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Formation of hetero-structured titanium with high performance and its evaluation of mechanism of damage

Research Project

Project/Area Number 15K05677
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionKobe University

Principal Investigator

KIKUCHI Shoichi  神戸大学, 工学研究科, 助教 (80581579)

Co-Investigator(Kenkyū-buntansha) 中井 善一  神戸大学, 工学研究科, 教授 (90155656)
Co-Investigator(Renkei-kenkyūsha) AMEYAMA Kei  立命館大学, 理工学部, 教授 (10184243)
Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2017: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2016: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2015: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Keywordsチタン / 粉末冶金 / 疲労 / 金属疲労
Outline of Final Research Achievements

Titanium alloy (Ti-6Al-4V) with a bimodal harmonic structure, which consists of a coarse-grained structure surrounded by a network structure of fine equiaxed grains, was fabricated to achieve high strength and ductility. K-decreasing tests were conducted to investigate the near-threshold fatigue crack propagation. The crack growth rates in the harmonic structured material were higher than a material with coarse grains while the fatigue thresholds were lower. In some areas, fatigue cracks preferentially propagated across the network structure of fine grains. Furthermore, small fatigue crack propagation was examined under four-point bending. Fatigue crack paths were not influenced by the bimodal harmonic structure, and the crack growth rates in the harmonic structured Ti-6Al-4V were almost the same as those in a material with coarse grains. In contrast, the harmonic structured Ti-6Al-4V had a higher resistance of fatigue crack initiation, which resulted in an increase of fatigue limit.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (31 results)

All 2018 2017 2016 2015 Other

All Journal Article (9 results) (of which Peer Reviewed: 9 results,  Acknowledgement Compliant: 4 results,  Open Access: 4 results) Presentation (20 results) (of which Int'l Joint Research: 7 results,  Invited: 5 results) Remarks (2 results)

  • [Journal Article] Statistical fatigue properties and small fatigue crack propagation in bimodal harmonic structured Ti-6Al-4V alloy under four-point bending2018

    • Author(s)
      S. Kikuchi, H. Kubozono, Y. Nukui, A. Ueno, M. O. Kawabata and K. Ameyama
    • Journal Title

      Materials Science and Engineering A

      Volume: 711 Pages: 29-36

    • DOI

      10.1016/j.msea.2017.11.010

    • NAID

      120006398791

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Fractographic analysis of fatigue crack initiation and propagation in CP titanium with a bimodal harmonic structure2018

    • Author(s)
      Y. Nukui, H. Kubozono, S. Kikuchi, Y. Nakai, A. Ueno, M.O. Kawabata and K. Ameyama
    • Journal Title

      Materials Science and Engineering A

      Volume: 716 Pages: 228-234

    • DOI

      10.1016/j.msea.2018.01.054

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Evaluation of near-threshold fatigue crack propagation in harmonic-structured CP Titanium with a bimodal grain size distribution2017

    • Author(s)
      S. Kikuchi, T. Mori, H. Kubozono, Y. Nakai, M.O. Kawabata and K. Ameyama,
    • Journal Title

      Engineering Fracture Mechanics

      Volume: 181 Pages: 77-86

    • DOI

      10.1016/j.engfracmech.2017.06.026

    • NAID

      120006398790

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Low Temperature Nitriding of Commercially Pure Titanium with Harmonic Structure2016

    • Author(s)
      菊池将一,中村悠太,太田美絵,上野明,飴山惠
    • Journal Title

      Journal of the Japan Society of Powder and Powder Metallurgy

      Volume: 63 Issue: 8 Pages: 731-738

    • DOI

      10.2497/jjspm.63.731

    • NAID

      130005253110

    • ISSN
      0532-8799, 1880-9014
    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Effect of harmonic structure design with bimodal grain size distribution on near-threshold fatigue crack propagation in Ti-6Al-4V alloy2016

    • Author(s)
      Shoichi Kikuchi, Takafumi Imai, Hiroki Kubozono, Yoshikazu Nakai, Mie Ota, Akira Ueno, Kei Ameyama
    • Journal Title

      International Journal of Fatigue

      Volume: 92 Pages: 616-622

    • DOI

      10.1016/j.ijfatigue.2016.02.038

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effect of bimodal grain size distribution on fatigue properties of Ti-6Al-4V alloy with harmonic structure under four-point bending2016

    • Author(s)
      S. Kikuchi, Y. Hayami, T. Ishiguri, B. Guennec, M. Ota, A. Ueno and K. Ameyama
    • Journal Title

      Materials Science and Engineering A

      Volume: 687 Pages: 269-275

    • DOI

      10.1016/j.msea.2017.01.076

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Evaluation of near-threshold fatigue crack propagation in Ti-6Al-4V alloy with harmonic structure created by mechanical milling and spark plasma sintering2015

    • Author(s)
      S. Kikuchi, T. Imai, H. Kubozono, Y. Nakai, A. Ueno and K. Ameyama
    • Journal Title

