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Development of a rapid and simple measurement system for oxygen-containing components in fuel oil using a compact atomic emission detection device

Research Project

Project/Area Number 15K00587
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Environmental engineering and reduction of environmental burden
Research InstitutionNihon University

Principal Investigator

NAKAGAMA Tatsuro  日本大学, 生産工学部, 教授 (50244421)

Co-Investigator(Renkei-kenkyūsha) SAITOH Kazunori  日本大学, 生産工学部, 准教授 (90409087)
Project Period (FY) 2015-10-21 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2017: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2016: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2015: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Keywords原子発光検出 / 迅速簡易測定 / ガスクロマトグラフィー / マイクロリアクター / プラズマ / 含酸素化合物 / 燃料油 / 簡易測定 / 熱分解
Outline of Final Research Achievements

A gas chromatographic (GC) system equipped with a compact atomic emission detection (AED) device was developed for the elemental-selective, rapid and simple measurement of oxygen-containing compounds in fuel oil. Prototype online microreactors for thermal or plasma degradations were developed for improving the compound-dependent sensitivity for oxygen using the AED device alone. In this study, the former reactor was relatively effective for resolving the sensitivity. The similar AED sensitivity for oxygen was performed using the GC-AED system connected with the thermal-degradation device when methanol, methyl tert- butyl ester (MTBE) and ethyl tert- butyl ester (ETBE) containing in fuel oil were used as the test samples.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (4 results)

All 2018 2017

All Presentation (4 results)

  • [Presentation] マイクロプラズマを利用したガスクロマトグラフ内蔵型原子発光検出デバイスの試作2018

    • Author(s)
      髙野真佐志,齊藤和憲,中釜達朗
    • Organizer
      日本海水学会第9回学生研究発表会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 原子発光検出における含酸素化合物の 分子構造依存性改善のための ガスクロマトグラフィー用小型加熱分解デバイスの試作と評価2017

    • Author(s)
      )佐藤達哉,齊藤和憲,中釜達朗
    • Organizer
      分離技術会年会2017
    • Place of Presentation
      明治大学生田キャンパス
    • Year and Date
      2017-05-26
    • Related Report
      2016 Research-status Report
  • [Presentation] 原子発光検出における含酸素化合物の分子構造依存性改善のためのガスクロマトグラフィー用小型加熱分解デバイスの試作と評価2017

    • Author(s)
      佐藤達哉,齊藤和憲,中釜達朗
    • Organizer
      分離技術会2017
    • Related Report
      2017 Annual Research Report
  • [Presentation] 含酸素有機化合物の原子発光検出における分子構造依存性改善のためのキャピラリーGC用オンライン小型予備分解デバイスの試作2017

    • Author(s)
      佐藤達哉,齊藤和憲,中釜達朗
    • Organizer
      日本分析化学会第66年会
    • Related Report
      2017 Annual Research Report

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Published: 2015-10-21   Modified: 2019-03-29  

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