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Elucidation of abnormal phenomena of elongation increase induced by He in metal

Research Project

Project/Area Number 15K06423
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Physical properties of metals/Metal-base materials
Research InstitutionKyoto University

Principal Investigator

Xu Qiu  京都大学, 原子炉実験所, 准教授 (90273531)

Co-Investigator(Kenkyū-buntansha) 張 倹  京都大学, 原子炉実験所, 技術職員 (30379010)
Research Collaborator LUO Laima  合肥工業大学, 准教授
CAO Xingzhong  高エネルギー物理研究所, 准教授
WANG Yuxia  復旦大学, 准教授
Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2017: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2016: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2015: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Keywords鉄 / 力学特性 / 転位 / 原子空孔 / ヘリウム / 水素 / 脆化 / ヘリウム注入 / 金属 / 欠陥 / 引張強度
Outline of Final Research Achievements

He atoms are insoluble in most metals, and the presence of He atoms in metals decreases the ductility. Recently, however, Xu et al. indicated that He implantation increased the total elongation of pure Fe and Ni containing only dislocations. In order to understand the mechanism of this phenomenon, the interaction between He atoms and defects in Fe was investigated. He atoms were trapped at the dislocations in Fe containing only dislocations when He was implanted. The He atoms were once released from the dislocation during tension and were trapped again at vacancies induced by tension. Therefore, vacancy aggregation, in other words, the nucleation and growth of cracks were suppressed. As a result, elongation increased. By this method, hydrogen embrittlement in iron is also reduced.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (44 results)

All 2018 2017 2016 Other

All Int'l Joint Research (1 results) Journal Article (32 results) (of which Int'l Joint Research: 21 results,  Peer Reviewed: 32 results,  Open Access: 2 results,  Acknowledgement Compliant: 2 results) Presentation (10 results) Remarks (1 results)

  • [Int'l Joint Research] 合肥工業大学/中国科学院高エネルギー物理研究所/復旦大学(中国)

    • Related Report
      2017 Annual Research Report
  • [Journal Article] Repair Behavior of He-Irradiated W-Y2O3 Composites after Different Temperature-Isochronal Annealing Experiments2018

    • Author(s)
      G. Yao, X.Y. Tan, L.M. Luo, X. Zan, J.Q. Liu, Q. Xu, X.Y. Zhu, Y.C. Wu
    • Journal Title

      Nuclear Inst. and Methods in Physics Research B

      Volume: 415 Pages: 82-88

    • DOI

      10.1016/j.nimb.2017.11.013

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Deuterium Trapping at Vacancy Clusters in Electron/Neutron-Irradiated Tungsten Studied by Positron Annihilation Spectroscopy2018

    • Author(s)
      T. Toyama, K. Ami, K. Inoue, Y. Nagai, K. Sato, Q. Xu, Y. Hatano
    • Journal Title

      Journal of Nuclear Materials

      Volume: 499 Pages: 464-470

    • DOI

      10.1016/j.jnucmat.2017.11.002

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Microstructure and Damage Behavior of W-Cr Alloy under He Irradiation2018

    • Author(s)
      K. Huang, L.M. Luo, X. Zan, Q. Xu, D.G. Liu, X.Y. Zhu, J.G. Cheng, Y.C. Wu
    • Journal Title

      Journal of Nuclear Materials

      Volume: 501 Pages: 181-188

    • DOI

      10.1016/j.jnucmat.2018.01.019

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Microstructure and Helium Irradiation Performance of W-ZrC/Sc2O3 Composites Prepared Spark Plasma Sintering2018

    • Author(s)
      H.Y. Chen, L.M. Luo, X. Zan, Q. Xu, X.Y. Zhu, J.Q. Liu, J.G. Cheng, Y.C. Wu
    • Journal Title

      International Journal of Refractory Metals & Hard Materials

      Volume: 72 Pages: 373-379

    • DOI

      10.1016/j.ijrmhm.2018.01.011

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Influence of Nb Content on the Microstructure and Deuterium Retention of W-Nb Alloys2018

