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Development of Novel Porous Polyimide-Coated Separation Media

Research Project

Project/Area Number 15K05537
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Analytical chemistry
Research InstitutionToyohashi University of Technology

Principal Investigator

SAITO Yoshihiro  豊橋技術科学大学, 工学(系)研究科(研究院), 教授 (00303701)

Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2017: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2016: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2015: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Keywordsポリイミド / 表面多孔性粒子 / 抽出媒体 / 試料前処理 / 分離媒体 / クロマトグラフィー / 微量分離分析 / 環境分析
Outline of Final Research Achievements

In this work, novel polyimide-based stationary phases in liquid chromatography and novel sample extraction media in solid-phase extraction have been developed. Coated with cross-linked polyimide materials onto the surface of core particles having uniform particle size, the developed materials showed a retentivity as a stationary phase in liquid chromatography and also showed an extraction capability in solid-phase extraction. A different molecular shape selectivity from conventional stationary phases, such as octadecylsilica, for the retention of a group of aromatic compounds as the sample probe, was obtained in liquid chromatography.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (25 results)

All 2018 2017 2016 2015

All Journal Article (10 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 10 results,  Open Access: 8 results,  Acknowledgement Compliant: 3 results) Presentation (15 results) (of which Int'l Joint Research: 2 results,  Invited: 4 results)

  • [Journal Article] Separation of Triglycerides in Oils and Fats by Comprehensive Two-Dimensional Liquid Chromatography and the Determination of the Fatty Acid Composition in Gas Chromatography2018

    • Author(s)
      T. Sato, Y. Saito, A. Kobayashi, I. Ueta
    • Journal Title

      CHROMATOGRAPHY

      Volume: 39 Issue: 2 Pages: 67-74

    • DOI

      10.15583/jpchrom.2018.004

    • NAID

      130007403280

    • ISSN
      1342-8284, 1348-3315
    • Year and Date
      2018-06-20
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Simultaneous Derivatization and Extraction of Volatile Amines with Fiber-Packed Needle and Subsequent Analysis in Gas Chromatography2018

    • Author(s)
      K. Nakagami, T. Tazawa, O. Sumiya, I. Ueta, Y. Satio
    • Journal Title

      CHROMATOGRAPHY

      Volume: 39 Issue: 2 Pages: 75-81

    • DOI

      10.15583/jpchrom.2018.005

    • NAID

      130007403283

    • ISSN
      1342-8284, 1348-3315
    • Year and Date
      2018-06-20
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Polyimide Filaments as a Novel Stationary Phase in Packed-Capillary Gas Chromatography2018

    • Author(s)
      K. Nakagami, O. Sumiya, T. Tazawa, T. Monobe, M. Watanabe, I. Ueta, Y. Saito
    • Journal Title

      CHROMATOGRAPHY

      Volume: 39 Issue: 2 Pages: 91-96

    • DOI

      10.15583/jpchrom.2018.008

    • NAID

      130007403276

    • ISSN
      1342-8284, 1348-3315
    • Year and Date
      2018-06-20
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Determination of Aqueous Formic and Acetic Acids by Purge-and-Trap Analysis with a Needle-Type Extraction Device and Gas Chromatography Barrier Discharge Ionization Detector2018

    • Author(s)
      I. Ueta, Y. Nakamura, S. Kawakubo, Y. Saito
    • Journal Title

      Analytical Sciences

      Volume: 34 Issue: 2 Pages: 201-205

    • DOI

      10.2116/analsci.34.201

    • NAID

      130006342070

    • ISSN
      0910-6340, 1348-2246
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Miniaturization for the Development of High Performance Separation Systems2017

    • Author(s)
      Y. Saito, I. Ueta
    • Journal Title

      CHROMATOGRAPHY

      Volume: 38 Issue: 3 Pages: 85-94

    • DOI

      10.15583/jpchrom.2017.019

    • NAID

      130007040473

    • ISSN
      1342-8284, 1348-3315
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Unexpected Differences Between Planar and Column Liquid Chromatographic Retention of 1-Acenaphthenol Enantiomers Controlled by Supramolecular Interactions Involving β-Cyclodextrin at Subambient Temperatures2017

