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Development of control technology for flame synthesis by clustered microflame

Research Project

Project/Area Number 15K05843
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Thermal engineering
Research InstitutionChubu University

Principal Investigator

HIRASAWA Taro  中部大学, 工学部, 教授 (30350987)

Research Collaborator WINTER Michael  
SAITO Kozo  
ISHINO Yojiro  
Project Period (FY) 2015-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
Fiscal Year 2017: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2016: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2015: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Keywords還元合成 / 合成条件制御 / 温度履歴計測 / 火炎構造計測 / 加熱時間制御 / 加熱温度制御 / 粒子加熱時間 / 粒子加熱温度 / 微小拡散火炎群内部のガス組成 / 3次元火炎構造 / 火炎による粒子還元合成 / 火炎合成反応場の制御 / 粒子温度履歴の計測 / 還元合成の実現 / 粒子温度履歴計測 / 3次元火炎構造 / 粒子温度計測 / 火炎融合状態のマッピング / 火炎形状計測 / 粒子温度分布計測 / 速度分布計測
Outline of Final Research Achievements

In order to achieve the control of flame synthesis by clustered microflames, the temperature, time and gas composition during particle travel in the synthesis field were measured at varied parameters of the distance between the fuel gas jets and the flow rate of the fuel and air jets. Then, the main part of the method of controlling flame synthesis was clarified in the present research project, particularly owing to obtaining the temperature histories of the raw material particles by measuring the velocity and temperature distribution, and revealing the complex three-dimensional structure of the clustered microflames by applying the CT method to the chemiluminescence from the flame front. Furthermore, by achieving highly reductive gas composition where material particles were introduced, the present project succeeded in the reduction synthesis of fine particles, which demonstrated its technical achievements most clearly.

Academic Significance and Societal Importance of the Research Achievements

拡散が支配的となる微小スケールでの燃焼現象の解明に関する進展は、本研究成果の学術的意義と言える。また、その解明により成された燃焼制御は燃焼利用の高度化につながり、例えば本研究では、火炎により酸化チタンから低次酸化チタンの還元合成に成功し、その技術的・社会的意義の一端が示された.低次酸化チタンは,省エネ効果のある外壁塗料、肌に優しく安全な化粧品原料、燃料電池やバッテリーなどの電極材料としても期待されている。この新たな合成手法を用いることで、従来の手法では合成できなかった様々な新材料の開発につながると期待される。

Report

(5 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Research-status Report
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (22 results)

All 2019 2018 2017 2016 Other

All Int'l Joint Research (4 results) Journal Article (3 results) (of which Int'l Joint Research: 3 results,  Peer Reviewed: 3 results,  Open Access: 1 results) Presentation (13 results) (of which Int'l Joint Research: 5 results) Remarks (1 results) Patent(Industrial Property Rights) (1 results)

  • [Int'l Joint Research] University of Kentucky(米国)

    • Related Report
      2018 Annual Research Report
  • [Int'l Joint Research] University of Kentucky(米国)

    • Related Report
      2017 Research-status Report
  • [Int'l Joint Research] University of Kentucky(米国)

    • Related Report
      2016 Research-status Report
  • [Int'l Joint Research] University of Kentucky(米国)

    • Related Report
      2015 Research-status Report
  • [Journal Article] Characterization of six clustered methane-air diffusion microflames through spectroscopic and tomographic analysis of CH* and C2* chemiluminescence2019

    • Author(s)
      Diao Zhaojin、Winter Michael、Hirasawa Taro、Kato Yuichi、Ishino Yojiro、Saito Kozo
    • Journal Title

      Experimental Thermal and Fluid Science

      Volume: 102 Pages: 20-27

    • DOI

      10.1016/j.expthermflusci.2018.10.032

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Characterization of the thermal structure of six clustered microflames seeded with TaN particles through emission spectroscopy2018

    • Author(s)
      Diao Zhaojin、Winter Michael、Hirasawa Taro、Saito Kozo
    • Journal Title

      Experimental Thermal and Fluid Science

      Volume: 96 Pages: 295-302

    • DOI

      10.1016/j.expthermflusci.2018.03.022

    • Related Report
      2017 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Heating Characteristics of Methane Diffusion Microflame Established on Stainless Steel and Copper Micro-tube Burner2018

    • Author(s)
      平沢 太郎、松岡 常吉、中村 祐二
    • Journal Title

      Journal of the Japanese Society for Experimental Mechanics

      Volume: 17 Issue: 4 Pages: 320-325

    • DOI

      10.11395/jjsem.17.320

    • NAID

      130006318284

    • ISSN
      1346-4930, 1884-4219
    • Related Report
      2017 Research-status Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Presentation] 微小拡散火炎群による低次酸化チタン粒子の還元合成2018

    • Author(s)
      加藤祐一, 平沢太郎, 加藤圭一
    • Organizer
      化学工学会第50回秋季大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Silicon Carbide as Seed Particle for Flame Temperature Measurement Based on Emission Spectroscopy2018