    • Author(s)
      L.M. Luo, J.B. Chen, J.S. Lin, X. Zan, X.Y. Zhu, Q. Xu, Y.C. Wu
    • Journal Title

      Fusion Engineering and Design

      Volume: 129 Pages: 120-129

    • DOI

      10.1016/j.fusengdes.2018.02.085

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Charaterization of Helium-Vacancy Complexes in He-Ions Implanted Fe9Cr by using Positron Annihilation Spectroscopy2018

    • Author(s)
      T. Zhu, S.X. Jin, P. Zhang, L.G. Song, X.Y. Lian, P. Fan, Q.L. Zhang, D.Q. Yuan, H.B. Wu, R.S. Yu, X.Z. Cao, Q. Xu, B.Y. Wang
    • Journal Title

      Journal of Nuclear Materials

      Volume: 505 Pages: 69-72

    • DOI

      10.1016/j.jnucmat.2018.03.048

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Novel Methods for Prevention of Hydrogen Embrittlement in Iron2017

    • Author(s)
      Q. Xu, J. Zhang
    • Journal Title

      Scientific Reports

      Volume: 7 Issue: 1 Pages: 16927-16927

    • DOI

      10.1038/s41598-017-17263-8

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] D2 Retention and Microstructural Evolution during He Irradiation in Candidate Plasma Facing Material W-La2O3 Alloy2017

    • Author(s)
      Q. Xu, X.Y. Ding, L.M. Luo, M. Miyamoto, M. Tokitani, J. Zhang, Y.C. Wu
    • Journal Title

      Journal of Nuclear Materials

      Volume: 496 Pages: 227-233

    • DOI

      10.1016/j.jnucmat.2017.09.033

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Microstructural Evolution and Changes in Mechanical Property of Irradiated Fe-0.6Cu Alloy under Uniaxial Tension Stress in Reactor2017

    • Author(s)
      Q. Xu, T. Yokotani, J. Zhang
    • Journal Title

      Radiation Effects & Defects in Solids

      Volume: 172 Issue: 3-4 Pages: 305-312

    • DOI

      10.1080/10420150.2017.1313842

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Microstructure and Deuterium Retention after Ion Irradiation of W-Lu2O3 Composites2017

    • Author(s)
      J.S. Lin, L.M. Luo, Q. Xu, X. Zan, X.Y. Zhu, Y.C. Wu
    • Journal Title

      Journal of Nuclear Materials

      Volume: 490 Pages: 272-278

    • DOI

      10.1016/j.jnucmat.2017.04.042

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] The Influence of Dislocation and Hydrogen on Thermal Helium Desoption Behavior in Fe9Cr Alloys2017

    • Author(s)
      T. Zhu, S.X. Jin, Y.H. Gong, E.Y. Lu, L.G. Song, Q. Xu, L.P. Guo, X.Z. Cao, B.Y. Wang
    • Journal Title

      Journal of Nuclear Materials

      Volume: 495 Pages: 244-248

    • DOI

      10.1016/j.jnucmat.2017.08.027

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Quantitative Evaluation of Hydrogen Atoms Trapped at Single Vacancies in Tungsten using Positron Annihilation lifetime Measurements: Experiments and Theoretical Calculations2017

    • Author(s)
      K .Sato, A. Hirosako, K. Ishibashi, Y. Miura, Q. Xu, M. Onoue, Y. Fukutoku, T. Onitsuka, M. Hatakeyama, S. Sunada, T. Yoshiie
    • Journal Title

      Journal of Nuclear Materials

      Volume: 496 Pages: 9-17

    • DOI

      10.1016/j.jnucmat.2017.09.002

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effects of He, D Interaction on Thermal Desorption of He and D2 and Microstructural Evolution in Pure Fe2016

    • Author(s)
      Q. Xu, J. Zhang
    • Journal Title

      J. Nucl. Mater.

      Volume: 479 Pages: 255-259

    • DOI

      10.1016/j.jnucmat.2016.07.032

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Retention and Thermal Desorption of Helium in Pure Tungsten2016

    • Author(s)
      Q. Xu, J. Zhang, K. Maejima, N. Hirashita
    • Journal Title

      Phil. Mag. Lett.

