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Measurement method for polarity-inverted layered piezoelectric thin films using scanning nonlinear dielectric microscopy

Research Project

Project/Area Number 15K04725
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field General applied physics
Research InstitutionNational Institute of Technology, Kumamoto College

Principal Investigator

ODAGAWA HIROYUKI  熊本高等専門学校, 地域イノベーションセンター(熊本キャンパス), 教授 (00250845)

Co-Investigator(Kenkyū-buntansha) 柳谷 隆彦  早稲田大学, 理工学術院, 准教授 (10450652)
Co-Investigator(Renkei-kenkyūsha) CHO YASUO  東北大学, 電気通信研究所, 教授 (40179966)
Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
Fiscal Year 2017: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2016: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2015: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Keywords分極反転 / 圧電薄膜 / 走査型非線形誘電率顕微法 / 極性反転構造 / 極性反転圧電薄膜 / 層厚測定 / 分極反転層 / AlN圧電薄膜
Outline of Final Research Achievements

Recently, it is reported that the polarity of ZnO and AlN piezoelectric thin film fabricated by radio frequency (RF) magnetron sputtering method can be switched by changing the growth condition, and polarity-inverted structure has been obtained. In this research, we have developed the quantitative measurement method for the thickness of a polarity inverted layer using canning nonlinear dielectric microscopy (SNDM). We derive an equation that represents the relationship between the output signal and the oscillation frequency of the SNDM probe, and developed the measurement procedure that can determine the thickness of polarity-inverted single layer structure. We applied it to two-dimensional distribution measurements of the layer thickness. Moreover, we investigated the measurement for double layered structure. We showed that it is possible to determine the thickness of two layers by controlling depth profile of electric field inside the measurement materials using a soft probe tip.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (8 results)

All 2017 2016 2015

All Journal Article (3 results) (of which Peer Reviewed: 2 results,  Acknowledgement Compliant: 2 results) Presentation (5 results) (of which Int'l Joint Research: 4 results)

  • [Journal Article] Quantitative thickness measurement of polarity-inverted piezoelectric thin-film layer by scanning nonlinear dielectric microscopy2017

    • Author(s)
      Hiroyuki Odagawa, Koshiro Terada, Yohei Tanaka, Hiroaki Nishikawa, Takahiko Yanagitani and Yasuo Cho
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 56 Issue: 10S Pages: 10PF18-10PF18

    • DOI

      10.7567/jjap.56.10pf18

    • NAID

      210000148395

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Method for measuring polarity-inverted layered structure in dielectric thin films using scanning nonlinear dielectric microscopy2016

    • Author(s)
      Hiroyuki Odagawa, Koshiro Terada, Hiroaki Nishikawa, Takahiko Yanagitani, Yasuo Cho
    • Journal Title

      Ferroelectrics

      Volume: 498(1) Issue: 1 Pages: 47-51

    • DOI

      10.1080/00150193.2016.1169493

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] 走査型非線形誘電率顕微法に・E謔驪ノ性反転層状構造圧電薄膜の層厚の定量測定2015

    • Author(s)
      寺田浩士朗, 西川宏明, 田中陽平, 小田川裕之, 柳谷隆彦, 長康雄
    • Journal Title

      電子情報通信学会技術報告

      Volume: US2015-62 Pages: 23-26

    • Related Report
      2015 Research-status Report
    • Acknowledgement Compliant
  • [Presentation] Quantitative thickness measurement in polarity-inverted piezoelectric layered thin film using scanning nonlinear dielectric microscopy2017

    • Author(s)
      H. Odagawa, K. Terada, H. Nishikawa, Y. Tanaka, T. Yanagitani and Y. Cho
    • Organizer
      2017 Joint IEEE ISAF - IWATMD - PFM (26th International Symposium on Applications of Ferroelectrics (ISAF))
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Quantitative thickness measurement in polarityinverted piezoelectric layered thin film using scanning nonlinear dielectric microscopy2016

    • Author(s)
      Hiroyuki Odagawa, Koshiro Terada, Hiroaki Nishikawa, Yohei Tanaka, Takahiko Yanagitani and Yasuo Cho
    • Organizer
      2016 Joint IEEE International Symposium on the Applications of Ferroelectrics, European Conference on Applications of Polar Dielectrics & Workshop on Piezoresponse Force Microscopy (ISAF/ECAPD/PFM)
    • Place of Presentation
      Darmstadt, Germany
    • Year and Date
      2016-08-21
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Quantitative Thickness Measurement in Layered Polarity-Inverted Piezoelectric Thin Films Using Scanning Nonlinear Dielectric Microscopy2016

    • Author(s)
      Koshiro Terada, Hiroaki Nishikawa, Yohei Tanaka1, Hiroyuki Odagawa1, Takahiko Yanagitani, and Yasuo Cho
    • Organizer
      The 3rd International Conference of Global Network for Innovative Technology
    • Place of Presentation
      Penang, Malaysia
    • Year and Date
      2016-01-27
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 走査型非線形誘電率顕微法による層状極性反転圧電膜の層厚の定量測定2015

    • Author(s)
      寺田浩士朗, 西川宏明, 田中陽平, 小田川裕之, 柳谷隆彦, 長康雄
    • Organizer
      超音波エレクトロニクスの基礎と応用に関するシンポジウム(USE2015)
    • Place of Presentation
      つくば
    • Year and Date
      2015-11-05
    • Related Report
      2015 Research-status Report
  • [Presentation] Method for Measuring Polarity-Inverted Layered Structure in Dielectric Thin Films Using Scanning Nonlinear Dielectric Microscocpy2015

    • Author(s)
      Hiroyuki Odagawa, Koshiro Terada, Hiroaki Nishikawa, TakahikoYanagitani abd Yasuo Cho
    • Organizer
      13th European Meeting on Ferroelectricity (EMF2015)
    • Place of Presentation
      Porto, Portugal
    • Year and Date
      2015-06-28
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research

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Published: 2015-04-16   Modified: 2019-03-29  

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