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Ferroelectric domain dynamics studied via atomic-resolution in-situ electrical biasing TEM

Research Project

Project/Area Number 15H05545
Research Category

Grant-in-Aid for Young Scientists (A)

Allocation TypeSingle-year Grants
Research Field Inorganic materials/Physical properties
Research InstitutionKyushu University

Principal Investigator

Sato Yukio  九州大学, 工学研究院, 准教授 (80581991)

Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥24,180,000 (Direct Cost: ¥18,600,000、Indirect Cost: ¥5,580,000)
Fiscal Year 2017: ¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2016: ¥7,280,000 (Direct Cost: ¥5,600,000、Indirect Cost: ¥1,680,000)
Fiscal Year 2015: ¥13,130,000 (Direct Cost: ¥10,100,000、Indirect Cost: ¥3,030,000)
Keywords誘電体 / 圧電体 / 強誘電体 / 電子顕微鏡 / 電子セラミックス / その場観察 / ドメイン / 電圧印加 / イオン分極 / ナノドメイン / 透過型電子顕微鏡
Outline of Final Research Achievements

In this project, we have developed atomic resolution electrical biasing in-situ electron microscopy, which allows us to observe atomistic structure of material under external electric field and determine the atomic position precisely. Also, we have applied this method to characterize ferroelectric materials. We have demonstrated that in a prototypical dielectric crystal, strontium titanate, precision below 10 pm in the atomic position determination can be achieved. (Sato et al., Appl. Phys. Lett., 2017.) We are characterizing other ferroelectric materials using this method and we will publish the results in near future.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Annual Research Report
  • 2015 Annual Research Report
  • Research Products

    (49 results)

All 2018 2017 2016 2015 Other

All Int'l Joint Research (1 results) Journal Article (11 results) (of which Peer Reviewed: 11 results,  Acknowledgement Compliant: 3 results) Presentation (32 results) (of which Int'l Joint Research: 14 results,  Invited: 11 results) Remarks (5 results)

  • [Int'l Joint Research] Indian Institute of Science, Bangalore(India)

    • Related Report
      2017 Annual Research Report
  • [Journal Article] Measurement of Barium Ion Displacement Near Surface in a Barium Titanate Nanoparticle by Scanning Transmission Electron Microscopy2018

    • Author(s)
      Mai Aoki, Yukio Sato, Ryo Teranishi, Kenji Kaneko
    • Journal Title

      Applied Microscopy

      Volume: 48 Issue: 1 Pages: 27-32

    • DOI

      10.9729/am.2018.48.1.27

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Electron microscopy with high accuracy and precision at atomic resolution: In-situ observation of a dielectric crystal under electric field2017

    • Author(s)
      Yukio Sato, Takashi Gondo, Hiroya Miyazaki, Ryo Teranishi, and Kenji Kaneko
    • Journal Title

      Applied Physics Letters

      Volume: 111 Issue: 6 Pages: 062904-062904

    • DOI

      10.1063/1.4986361

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of heat treatments on the microstructure and formability of Al-Mg-Mn-Sc-Zr alloy2017

    • Author(s)
      Yudai Miyake, Yukio Sato, Ryo Teranishi, Kenji Kaneko
    • Journal Title

      Micron

      Volume: 101 Pages: 151-155

    • DOI

      10.1016/j.micron.2017.07.003

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Phase Transformation and Interface Segregation Behavior in Si3N4 Ceramics Sintered with La2O3-Lu2O3 Mixed Additive2017

    • Author(s)
      R. Urakami, Y. Sato, M. Ogushi, T. Nishiyama, A. Goto, K. Yamada, R. Teranishi, K. Kaneko, and M. Kitayama
    • Journal Title

      Journal of the American Ceramic Society

      Volume: 100 Issue: 3 Pages: 1231-1240

    • DOI

      10.1111/jace.14663

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Electron microscopic analysis of surface damaged layer in Pb(Mg1/3Nb2/3)O3-PbTiO3 single crystal2017

    • Author(s)
      Y. Kasuya, Y. Sato, R. Urakami, K. Yamada, R. Teranishi, and K. Kaneko
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 56 Issue: 1 Pages: 010312-010312

    • DOI

      10.7567/jjap.56.010312

    • NAID

      210000147324

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Nanostructural characterization of artificial pinning centers in PLD-processed REBa2Cu3O7-d films2017

    • Author(s)
      T. Maeda, K. Kaneko, K. Yamada, A. Roy, Y. Sato, R. Teranishi, T. Kato, T. Izumi, and Y. Shiohara
    • Journal Title

      Ultramicroscopy

      Volume: 176 Pages: 151-160

    • DOI

      10.1016/j.ultramic.2016.11.015

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Three-dimensional studies of intergranular carbides in austenitic stainless steel2017

