
      特許
    • Patent Publication Number
      2016-182103
    • Filing Date
      2016
    • Related Report
      2016 Annual Research Report

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Published: 2015-04-16   Modified: 2019-03-29  

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