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Development of the rapid measurement technology of the trans-fatty acid in frying oils using near infrared spectroscopy

Research Project

Project/Area Number 15K00789
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Eating habits
Research InstitutionAkita Prefectural University

Principal Investigator

Chen Jie Yu  秋田県立大学, 生物資源科学部, 教授 (20315584)

Co-Investigator(Kenkyū-buntansha) 張 函  秋田県立大学, 生物資源科学部, 准教授 (10315608)
Project Period (FY) 2015-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2017: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2016: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2015: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywordsフライ油 / トランス脂肪酸 / 劣化 / 酸化 / 迅速測定 / 近赤外 / 酸価 / カルボニル価 / 総極性化合物量 / 極性化合物 / 総極性化合物
Outline of Final Research Achievements

This study examined the relation between trans fatty acid of frying oil and the near infrared spectra to try the development of a simple and rapid measurement technology of the trans fatty acid of frying oil using near infrared spectroscopy. As the results, the close relation was confirmed between near infrared spectrum and trans fatty acid of the frying oil, and it was possible to use in the measurement of trans fatty acid of frying oil by near infrared spectroscopy. Although the temperature of frying oil affected the measurement accuracy of trans fatty acid, the prediction accuracy was the highest at around 40 degrees Celsius. Furthermore, it was possible to construct the prediction model of trans fatty acid which can correspond for various edible frying oil.

Academic Significance and Societal Importance of the Research Achievements

近赤外スペクトルによるフライ油のトランス脂肪酸の簡便かつ迅速的な分析技術を開発することにより、従来のGC法における煩雑な前処理や手間などの長時間操作から解放されると同時に環境にも優しい。またこれらの研究成果をベースにするハンディータイプの計測機器を開発すれば現場での利用も可能であり、食品の製造プロセスにおけるフライ油の有害なトランス脂肪酸の有効管理にも役に立つ。さらに将来フライ食品をはじめ、一般の食品への応用も見据え、その開発の基礎を提供し、食品の安全・安心への貢献が期待される。

Report

(5 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Research-status Report
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (29 results)

All 2018 2017 2016 2015

All Journal Article (7 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 5 results) Presentation (22 results) (of which Int'l Joint Research: 14 results)

  • [Journal Article] A Novel Evaluation Index for Predicting the Degradation Rate of Frying Oils Based on Their Fatty Acid Composition2018

    • Author(s)
      Liu Xiaofang、Hoshino Nozomi、Wang Shuo、Masui Eitaro、Chen Jieyu、Zhang Han
    • Journal Title

      European Journal of Lipid Science and Technology

      Volume: 120 Issue: 7 Pages: 1700528-1700528

    • DOI

      10.1002/ejlt.201700528

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] 味噌の品質評価への可視・近赤外スペクトルの利用2018

    • Author(s)
      陳 介余、張 函、田村岳大、京野信行
    • Journal Title

      美味技術学会誌

      Volume: 16(2) Pages: 23-29

    • NAID

      130007484443

    • Related Report
      2017 Research-status Report
    • Peer Reviewed
  • [Journal Article] 近赤外分光法による乾麺の水分測定に関する基礎研究2017

    • Author(s)
      陳 介余、張 函
    • Journal Title

      秋田県立大学ウエブジャーナルB(研究成果部門)

      Volume: 4 Pages: 131-135

    • NAID

      120006354893

    • Related Report
      2017 Research-status Report
  • [Journal Article] 近赤外分光スペクトルを用いた乾麺の簡易水分測定システムの構築2017

    • Author(s)
      陳 介余、張 函
    • Journal Title

      秋田県立大学ウエブジャーナルB(研究成果部門)

      Volume: 4 Pages: 136-140

    • NAID

      120006354894

    • Related Report
      2017 Research-status Report
  • [Journal Article] Determination of the Carbonyl Values for Frying Rapeseed Oil Using Near-Infrared Spectroscopy2015

    • Author(s)
      1)Jie Yu Chen, Han Zhang, Jinkui MA, Tomohiro Tuchiya, Yelian Miao
    • Journal Title