    • Author(s)
      M. Ochi, R. Kawano, T. Maeda, Y. Sato, R. Teranishi, T. Hara, M. Kikuchi, and K. Kaneko
    • Journal Title

      Microscopy

      Volume: 66 Pages: 89-94

    • DOI

      10.1093/jmicro/dfw103

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Miniaturization of BaHfO3 Nanoparticles in YBa2Cu3Oy Coated Conductors by Two-step Heating Process in TFA-MOD Method2017

    • Author(s)
      H. Horita, R. Teranishi, K. Yamada, K. Kaneko, Y. Sato, K. Otaguro, T. Nishiyama, S. Awaji, and T. Izumi
    • Journal Title

      Superconductor Science and Technology

      Volume: 30 Issue: 2 Pages: 025022-025022

    • DOI

      10.1088/1361-6668/30/2/025022

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Joint of REBa2Cu3O7-d Coated Conductors using Metal Organic Deposition2016

    • Author(s)
      K. Hiramatsu, R. Teranishi, K. Yamada, Y. Sato, and K. Kaneko
    • Journal Title

      Physics Rrocedia

      Volume: 81 Pages: 109-112

    • DOI

      10.1016/j.phpro.2016.04.003

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Orientation control of LiCoO2 epitaxial thin films on metal substrates2016

    • Author(s)
      Susumu Shiraki, Yoshitaka Takagi, Ryota Shimizu, Tohru Suzuki, Masakazu Haruta, Yukio Sato, Yuichi Ikuhara and Taro Hitosugi
    • Journal Title

      Thin Solid Films

      Volume: 600 Pages: 175-178

    • DOI

      10.1016/j.tsf.2016.01.032

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] 負の熱膨張材料ZrW2O8の微構造解析2015

    • Author(s)
      佐藤幸生,山村泰久,幾原雄一
    • Journal Title

      顕微鏡

      Volume: 50 Pages: 197-200

    • NAID

      130007701847

    • Related Report
      2015 Annual Research Report
    • Peer Reviewed
  • [Presentation] 電圧印加STEM法による誘電体結晶の高分解能観察2018

    • Author(s)
      佐藤 幸生,權堂 貴志,宮崎 裕也,寺西 亮,金子 賢治
    • Organizer
      強的秩序とその操作に関わる研究グループ 第6回 研究会
    • Related Report
      2017 Annual Research Report
  • [Presentation] An In-situ Electrical Biasing Electron Microscopic Study of Dielectric Crystal at Nano and Atomic Scale2018

    • Author(s)
      Yukio Sato, Takashi Gondo, Hiroya Miyazaki, Ryo Teranishi, and Kenji Kaneko
    • Organizer
      Fundamental Physics of Ferroelectrics and Related Materials 2018
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 電圧印加その場電子顕微鏡法による誘電体研究2018

    • Author(s)
      佐藤幸生
    • Organizer
      WFF & WFSM 2018
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] 電圧印加その場電子顕微鏡法によるPMN-0.3PT単結晶の高分解能観察2018

    • Author(s)
      佐藤幸生,青木舞,寺西亮,金子賢治
    • Organizer
      日本物理学会2018年春季大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Atomic scale and in-situ electron microscopic analysis of ferroelectrics2017

    • Author(s)
      Yukio Sato
    • Organizer
      12th Pacific Rim Conference on Ceramic and Glass Technology (PACRIM 12)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 電圧印加その場走査透過型電子顕微鏡法の高分解能化および誘電体研究への適用の試み2017

    • Author(s)
      佐藤幸生,東山幸平,權堂貴志,宮崎裕也,寺西 亮,金子賢治
    • Organizer
      第34回強誘電体応用会議
    • Related Report
      2017 Annual Research Report
  • [Presentation] チタン酸バリウムナノ粒子の表面近傍における原子スケール構造解析2017

    • Author(s)
      青木舞、佐藤幸生、寺西亮、金子賢治
    • Organizer
      日本セラミックス協会第30回秋季シンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] 電圧印加その場電子顕微鏡法による原子位置の解析2017

    • Author(s)
      佐藤幸生,權堂貴志,宮崎裕也,Ahin Roy,寺西亮,金子賢治
    • Organizer
      日本セラミックス協会第30回秋季シンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] 高分解能電圧印加その場電子顕微鏡法による原子位置解析2017

    • Author(s)
      佐藤幸生,權堂貴志,宮崎裕也,Ahin Roy,寺西亮,金子賢治
    • Organizer
      日本物理学会2017年秋季大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Nano- and atomic-scale characterization of electroceramics2017

    • Author(s)
      Yukio Sato,Ryo Teranishi,and Kenji Kaneko
    • Organizer
      International Symposium on Microscopy and Microanalysis of Materials 2017
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 電圧印加その場走査透過型電子顕微鏡観察における原子位置精度の評価2017