      Fracture and Structural Integrity

      Volume: 34 Issue: 34 Pages: 261-270

    • DOI

      10.3221/igf-esis.34.30

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Evaluation of the Fatigue Properties of Ti-6Al-4V Alloy with Harmonic Structure in 4-Points Bending2015

    • Author(s)
      S. Kikuchi, K. Takemura, Y. Hayami, A. Ueno and K. Ameyama
    • Journal Title

      Journal of the Society of Materials Science, Japan

      Volume: 64 Issue: 11 Pages: 880-886

    • DOI

      10.2472/jsms.64.880

    • NAID

      130005109750

    • ISSN
      0514-5163, 1880-7488
    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] Low Temperature Nitriding of Commercially Pure Titanium with Harmonic Structure2015

    • Author(s)
      S. Kikuchi, Y. Nakamura, A. Ueno and K. Ameyama
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 56 Issue: 11 Pages: 1807-1813

    • DOI

      10.2320/matertrans.Y-M2015822

    • NAID

      130005104240

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] Small fatigue crack propagation in bimodal harmonic structured CP titanium and Ti-6Al-4V alloy2018

    • Author(s)
      S. Kikuchi
    • Organizer
      4th Symposium on the Ritsumeikan University Research Center for Energy-Innovation Materials
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 加工熱処理された工業用純チタン調和組織材料の4点曲げ疲労特性2018

    • Author(s)
      大崎航平,温井悠平,菊池将一,中井善一,川畑美絵,飴山恵
    • Organizer
      日本機械学会関西学生会平成29年度学生員卒業研究発表講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 強度と延性を兼ね備えた調和組織材料の疲労破壊メカニズム解明2018

    • Author(s)
      菊池将一
    • Organizer
      第8回産学新日鐵住金シンポジウム
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] 調和組織を有する工業用純チタンの4 点曲げ疲労特性2017

    • Author(s)
      温井悠平,久保薗宏樹,菊池将一,中井善一,太田美絵,飴山惠
    • Organizer
      日本機械学会関西学生会 平成28 年度学生員卒業研究発表講演会
    • Place of Presentation
      大阪大学(大阪府・吹田市)
    • Year and Date
      2017-03-11
    • Related Report
      2016 Research-status Report
  • [Presentation] Effect of bimodal grain size distribution on fatigue properties of Ti-6Al-4V alloy with harmonic structure2017

    • Author(s)
      Shoichi Kikuchi, Hiroki Kubozono, Yoshikazu Nakai, Takayuki Ishiguri, Mie Ota, Akira Ueno and Kei Ameyama
    • Organizer
      6th International Symposium on Functionalization and Applications of Soft/Hard Materials
    • Place of Presentation
      立命館大学(滋賀県・草津市)
    • Year and Date
      2017-01-21
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Evaluation of four-point bending fatigue properties and crack propagation of commercially pure titanium with harmonic structure2017

    • Author(s)
      Y. Nukui, H. Kubozono, S. Kikuchi, Y. Nakai, M.O. Kawabata, K. Ameyama
    • Organizer
      14th International Conference on Fracture
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 調和組織を有する工業用純チタンの微小疲労き裂発生および伝ぱ特性2017

    • Author(s)
      温井悠平,久保薗宏樹,菊池将一,中井善一,太田美絵,上野明,飴山恵
    • Organizer
      日本材料学会第66期学術講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Study of the crack initiation mechanism of Ti-6Al-4V designed in harmonic structure2017

    • Author(s)
      ゲネックベンジャミン,石栗崇之,菊池将一,上野明
    • Organizer
      日本材料学会第115回フラクトグラフィ部門委員会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 高強度・高延性を有する工業用純チタンの疲労き裂発生および進展メカニズム2017

    • Author(s)
      温井悠平,久保薗宏樹,菊池将一,中井善一,川畑美絵,上野明,飴山恵
    • Organizer
      日本材料学会第15回機械・構造物の強度設計,安全性評価に関するシンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] 調和組織を有するTi-6Al-4V合金の4点曲げ疲労特性評価と破壊起点の結晶方位解析2016

    • Author(s)
      石栗崇之,上野明,ゲネック ベンジャミン,菊池将一
    • Organizer
      日本材料学会第14回フラクトグラフィシンポジウム
    • Place of Presentation
      京都テルサ(京都府・京都市)
    • Year and Date
      2016-10-14
    • Related Report
      2016 Research-status Report
  • [Presentation] 調和組織を有するTi-6Al-4V 合金の微小疲労き裂発生および伝ぱ挙動2016

    • Author(s)
      久保薗宏樹,菊池将一,中井善一,上野明,飴山惠
    • Organizer
      日本機械学会M&M2016 材料力学カンファレンス
    • Place of Presentation
      神戸大学(兵庫県・神戸市)
    • Year and Date
      2016-10-08
    • Related Report
      2016 Research-status Report
  • [Presentation] Fatigue properties and fatigue crack propagation in Ti-based harmonic structural materials2016