      Food Anal. Methods

      Volume: 8 Pages: 1508-1514

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] Determination of The Degree of Degradation of Frying Rapeseed Oil Using Fourier-Transform Infrared Spectroscopy Combined with Partial Least-squares Regression2015

    • Author(s)
      2)Jie Yu Chen, Han Zhang, Jinkui Ma, Tomohiro Tuchiya, and Yelian Miao
    • Journal Title

      International Journal of Analytical Chemistry

      Volume: 2015 ID:185367 Pages: 1-6

    • DOI

      10.1155/2015/185367

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] Analysis of carbonyl value of frying oil by Fourier transform infrared spectroscopy2015

    • Author(s)
      3)Han Zhang, Jinkui Ma, Yelian Miao, Tomohiro Tuchiya, Jie Yu Chen
    • Journal Title

      Journal of Oleo Science

      Volume: 64 Pages: 375-380

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Presentation] Near infrared spectroscopic determination of acid value in vegetable frying oil2018

    • Author(s)
      Jie Yu Chen, Xiaofang Liu, Shuo Wang, Jinkui Ma and Han Zhang
    • Organizer
      The Sixth Asian NIR Symposium
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] NIR determination of trans-fatty acid content in frying oils2018

    • Author(s)
      Han Zhang and Jie Yu Chen
    • Organizer
      The Sixth Asian NIR Symposium
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Application of electronic nose for quality evaluation of the miso paste2018

    • Author(s)
      Jie Yu Chen and Han Zhang
    • Organizer
      The 2nd International Flavor and Fragrance Conference
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Changes of Oxidation Volatile Compounds in Brown Rice during Storage Period2018

    • Author(s)
      Han Zhang and Jie Yu Chen
    • Organizer
      The 2nd International Flavor and Fragrance Conference
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Deterioration of fatty acid and reduction of tocopherol content in commercial oils during deep-frying2018

    • Author(s)
      Xiaofang Liu,Eitaro Masui,Shuo Wang,Shigeru Tamogami,JieYu Chen,Han Zhang
    • Organizer
      日本食品科学工学会第65 回大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 混合脂肪酸の自動酸化における粉末緑茶添加の影響2018

    • Author(s)
      増井栄太郎, 劉暁芳,陳 介余,秋山美展,張 函
    • Organizer
      日本食品科学工学会第65 回大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Examination of the possibility of analysis of trans-fatty acid content in frying oil by measuring the fried potatoes with near infrared spectroscopy2017

    • Author(s)
      Jie Yu Chen, Shuo Wang, Xiaofang Liu, Eitaro Masui, Yelian Miao and Han Zhang
    • Organizer
      2nd Innovations in Food Packaging, Shelf Life and Food Safety Conference
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research
  • [Presentation] Analysis of degradation degree of the frying edible oil by measuring a frying potato with near infrared spectroscopy2017

    • Author(s)
      Han Zhang, Xiaofang Liu, Shuo Wang, Eitaro Masui, Yelian Miao and Jie Yu Chen
    • Organizer
      2nd Innovations in Food Packaging, Shelf Life and Food Safety Conference
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research
  • [Presentation] 味噌の品質評価への近赤外分光法の利用可能性の探索2017

    • Author(s)
      陳 介余、張 函
    • Organizer
      第17回日本美味技術学会年次大会
    • Related Report
      2017 Research-status Report
  • [Presentation] 食用油に含まれる不飽和脂肪酸のにおい生成とその制御について2017

    • Author(s)
      増井 栄太郎、劉暁芳、陳 介余、張 函
    • Organizer
      第17回日本美味技術学会年次大会
    • Related Report
      2017 Research-status Report
  • [Presentation] 近赤外分光法による醤油のアミノ酸組成の迅速測定2017

    • Author(s)
      王 碩、劉 暁芳、張 函、秋山 美展、陳 介余
    • Organizer
      第33回近赤外フォーラム
    • Related Report
      2017 Research-status Report
  • [Presentation] 抗酸化性食素材の添加によるオレイン酸の酸化抑制効果について2017