    • Author(s)
      佐藤 幸生,權堂 貴志,宮崎 裕也,寺西 亮,金子 賢治
    • Organizer
      日本顕微鏡学会 第60回記念シンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] Electron microscopic analysis of piezoelectric material for medical imaging device2017

    • Author(s)
      Yukio Sato
    • Organizer
      BIT’s 3rd Annual World Congress of Smart Materials - 2017
    • Place of Presentation
      Bangkok, Thailand
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 高分解能およびその場電子顕微鏡法による強誘電体の研究2017

    • Author(s)
      佐藤幸生
    • Organizer
      第4回強的秩序に関する研究会
    • Place of Presentation
      東京大学、東京
    • Related Report
      2016 Annual Research Report
    • Invited
  • [Presentation] Nanoscopic study on domain structure in morphotropic phase boundary Pb(Mg1/3Nb2/3)O3-PbTiO32016

    • Author(s)
      Yukio Sato
    • Organizer
      International Conference on Technologically Advanced Materials & Asian Meeting of Ferroelectricity (ICTAM-AMF10)
    • Place of Presentation
      Dehli, India
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Atomic Scale Characterization of Grain Boundary in Zinc Oxide Ceramics Using Electron Microscopy and First-Principles Calculation2016

    • Author(s)
      Yukio Sato
    • Organizer
      International Symposium on Microscopy and Microanalysis of Materials 2016 (ISMMM 2016)
    • Place of Presentation
      Nanjing, China
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Nanostrain Observation of BaHfO3 introduced GdBa2Cu3O7-y Superconductive Film by Geometric Phase Analysis2016

    • Author(s)
      T. Maeda, K. Kaneko, R. Teranishi, Y. Sato, K. Yamada, T. Kato, A. Ibi, T. Izumi, Y. Shiohara
    • Organizer
      The 5th International Symposium on Advanced Microscopy and Theoretical Calculations
    • Place of Presentation
      ウインク愛知、愛知
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Transimission Electron Microscopy Observation of Mechanically Processed Pb(Mg1/3Nb2/3)O3-PbTiO3 Single Crystal2016

    • Author(s)
      Y. Kasuya, Y. Sato, R. Urakami, K. Yamada, R. Teranishi, K. Kaneko
    • Organizer
      International Symposium in Korean Microscopy Society Meeting 2016
    • Place of Presentation
      Nanjing, China
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] チタン酸バリウム粒子の表面近傍における高分解能構造解析2016

    • Author(s)
      佐藤幸生,稲田幹,Ahin Roy,青木舞,林克郎,金子賢治
    • Organizer
      日本セラミックス協会第29回秋季シンポジウム
    • Place of Presentation
      広島大学、広島
    • Related Report
      2016 Annual Research Report
  • [Presentation] BaTiO3粒子の表面およびその近傍における構造解析2016

    • Author(s)
      佐藤幸生,稲田幹,Ahin Roy,青木舞,林克郎,金子賢治
    • Organizer
      日本物理学会2016年秋季大会
    • Place of Presentation
      金沢大学、石川
    • Related Report
      2016 Annual Research Report
  • [Presentation] Nb-doped TiO2 polymorphs for Transparent Conducting Oxide: An insight from first-principles calculation2016

    • Author(s)
      S. Yoshida, R. Nakashima, Y. Kasuya, R. Urakami, Y. Sato
    • Organizer
      9th Pacific Rim International Conference on Advanced Materials and Processing
    • Place of Presentation
      京都国際会議場、京都
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Sb添加アナターゼ型SnO2の理論計算2016

    • Author(s)
      佐藤幸生,牝小路諒, 浦上亮介, 金子賢治
    • Organizer
      金属学会・鉄鋼協会・軽金属学会九州支部 平成28年度合同学術講演会
    • Place of Presentation
      九州大学、福岡
    • Related Report
      2016 Annual Research Report
  • [Presentation] First-principles study of antimony-doped anatase tin dioxide2016

    • Author(s)
      A. Roy, R. Hinkoji, K. Kaneko, and Y. Sato
    • Organizer
      第36回エレクトロセラミックス研究討論会
    • Place of Presentation
      ユニオンビル,東京
    • Related Report
      2016 Annual Research Report
  • [Presentation] Phosphorus Doping Induced Enhancement in Electrical Conductivity in Graphitic Carbon Nitride: Insights from ab initio Simulations2016

    • Author(s)
      A. Roy, K. Kaneko, Y. Sato
    • Organizer
      International Conference on Technologically Advanced Materials & Asian Meeting of Ferroelectricity (ICTAM-AMF10)
    • Place of Presentation
      Dehli, India
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Electron microscopic study on dynamics of nanoscale ferroelectric domains in Pb(Mg1/3Nb2/3)O3 – PbTiO32015