    • Author(s)
      Yuta UCHIDA, Yuichi KATO, Taro HIRASAWA
    • Organizer
      13th International Symposium on Advanced Science and Technology in Experimental Mechanics (13th ISEM'18)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 6つの燃料噴流と1つの空気噴流で形成される微小拡散火炎群による微粒子の還元合成2018

    • Author(s)
      加藤祐一, 平沢太郎, 加藤圭一
    • Organizer
      第56回燃焼シンポジウム
    • Related Report
      2018 Annual Research Report
  • [Presentation] Characterization of different microflame burner designs seeded with TaN particles through emission spectroscopy2017

    • Author(s)
      Z. Diao, M. Winter, T. Hirasawa, K. Saito
    • Organizer
      10th US National Combustion Meeting
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research
  • [Presentation] Structure of Six Clustered Methane-Air Diffusion Microflames2017

    • Author(s)
      Zhaojin Diao, Kozo Saito, Michael Winter, Taro Hirasawa
    • Organizer
      The 8th International Symposium on Scale Modeling (ISSM-8)
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research
  • [Presentation] Three-Dimensional Flame Structure and Characteristics of Heating Particles in Methane Clustered Microflames on Six Fuel and One Air Jets2017

    • Author(s)
      Yuichi Kato, Taro Hirasawa, Zhaojin Diao, Michael Winter, Yojiro Ishino
    • Organizer
      The Ninth JSME-KSME Thermal and Fluids Engineering Conference (TFEC9)
    • Related Report
      2017 Research-status Report
    • Int'l Joint Research
  • [Presentation] 6つの燃料噴流と 1つの空気噴流で形成さ れる微小火炎群による添 加粒子の酸化特性2017

    • Author(s)
      加藤祐一,平沢太郎,Zhaojin Diao, Michael Winter
    • Organizer
      第55回燃焼シンポジウム
    • Related Report
      2017 Research-status Report
  • [Presentation] 6つの燃料噴流と1つの空気噴流で形成される微小火炎群の三次元火炎構造と微粒子の加熱特性2017

    • Author(s)
      加藤祐一,平沢太郎, Michael Winter,Zhaojin Diao, 石野洋二郎
    • Organizer
      第26 回日本エネルギー学会大会
    • Related Report
      2017 Research-status Report
  • [Presentation] 6つの燃料噴流と1つの空気噴流で形成される微小火炎群のCH*発光および熱的特性2016

    • Author(s)
      平沢太郎
    • Organizer
      第54回燃焼シンポジウム
    • Place of Presentation
      仙台国際センター(仙台市)
    • Year and Date
      2016-11-23
    • Related Report
      2016 Research-status Report
  • [Presentation] メタン微小火炎群による微粒子加熱とその火炎構造に関する検討2016

    • Author(s)
      平沢太郎
    • Organizer
      熱工学コンファレンス2016
    • Place of Presentation
      愛媛大学(松山市)
    • Year and Date
      2016-10-22
    • Related Report
      2016 Research-status Report
  • [Presentation] Characterization of a Methane-Air Diffusion Microflame with Seeding Particles through Emission Spectroscopy2016

    • Author(s)
      平沢太郎
    • Organizer
      WiPP at 36th international symposium on combustion
    • Place of Presentation
      COEX, Seoul, Korea
    • Year and Date
      2016-07-31
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Characterization of a Methane-Air Diffusion Microflame with Seeding Particles through Emission Spectroscopy2016

    • Author(s)
      Zhaojin Diao
    • Organizer
      2016 Spring Technical Meeting Central States Section of the Combustion Institute
    • Place of Presentation
      Knoxville, Tennessee, USA
    • Year and Date
      2016-05-15
    • Related Report
      2016 Research-status Report
  • [Presentation] Characterization of a Methane-Air Diffusion Microflame with Seeding Particles through Emission Spectroscopy2016

    • Author(s)
      Zhaojin Diao, Michael Winter, Taro Hirasawa, Kozo Saito
    • Organizer
      The 2016 Spring Technical Meeting of the Central States Section of The Combustion Institute
    • Place of Presentation
      Knoxville, USA
    • Year and Date
      2016-05-15
    • Related Report
      2015 Research-status Report
  • [Remarks] 炎で機能性材料を合成する新技術を開発 ─塗料や化粧品生産から応用─ (平沢太郎教授ら)

    • URL

      https://www3.chubu.ac.jp/research/news/24327/

    • Related Report
      2018 Annual Research Report
  • [Patent(Industrial Property Rights)] 還元性無機酸化物の火炎合成による製造方法2018

    • Inventor(s)
      平沢太郎,加藤祐一,内田裕太,岩ケ谷進介,服部絵美,加藤圭一
    • Industrial Property Rights Holder
      中部大学,三商株式会社
    • Industrial Property Rights Type
      特許
    • Filing Date
      2018
    • Related Report
      2018 Annual Research Report

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Published: 2015-04-16   Modified: 2022-06-07  

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