      Volume: 96 Pages: 477-481

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Electrical resistivity measurement of Fe-0.6%Cu alloy irradiated by neutrons at 14-19 K2016

    • Author(s)
      Q. Xu, T. Yokotani, K. Sato, F. Hori
    • Journal Title

      Journal of Nuclear Materials

      Volume: 481 Pages: 176-180

    • DOI

      10.1016/j.jnucmat.2016.09.023

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Synchrotron VUV-UV and Positron Lifetime Spectroscopy Study of Vacancy-Type Defects in Reactor Neutron-Irradiated MgO・nAl2O3 n(=2)2016

    • Author(s)
      A.Z.M.S. Rahman, X.Z. Cao, B.Y. Wang, J. Evslin, Q. Xu, K. Atobe
    • Journal Title

      Cogent Physics

      Volume: 3 Issue: 1 Pages: 1133481-1133481

    • DOI

      10.1080/23311940.2015.1133481

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Subcascade Formation Ratio in Neutron-Irradiated Stainless Steels2016

    • Author(s)
      T. Yoshiie, Y. Satoh, S.S. Huang, M. Horiki, K. Sato, Q. Xu
    • Journal Title

      J. Phys. C

      Volume: 674 Pages: 012002-012002

    • DOI

      10.1088/1742-6596/674/1/012002

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Ni Ion Damage Structures and Hardness Changes in Austenitic Stainless Steels and Their Model Alloys2016

    • Author(s)
      K. Sato, S. Ishioka, Q. Xu, T. Yoshiie, H. Tsuchida, A. Itoh
    • Journal Title

      J. Phys. C

      Volume: 674 Pages: 012009-012009

    • DOI

      10.1088/1742-6596/674/1/012009

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Electron Irradiation-Induced Defects in Mo-Diluted FeCrNi Austenitic Alloy during Void Swelling Incubation2016

    • Author(s)
      B.Y. Wang, E.Y. Lu, C.X. Zhang, Q. Xu, S.X. Jin, P. Zhang, X.Z. Cao
    • Journal Title

      J. Phys. C

      Volume: 674 Pages: 012010-012010

    • DOI

      10.1088/1742-6596/674/1/012010

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Laser Excited Novel Near-Infrared Photoluminescence Bands in Fast Neutron-Irradiated MgO・nAl2O32016

    • Author(s)
      A.Z.M.S. Rahman, A.S.M.A. Haseeb, Q. Xu, J. Evslin, M. Cinausero
    • Journal Title

      Radiat. Phys. Chem.

      Volume: 125 Pages: 122-126

    • DOI

      10.1016/j.radphyschem.2016.04.001

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Effects of Cr and W on defects evolution in irradiated F82H model alloys2016

    • Author(s)
      S.S. Huang, Q. Xu, T. Yoshiie
    • Journal Title

      Materials Letters

      Volume: 178 Pages: 272-275

    • DOI

      10.1016/j.matlet.2016.05.019

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Properties of Lu2O3 Doped Tungsten and Thermal Shock Performance2016

    • Author(s)
      S. Wang, J. Zhang, L.M. Luo, X. Zan, Q. Xu, X.Y. Zhu, K. Tokunaga, Y.C. Wu
    • Journal Title

      Powder Technol.

      Volume: 301 Pages: 65-69

    • DOI

      10.1016/j.powtec.2016.05.056

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Effects of Zirconium Element on the Microstructure and Deuterium Retention of W-Zr/Sc2O3 Composites2016

    • Author(s)
      H.Y. Chen, L.M. Luo, J.B. Chen, X. Zan, X.Y. Zhu, Q. Xu, G.N. Luo, J.L. Chen, Y.C. Wu
    • Journal Title

      Sci. Rep.

      Volume: 6 Issue: 1 Pages: 32678-32678

    • DOI

      10.1038/srep32678

    • NAID

      120006840156

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Microstructure and Performance of Rare Earth Element-Strengthened Plasma-Facing Tungsten Material2016

    • Author(s)
      L.M. Luo, J. Shi, J.S. Lin, X. Zan, X.Y. Zhu, Q. Xu, Y.C. Wu
    • Journal Title

      Sci. Rep.