    • Author(s)
      H. Ohta, E. Wlodarczyk, K. Piaskowski, A. Kaleniecka, L. Lewandowska, M. J. Baran, M. Wojnicz, K. Jinno, Y. Saito and P. K. Zarzycki
    • Journal Title

      Analytical and Bioanalytical Chemistry

      Volume: 409 Issue: 14 Pages: 3695-3706

    • DOI

      10.1007/s00216-017-0313-y

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Determination of Gaseous Formic and Acetic Acids by a Needle-Type Extraction Device coupled to a Gas Chromatography-Barrier Discharge Ionization Detector2017

    • Author(s)
      I. Ueta, Y. Nakamura, K. Fujimura, S. Kawakubo and Y. Saito
    • Journal Title

      Chromatographia

      Volume: 80 Issue: 1 Pages: 151-156

    • DOI

      10.1007/s10337-016-3201-2

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Preconcentration of Aromatic Compounds in Aqueous Samples with a Polymer-coated Fiber-packed Capillary and Subsequent Temperature-programmed Elution with Water for Pseudo-2D LC Separations2015

    • Author(s)
      T. Tazawa Y. Mori, A. Kobayashi, K. Nakane, T. Monobe, I. Ueta and Y. Saito
    • Journal Title

      Analytical Sciences

      Volume: 31 Issue: 11 Pages: 1137-1141

    • DOI

      10.2116/analsci.31.1137

    • NAID

      130005108608

    • ISSN
      0910-6340, 1348-2246
    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Polymer-Coated Fiber-Packed Capillary as the Sample Preparation Medium in Liquid Chromatography: Heart-Cutting Analysis of Phthalates in Aqueous Matrices2015

    • Author(s)
      K. Nakane, T. Tazawa, Y. Mori, A. Kobayashi, I. Ueta and Y. Saito
    • Journal Title

      CHROMATOGRAPHY

      Volume: 36 Issue: 2 Pages: 61-65

    • DOI

      10.15583/jpchrom.2015.025

    • NAID

      130005098792

    • ISSN
      1342-8284, 1348-3315
    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Purge-and-Trap Analysis of Flavor Compounds inAqueous Samples by a Needle-Type Extraction Device2015

    • Author(s)
      I. Ueta, T Mitsumori, Y Suzuki, S. Kawakubo and Y. Saito
    • Journal Title

      CHROMATOGRAPHY

      Volume: 36 Issue: 3 Pages: 99-104

    • DOI

      10.15583/jpchrom.2015.031

    • NAID

      130005118197

    • ISSN
      1342-8284, 1348-3315
    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] 針型試料前処理デバイスを用いた揮発性アミンの抽出・誘導体化およびそのGC分析2018

    • Author(s)
      中神 光喜, 田澤 寿明, 隅谷 王士郎, 植田 郁生, 齊戸 美弘
    • Organizer
      第25回クロマトグラフィーシンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] 新規ポリマ-ベース固定相を用いたLCにおける多環芳香族化合物の保持挙動2018

    • Author(s)
      隅谷 王士郎, 中神 光喜, 小池 凌太, 植田 郁生, 齊戸 美弘
    • Organizer
      第25回クロマトグラフィーシンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] 試料濃縮針を用いた溶液中のギ酸及び酢酸のパージトラップ・GC-BID分析2017

    • Author(s)
      中村 陽平, 植田 郁生, 川久保 進, 齊戸 美弘
    • Organizer
      第24回クロマトグラフィーシンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] Online Coupled MicroSPE-LC for Pseudo LC-LC Separations2017

    • Author(s)
      Y. Saito, I. Ueta
    • Organizer
      Separation Science 2017
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] マイクロ化による分離分析システムの高性能化2016

    • Author(s)
      齊戸美弘
    • Organizer
      第27回クロマトグラフィー科学会議
    • Place of Presentation
      慶応義塾大学芝共立キャンパス(東京都港区)
    • Year and Date
      2016-11-16
    • Related Report
      2016 Research-status Report
    • Invited
  • [Presentation] ポリイミド繊維を固定相に用いたガスクロマトグラフィー2016

    • Author(s)
      中神光喜, 田澤 寿明, 植田郁生, 齊戸 美弘
    • Organizer
      第27回クロマトグラフィー科学会議
    • Place of Presentation
      慶応義塾大学芝共立キャンパス(東京都港区)
    • Year and Date
      2016-11-16
    • Related Report
      2016 Research-status Report
  • [Presentation] ポリイミド粒子を抽出媒体に用いた試料前処理およびHPLCへのオンライン結合2016

