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Crystal growth mechanisms of mixed oxide nanoparticles

Research Project

Project/Area Number 15K04608
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Nanomaterials chemistry
Research InstitutionNara Women's University

Principal Investigator

HARADA MASAFUMI  奈良女子大学, 生活環境科学系, 准教授 (90314525)

Project Period (FY) 2015-10-21 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2017: ¥390,000 (Direct Cost: ¥300,000、Indirect Cost: ¥90,000)
Fiscal Year 2016: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2015: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywordsナノ粒子 / マイクロ波合成 / 複合酸化物ナノ粒子 / 混合フェライト / 磁化曲線 / 結晶成長 / X線吸収微細構造 / 構造解析 / X線吸収微細構造 / マイクロリアクター / 酸化物ナノ粒子 / フェライト
Outline of Final Research Achievements

Spinel ferrites are a class of compounds of general formula MFe2O4 (M = Mn, Co, Ni, Cu, Zn), which are of great interest for their remarkable magnetic properties. Spinel ferrite nanoparticles have been synthesized by microwave irradiation, and their structural and magnetic properties have been investigated by using XRD, XPS, HRTEM, EELS, EXAFS, and SQUID measurements. Furthermore, since the particular properties of ferrite nanoparticles are strictly related to the distribution of cations between octahedral and tetrahedral sites in the spinel structure, EXAFS measurements have been used to determine quantitatively the distribution of cations in the nanoparticle.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (11 results)

All 2017 2016 Other

All Journal Article (3 results) (of which Peer Reviewed: 3 results) Presentation (7 results) Remarks (1 results)

  • [Journal Article] Microwave-Assisted Polyol Synthesis of Pt/Pd and Pt/Rh Bimetallic Nanoparticles in Polymer Solutions Prepared by Batch and Continuous-Flow Processing2017

    • Author(s)
      Cong Cong、Nakayama Sayaka、Maenosono Shinya、Harada Masafumi
    • Journal Title

      Ind. Eng. Chem. Res.

      Volume: 57 Issue: 1 Pages: 179-190

    • DOI

      10.1021/acs.iecr.7b03154

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Properties of Protic Ionic Liquids Comprised of N-Alkyldiethylenetriamine and Their Complexation of Copper(II) Ions2017

    • Author(s)
      Nakayama Chisayo、Harada Masafumi、Iida Masayasu
    • Journal Title

      Eur. J. Inorg. Chem.

      Volume: 2017 Issue: 31 Pages: 3744-3754

    • DOI

      10.1002/ejic.201700568

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Formation of silver nanoparticles from ionic liquids comprising N -alkylethylenediamine: Effects of dissolution modes of the silver(I) ions in the ionic liquids2017

    • Author(s)
      Er Hua、Yasuda Haruka、Harada Masafumi、Taguchi Eiji、Iida Masayasu
    • Journal Title

      Colloids and Surfaces A: Physicochemical and Engineering Aspects

      Volume: 522 Pages: 503-513

    • DOI

      10.1016/j.colsurfa.2017.03.046

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Presentation] 複合酸化物ナノ粒子の構造と磁気特性2017

    • Author(s)
      原田雅史、桑 雅子、中川あすみ、佐藤良太、寺西利治
    • Organizer
      2016年度量子ビームサイエンスフェスタ
    • Place of Presentation
      つくば国際会議場(エポカルつくば)
    • Year and Date
      2017-03-14
    • Related Report
      2016 Research-status Report
  • [Presentation] 複合フェライトナノ粒子のEXAFS構造解析と磁気特性2017

    • Author(s)
      桑 雅子、原田雅史、佐藤良太、寺西利治
    • Organizer
      第20回XAFS討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 高エネルギーX線回折を用いた貴金属ナノ粒子の三次元構造解析2017

    • Author(s)
      原田雅史、池上梨沙、ロシャンタクマーラ、小原真司、坂田修身
    • Organizer
      第68回コロイドおよび界面化学討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] イオン液体中における非イオン性界面活性剤の会合体形成と金属ナノ粒子合成への応用2017

    • Author(s)
      山本実穂、原田雅史
    • Organizer
      第68回コロイドおよび界面化学討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] マイクロ波加熱を用いた酸化物ナノ粒子の迅速合成と構造解析2016

    • Author(s)
      桑 雅子、原田雅史、佐藤良太、寺西利治
    • Organizer
      日本油化学会第55回年会
    • Place of Presentation
      奈良女子大学
    • Year and Date
      2016-09-07
    • Related Report
      2016 Research-status Report
  • [Presentation] Microwave-Assisted Synthesis of Transition-metal Oxide Nanoparticles.2016

    • Author(s)
      M. Kuwa, M. Harada, R. Sato, T. Teranishi
    • Organizer
      2nd Internanional Conference of Polyol Mediated Synthesis (IC-PMS2016)
    • Place of Presentation
      The University of Shiga Prefecture
    • Year and Date
      2016-07-11
    • Related Report
      2016 Research-status Report
  • [Presentation] マイクロ波加熱を用いた酸化物ナノ粒子の迅速合成と構造解析2016

    • Author(s)
      桑 雅子、原田雅史、佐藤良太、寺西利治
    • Organizer
      日本化学会第96春季年会
    • Place of Presentation
      同志社大学京田辺キャンパス(京都府京田辺市)
    • Year and Date
      2016-03-24
    • Related Report
      2015 Research-status Report
  • [Remarks]

    • URL

      http://koto10.nara-wu.ac.jp/Profiles/4/0000380/theses1.html

    • Related Report
      2016 Research-status Report

URL: 

Published: 2015-10-21   Modified: 2019-03-29  

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