      Volume: 6 Issue: 1 Pages: 32701-32701

    • DOI

      10.1038/srep32701

    • NAID

      120006345017

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Effect of Dislocations on Helium Retention in Deformed Pure Iron2016

    • Author(s)
      Y.H. Gong, X.Z. Cao, S.X. Jin, E.Y. Lu, Y.C. Hu, T. Zhu, P. Kuang, Q. Xu, B.Y. Wang
    • Journal Title

      J. Nucl. Mater.

      Volume: 482 Pages: 93-98

    • DOI

      10.1016/j.jnucmat.2016.10.014

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Investigation of Microstructure and Irradiation Behavior of W-Nb/Ti Composites Prepared by Spark Plasma Sintering2016

    • Author(s)
      J.B. Chen, L.M. Luo, M.L. Zhao, Q. Xu, X. Zan, Y.C. Wu
    • Journal Title

      Fusion Eng. Des.

      Volume: 112 Pages: 349-354

    • DOI

      10.1016/j.fusengdes.2016.07.003

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Damage Behavior of REE-Doped W-Based Material Exposed to High-Flux Transient Heat Loads2016

    • Author(s)
      J. Shi, L.M. Luo, J.S. Lin, X. Zan, X.Y. Zhu, Q. Xu, Y.C. Wu
    • Journal Title

      Fusion Eng. Des.

      Volume: 113 Pages: 92-101

    • DOI

      10.1016/j.fusengdes.2016.11.005

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Detection of Deuterium Sites in Tungsten by Thermal Desorption Spectroscopy and Positron Annihilation Spectroscopy2016

    • Author(s)
      K. Sato, R. Tamiya, Q. Xu, H. Tsuchida, T. Yoshiie
    • Journal Title

      Nucl. Mater. Energ.

      Volume: 9 Pages: 554-559

    • DOI

      10.1016/j.nme.2016.09.014

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Effect of Second-Phase Particles on the Properties of W-Based Materials under High-Heat Loading2016

    • Author(s)
      X.Y. Tan, P. Li, L.M. Luo, Q. Xu, K. Tokunaga, X. Zan, Y.C. Wu
    • Journal Title

      Nucl. Mater. Energ.

      Volume: 9 Pages: 399-404

    • DOI

      10.1016/j.nme.2016.07.009

    • NAID

      120005997678

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Irradiation Damage from Low-Dose High-Energy Protons on Mechanical Properties and Positron Annihilation Lifetimes of Fe-9Cr alloy2016

    • Author(s)
      Q. Xu, K. Fukumoto, Y. Ishi, Y. Kuriyama, T. Uesugi, K. Sato, Y. Mori, T. Yoshiie
    • Journal Title

      Journal of Nuclear Materials

      Volume: 468 Pages: 260-263

    • DOI

      10.1016/j.jnucmat.2015.07.011

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] The Tolerance of Ti3SiC2 to Hydrogen-Induced Embrittlement: A First Principles Calculation2016

    • Author(s)
      H.F. Zhang, B.D. Yao, J.Y. Zhang, Q. Xu, Y.J. Feng, Y.X.Wang
    • Journal Title

      Materials Letters

      Volume: 166 Pages: 93-96

    • DOI

      10.1016/j.matlet.2015.12.021

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Defect Structures of F82H Irradiated at SINQ Using Positron Annihilation Spectroscopy2016

    • Author(s)
      K. Sato, K. Ikemura, V. Krsjak, C. Vieh, R. Brun, Q. Xu, T. Yoshiie, Y. Dai
    • Journal Title

      Journal of Nuclear Materials

      Volume: 468 Pages: 281-284

    • DOI

      10.1016/j.jnucmat.2015.03.055

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Presentation] B2型金属間化合物中の欠陥における水素捕獲2018

    • Author(s)
      角倉優雅、鷹野陽弘、岩瀬彰宏、Q. Xu、大澤一人、堀史説
    • Organizer
      金属学会
    • Related Report
      2017 Annual Research Report
  • [Presentation] γ線照射還元法を用いた多元系金属ナノ微粒子の合成2017