    • Author(s)
      Shoichi Kikuchi, Hiroki Kubozono, Tetsuya Mori, Yoshikazu Nakai, Mie Ota, Akira Ueno and Kei Ameyama
    • Organizer
      1st International Hetero-Structure Materials Workshop
    • Place of Presentation
      立命館大学(滋賀県・草津市)
    • Year and Date
      2016-08-06
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] 調和組織を有する工業用純チタンの下限界近傍における疲労き裂伝ぱ特性2016

    • Author(s)
      森徹也,久保薗宏樹,今井貴文,菊池将一,中井善一,上野明,飴山惠
    • Organizer
      日本機械学会関西学生会平成27年度学生員卒業研究発表講演会
    • Place of Presentation
      大阪電気通信大学(大阪府寝屋川市)
    • Year and Date
      2016-03-10
    • Related Report
      2015 Research-status Report
  • [Presentation] Effect of Harmonic Structure on the Four-point Bending Fatigue Properties and Fatigue Crack Propagation of Ti-6Al-4V Alloy2016

    • Author(s)
      Shoichi Kikuchi, Takafumi Imai, Hiroki Kubozono, Yoshikazu Nakai, Mie Ota, Akira Ueno and Kei Ameyama
    • Organizer
      5th International Symposium on Functionalization and Applications of Soft/Hard Materials
    • Place of Presentation
      立命館大学びわこ・くさつキャンパス(滋賀県草津市)
    • Year and Date
      2016-01-23
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] 調和組織を有するTi-6Al-4V合金の疲労き裂伝ぱ特性に及ぼす応力比の影響2015

    • Author(s)
      今井貴文,久保薗宏樹,菊池将一,中井善一,上野明,飴山惠
    • Organizer
      日本機械学会M&M2015材料力学カンファレンス
    • Place of Presentation
      慶應義塾大学矢上キャンパス(神奈川県横浜市)
    • Year and Date
      2015-11-21
    • Related Report
      2015 Research-status Report
  • [Presentation] Effects of Harmonic Structure and Grain Size on Fatigue Crack Propagation of Ti-6Al-4V Alloy2015

    • Author(s)
      Hiroki Kubozono, Takafumi Imai, Shoichi Kikuchi, Yoshikazu Nakai, Akira Ueno and Kei Ameyama
    • Organizer
      International Conference on Advanced Technology in Experimental Mechanics 2015
    • Place of Presentation
      ロワジールホテル豊橋(愛知県豊橋市)
    • Year and Date
      2015-10-05
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 調和組織を有するTi-6Al-4V合金の4点曲げ疲労特性評価2015

    • Author(s)
      早水洋介,菊池将一,吉田翔,上野明,飴山惠
    • Organizer
      日本機械学会2015年度年次大会
    • Place of Presentation
      北海道大学(北海道札幌市)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Research-status Report
  • [Presentation] Evaluation of Near-threshold Fatigue Crack Propagation in Ti-6Al-4V Alloy with Harmonic Structure Created by Mechanical Milling and Spark Plasma Sintering2015

    • Author(s)
      Shoichi Kikuchi, Takafumi Imai, Hiroki Kubozono, Yoshikazu Nakai, Akira Ueno and Kei Ameyama
    • Organizer
      The 5th International Conference on Crack Paths
    • Place of Presentation
      Ferrara (ITALY)
    • Year and Date
      2015-09-16
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 粉末冶金を利用した高機能チタンの開発とその疲労特性評価2015

    • Author(s)
      菊池将一,今井貴文,久保薗宏樹,中井善一,太田美絵,上野明,飴山惠
    • Organizer
      日本材料学会第40回生体・医療材料部門委員会
    • Place of Presentation
      神戸大学六甲台第2キャンパス(兵庫県神戸市)
    • Year and Date
      2015-08-04
    • Related Report
      2015 Research-status Report
  • [Presentation] Ti-6Al-4V合金の疲労き裂伝ぱ特性に及ぼす調和組織の影響2015

    • Author(s)
      久保薗宏樹,今井貴文,菊池将一,中井善一,上野明,飴山惠
    • Organizer
      日本材料学会第64期学術講演会
    • Place of Presentation
      山形大学米沢キャンパス(山形県米沢市)
    • Year and Date
      2015-05-23
    • Related Report
      2015 Research-status Report
  • [Remarks]

    • URL

      https://scholar.google.co.jp/citations?user=JDyyTcYAAAAJ&hl=ja

    • Related Report
      2017 Annual Research Report
  • [Remarks] 神戸大学研究者紹介システム

    • URL

      http://kuid.ofc.kobe-u.ac.jp/InfoSearch/?language=ja

    • Related Report
      2016 Research-status Report

URL: 

Published: 2015-04-16   Modified: 2019-03-29  

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