    • Author(s)
      Yukio Sato
    • Organizer
      The International Chemical Congress of Pacific Basin Societies (Pacifichem) 2015,
    • Place of Presentation
      Honolulu, Hawaii, USA
    • Year and Date
      2015-12-20
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Transmission electron microscopic study on functional ceramics2015

    • Author(s)
      Yukio Sato
    • Organizer
      International Symposium in Korean Microscopy Society Meeting
    • Place of Presentation
      Changwon, Korea
    • Year and Date
      2015-11-12
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] LaおよびLu共添加Si3N4セラミックスにおける結晶粒‐粒界相界面の走査透過型電子顕微鏡観察2015

    • Author(s)
      浦上亮介, 佐藤幸生, 大串将巧, 西山武志,山田和広, 寺西亮, 金子賢治, 北山幹人
    • Organizer
      腐食防食学会2015年度秋期講演大会 第62回材料と環境討論会
    • Place of Presentation
      福岡工業大学、福岡
    • Year and Date
      2015-11-04
    • Related Report
      2015 Annual Research Report
  • [Presentation] Nano-scale and atomic-scale characterization of electroceramics2015

    • Author(s)
      Yukio Sato
    • Organizer
      IUMRS-ICAM (International Union of Materials Research Societies, International Conference of Advanced Materials) 2015
    • Place of Presentation
      Jeju, Korea
    • Year and Date
      2015-10-28
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Pb(Mg1/3Nb2/3)O3-PbTiO3単結晶の加工表面近傍における微細組織の解析2015

    • Author(s)
      糟谷祐輔, 佐藤幸生, 浦上亮介, 山田和広, 寺西亮, 金子賢治
    • Organizer
      第35回エレクトロセラミックス研究討論会
    • Place of Presentation
      東京工業大学、東京
    • Year and Date
      2015-10-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] LaおよびLu共添加Si3N4セラミックスにおける結晶粒界のSTEM観察2015

    • Author(s)
      浦上亮介,佐藤幸生,大串将巧,西山武志,山田和広,寺西亮,北山幹人,金子賢治
    • Organizer
      第35回エレクトロセラミックス研究討論会
    • Place of Presentation
      東京工業大学、東京
    • Year and Date
      2015-10-23
    • Related Report
      2015 Annual Research Report
  • [Presentation] La, Lu共添加Si3N4の焼結時における成長様式の解明2015

    • Author(s)
      浦上亮介,佐藤幸生,大串将巧,西山武志,山田和広,寺西亮,北山幹人,金子賢治
    • Organizer
      日本金属学会2015年秋期(第157回)講演大会
    • Place of Presentation
      九州大学、福岡
    • Year and Date
      2015-09-14
    • Related Report
      2015 Annual Research Report
  • [Presentation] Electron microscopic study on origin of function in electroceramics2015

    • Author(s)
      Yukio Sato
    • Organizer
      International Conference on Electron Microscopy and XXXVI Annual Meeting of the Electron Microscope Society of India (EMSI)
    • Place of Presentation
      Mumbai, India
    • Year and Date
      2015-07-10
    • Related Report
      2015 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 研磨加工を施したPb(Mg1/3Nb2/3)O3 – PbTiO3単結晶の表面近傍における微細組織の観察2015

    • Author(s)
      糟谷祐輔,佐藤幸生,浦上亮介,山田和広,金子賢治
    • Organizer
      金属学会・鉄鋼協会・軽金属学会九州支部 平成27年度合同学術講演会
    • Place of Presentation
      北九州国際会議場、福岡
    • Year and Date
      2015-06-06
    • Related Report
      2015 Annual Research Report
  • [Remarks] ナノ材料組織解析学・金子研究室 佐藤幸生准教授

    • URL

      http://zaiko13.zaiko.kyushu-u.ac.jp/sato.html

    • Related Report
      2017 Annual Research Report
  • [Remarks] academist Journal

    • URL

      https://academist-cf.com/journal/?p=5947

    • Related Report
      2017 Annual Research Report
  • [Remarks] 九州大学大学院工学研究院材料工学部門ホームページ

    • URL

      https://www.zaiko.kyushu-u.ac.jp/news489.html

    • Related Report
      2017 Annual Research Report
  • [Remarks] 九州大学 プレスリリース

    • URL

      https://www.kyushu-u.ac.jp/f/31256/17_08_09.pdf

    • Related Report
      2017 Annual Research Report
  • [Remarks] 九州大学大学院工学研究院 材料工学部門 ナノ材料組織解析学・金子研究室

    • URL

      http://zaiko13.zaiko.kyushu-u.ac.jp/

    • Related Report
      2015 Annual Research Report

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Published: 2015-04-16   Modified: 2019-03-29  

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