    • Author(s)
      戸田晋太郎、田中元彬、岩瀬彰宏、田口昇、田中真悟、徐ぎゅう、堀史説
    • Organizer
      第160回金属学会
    • Place of Presentation
      首都大学東京南大沢キャンパス
    • Year and Date
      2017-03-15
    • Related Report
      2016 Research-status Report
  • [Presentation] ZnOバルク単結晶へのガンマ線照射効果:低抵抗化の起源2017

    • Author(s)
      田代 惇也, 取田 祐樹, 栗山 一男, 串田 一雅, 徐 ぎゅう, 木野村 淳
    • Organizer
      第64回応用物理学会
    • Place of Presentation
      パシフィコ横浜
    • Year and Date
      2017-03-14
    • Related Report
      2016 Research-status Report
  • [Presentation] 電子線照射FeAl金属間化合物中の空孔による水素捕獲2017

    • Author(s)
      上野陽平、岩瀬彰宏、徐ぎゅう、佐藤紘一、大澤一人、河裾厚男、前川雅樹、斎藤勇一、堀史説
    • Organizer
      第51回KUR学術講演会
    • Place of Presentation
      京大・原子炉
    • Related Report
      2016 Research-status Report
  • [Presentation] KUR B1孔を利用した低速陽電子ビームライン輝度増強部の開発2017

    • Author(s)
      葛谷佳広、大島永康、木野村淳、籔内敦、佐藤紘一、徐ぎゅう
    • Organizer
      第51回KUR学術講演会
    • Place of Presentation
      京大・原子炉
    • Related Report
      2016 Research-status Report
  • [Presentation] ヘリウムによるニッケル、鉄の引張特性への影響2016

    • Author(s)
      徐 ぎゅう
    • Organizer
      金属学会
    • Place of Presentation
      東京理科大学葛飾キャンパス(東京都葛飾区)
    • Year and Date
      2016-03-23
    • Related Report
      2015 Research-status Report
  • [Presentation] 原子力先進材料における高エネルギー粒子線の照射効果2016

    • Author(s)
      徐 ぎゅう
    • Organizer
      京都大学原子炉実験所第50回学術講演会
    • Place of Presentation
      京都大学原子炉実験所(大阪府熊取町)
    • Year and Date
      2016-01-27
    • Related Report
      2015 Research-status Report
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    • Author(s)
      佐藤 紘一、田宮 怜、徐 ぎゅう、土田 秀次、義家 敏正
    • Organizer
      京都大学原子炉実験所第50回学術講演会
    • Place of Presentation
      京都大学原子炉実験所(大阪府熊取町)
    • Year and Date
      2016-01-27
    • Related Report
      2015 Research-status Report
  • [Presentation] 鉄クロム合金の相分離に与える電子線照射の影響2016

    • Author(s)
      鬼塚 貴志、佐藤 紘一、徐 ぎゅう、福元 謙一
    • Organizer
      京都大学原子炉実験所第50回学術講演会
    • Place of Presentation
      京都大学原子炉実験所(大阪府熊取町)
    • Year and Date
      2016-01-27
    • Related Report
      2015 Research-status Report
  • [Presentation] FeAl 金属間化合物への電子線照射による欠陥生成のエネルギー依存性2016

    • Author(s)
      上野 陽平、小林 一基、石山 大志、谷 真海、大澤 一人、岩瀬 彰宏、徐 ぎゅう、佐藤 紘一、堀 史説
    • Organizer
      京都大学原子炉実験所第50回学術講演会
    • Place of Presentation
      京都大学原子炉実験所(大阪府熊取町)
    • Year and Date
      2016-01-27
    • Related Report
      2015 Research-status Report
  • [Remarks] 鉄の水素脆化防止の新しい手法を提案

    • URL

      http://www.rri.kyoto-u.ac.jp/archives/9903

    • Related Report
      2017 Annual Research Report

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Published: 2015-04-16   Modified: 2019-03-29  

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