    • Author(s)
      増井 栄太郎、劉 暁芳、星野 望、陳 介余、張 函
    • Organizer
      日本食品科学工学会第64回大会
    • Related Report
      2017 Research-status Report
  • [Presentation] Correlating Visible/Near Infrared Spectra with Sensory Evaluation Values of Miso Paste2016

    • Author(s)
      Jie Yu Chen, Yuya Waizumi, Shuo Wang, Xiao-fang Liu, Han Zhang, Takayuki Watanabe, Takehiro Tamura, Nobuyuki Kyouno, and Yelian Miao
    • Organizer
      The 5th Asian NIR Symposium (ANS2016)
    • Place of Presentation
      Kagoshima, Japan
    • Year and Date
      2016-12-01
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Relationships between Visible/Near Infrared Spectra and Sensory Evaluations of Soy Sauce2016

    • Author(s)
      Han Zhang, Yuya Waizumi, Shuo Wang, Xiao-fang Liu, Takayuki Watanabe, Takehiro Tamura, Nobuyuki Kyouno, Yelian Miao, and Jie Yu Chen
    • Organizer
      The 5th Asian NIR Symposium (ANS2016)
    • Place of Presentation
      Kagoshima, Japan
    • Year and Date
      2016-12-01
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Near infrared spectroscopy technology for determination of tocopherols in frying oils2016

    • Author(s)
      Jie Yu Chen, Jinkui Ma, Han Zhang
    • Organizer
      The Food Factor I Barcelona Conference
    • Place of Presentation
      Barcelona, Spain
    • Year and Date
      2016-11-02
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Determination of frying oil deterioration by the HERACLES electronic nose and multivariate regression analysis2016

    • Author(s)
      Han Zhang, Jinkui Ma, Tomomi Konno, Jie Yu Chen
    • Organizer
      The Food Factor I Barcelona Conference
    • Place of Presentation
      Barcelona, Spain
    • Year and Date
      2016-11-02
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Effect of heating time on the volatile components from frying oil2016

    • Author(s)
      Han Zhang, Jin-Kui Ma, Tomoni, Konno, Jie Yu Chen
    • Organizer
      The Food Factor I Barcelona Conference
    • Place of Presentation
      Barcelona, Spain
    • Year and Date
      2016-11-02
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Analysis of trans-fatty acid content in frying oils using near-infrared spectroscopy2016

    • Author(s)
      Jie Yu Chen, Shin Suzuki, Yutaka Hiruma, Han Zhang, Jinkui Ma, Tomohiro Tuchiya, Yelian Miao
    • Organizer
      First Food Chemistry Conference - Shaping the Future of Food Quality, Health and Safety
    • Place of Presentation
      Amsterdam, Netherlands
    • Year and Date
      2016-10-30
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] フライ温度による菜種油の揮発成分変動の解析2016

    • Author(s)
      張 函、今野智美、星野 望、馬 金魁、陳 介余
    • Organizer
      日本食品工学会第17 回(2016 年度)年次大会
    • Place of Presentation
      東京海洋大学、日本
    • Year and Date
      2016-08-04
    • Related Report
      2016 Research-status Report
  • [Presentation] Rapid quality analysis of various kinds of frying oils by near infrared spectroscopy2016

    • Author(s)
      Jie Yu Chen, Shin Suzuki, Yutaka Hiruma and Han Zhang
    • Organizer
      The 2016 International Conference on Food Properties (ICFP2016)
    • Place of Presentation
      Bangkok, Thailand
    • Year and Date
      2016-05-31
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Comparison of frying stability of two types of sesame oils refined by the roasting method and the cold compression method2016

    • Author(s)
      Han Zhang, Shin Suzuki, Yutaka Hiruma and Jie Yu Chen
    • Organizer
      The 2016 International Conference on Food Properties (ICFP2016)
    • Place of Presentation
      Bangkok, Thailand
    • Year and Date
      2016-05-31
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] 近赤外分光法によるフライ油の劣化度分析2016

    • Author(s)
      真坂千尋、張 函、陳 介余
    • Organizer
      日本食品分析学会
    • Place of Presentation
      東洋大学白山キャンパス 日本
    • Related Report
      2016 Research-status Report

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Published: 2015-04-16   Modified: 2020-03-30  

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