    • Author(s)
      田澤 寿明, 植田郁生, 白井友貴, 森内幸司, 齊戸 美弘
    • Organizer
      第27回クロマトグラフィー科学会議
    • Place of Presentation
      慶応義塾大学芝共立キャンパス(東京都港区)
    • Year and Date
      2016-11-16
    • Related Report
      2016 Research-status Report
  • [Presentation] 移動相にβ-シクロデキストリンを添加したHPLCにおける芳香族化合物の保持挙動2016

    • Author(s)
      隅谷王士郎, 田澤 寿明, 植田郁生, 齊戸 美弘
    • Organizer
      第27回クロマトグラフィー科学会議
    • Place of Presentation
      慶応義塾大学芝共立キャンパス(東京都港区)
    • Year and Date
      2016-11-16
    • Related Report
      2016 Research-status Report
  • [Presentation] 細繊維充填キャピラリーによる試料前処理とLC分離への応用2016

    • Author(s)
      齊戸美弘, 田澤寿明, 物部寛也, 植田郁生
    • Organizer
      日本分析化学会第65年会
    • Place of Presentation
      北海道大学工学部(北海道札幌市)
    • Year and Date
      2016-09-14
    • Related Report
      2016 Research-status Report
    • Invited
  • [Presentation] 移動相にシクロデキストリンを添加したHPLC2016

    • Author(s)
      田澤 寿明, 植田郁生, 齊戸 美弘
    • Organizer
      日本分析化学会第65年会
    • Place of Presentation
      北海道大学工学部(北海道札幌市)
    • Year and Date
      2016-09-14
    • Related Report
      2016 Research-status Report
  • [Presentation] ポリイミド粒子を抽出媒体に用いたLC用新規試料前処理デバイス2016

    • Author(s)
      渡部 暢, 田澤 寿明, 植田 郁生, 齊戸美弘
    • Organizer
      第23回クロマトグラフィーシンポジウム
    • Place of Presentation
      山梨県立図書館(山梨県甲府市)
    • Year and Date
      2016-06-15
    • Related Report
      2016 Research-status Report
  • [Presentation] ポリイミド粒子固定相に用いたガスクロマトグラフィーにおけるアルカンの保持挙動2015

    • Author(s)
      物部 寛也, 田澤 寿明, 植田 郁生, 白井 友貴, 森内 幸司, 齊戸 美弘
    • Organizer
      第26回クロマトグラフィー科学会議
    • Place of Presentation
      九州大学医系キャンパス(福岡県福岡市)
    • Year and Date
      2015-11-11
    • Related Report
      2015 Research-status Report
  • [Presentation] ポリイミド被覆シリカ固定相を用いた液体クロマトグラフィーにおける芳香族化合物の保持挙動2015

    • Author(s)
      田澤 寿明, 植田 郁生, 白井 友貴, 森内 幸司, 齊戸 美弘
    • Organizer
      第26回クロマトグラフィー科学会議
    • Place of Presentation
      九州大学医系キャンパス(福岡県福岡市)
    • Year and Date
      2015-11-11
    • Related Report
      2015 Research-status Report
  • [Presentation] ポリイミドを新規固定相として用いた液体クロマトグラフィー2015

    • Author(s)
      田澤 寿明, 植田 郁生, 白井 友貴, 森内 幸司, 齊戸 美弘
    • Organizer
      日本分析化学会第64年会
    • Place of Presentation
      九州大学伊都キャンパス(福岡県福岡市)
    • Year and Date
      2015-09-09
    • Related Report
      2015 Research-status Report
  • [Presentation] Miniaturized Sample Preparation Devices with Polymeric Extraction Media2015

    • Author(s)
      Y. Saito, T. Tazawa and I. Ueta
    • Organizer
      The 22nd International Symposium on Electro- and Liquid Phase-Sapration Techniques (ITP2015)
    • Place of Presentation
      Hotel Hanasaari (Espo, Finland)
    • Year and Date
      2015-08-30
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research / Invited

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Published: 2015-04-16   Modified: 2019-03-29  

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