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Fabrication of EBC film with eutectic structure

Research Project

Project/Area Number 15K06442
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Inorganic materials/Physical properties
Research InstitutionNihon University

Principal Investigator

UENO Shunkichi  日本大学, 工学部, 准教授 (60339801)

Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2017: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2016: ¥650,000 (Direct Cost: ¥500,000、Indirect Cost: ¥150,000)
Fiscal Year 2015: ¥3,640,000 (Direct Cost: ¥2,800,000、Indirect Cost: ¥840,000)
Keywords共晶 / 耐環境皮膜 / 集光加熱 / 凝固 / 酸化物共晶皮膜 / 耐水蒸気腐食 / 共晶皮膜 / Al2O3-HfO2共晶 / 一方向凝固 / 傾斜機能層
Outline of Final Research Achievements

In this project, the preparation method and the formation mechanism of oxide eutectic environmental barrier coating layer containing HfO2 as an edge member on the silicon carbide substrate are developed. In one model, Al2O3-HfO2 eutectic EBC film is prepared by optical zone melting method on the silicon carbide substrate. The components of Al2O3 also react with the free carbon and vaporized as AlO from the molten phase. HfO2 phase also reacts with the free carbon and HfC phase is formed on the silicon carbide substrate, then a high density intermediate layer is formed. The Al2O3-HfO2 eutectic structure grow from the top of the intermediate layer.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (41 results)

All 2018 2017 2016 2015

All Journal Article (9 results) (of which Int'l Joint Research: 3 results,  Peer Reviewed: 9 results,  Acknowledgement Compliant: 3 results) Presentation (30 results) (of which Int'l Joint Research: 6 results,  Invited: 6 results) Patent(Industrial Property Rights) (2 results)

  • [Journal Article] Yb2Si2O7-Al6Si2O13共晶組成ガラスの結晶化と組織形成2017

    • Author(s)
      菅野直登,張炳國,上野俊吉
    • Journal Title

      材料の科学と工学

      Volume: 54 Pages: 22-25

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] TiO2-SiO2融液の急冷固化により得られるTiO2ナノドット組織形成と熱安定性2017

    • Author(s)
      上野俊吉,山田将平,岩野寛,関野徹
    • Journal Title

      材料の科学と工学

      Volume: 54 Pages: 24-27

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Corrosion behavior of volcanic ash and calcium magnesium aluminosilicate on Yb2SiO5 environmental barrier coatings2017

    • Author(s)
      B.K. JANG, F.J. FENG, K. SUZUTA, H. TANAKA, Y. MATSUSHITA, K.S. LEE and S. UENO
    • Journal Title

      Journal of the Ceramic Society of Japan

      Volume: 125 Pages: 326-332

    • NAID

      130005530342

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 粒界ガラス相を含まない酸化物共晶系耐環境皮膜の創製プロセス2016

    • Author(s)
      上野俊吉,瀬谷恭佑,古川裕貴,西村聡之,張炳國
    • Journal Title

      材料の科学と工学

      Volume: 52 Pages: 30-33

    • NAID

      40020834096

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] 溶融-凝固法によるZrO2系共晶皮膜の作製と超高温域におけるSiC基材とZrO2の反応性2016

    • Author(s)
      古川裕貴,箭内哲也,瀬谷恭佑,張炳國,上野俊吉
    • Journal Title

      材料の科学と工学,

      Volume: 53 Pages: 159-162

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Consideration of Formation Mechanism of Al2O3-HfO2 Eutectic Film on SiC Substrate2016

    • Author(s)
      K. Seya, S. Ueno, T. Nishimura and B-K Jang
    • Journal Title

      Journal of the Korean Physical Society

      Volume: 68 Pages: 73-76

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] 集光加熱によるAl2O3-HfO2共晶組織を有する耐環境皮膜の作製2015

    • Author(s)
      瀬谷恭佑,張炳國,上野俊吉
    • Journal Title

      材料の科学と工学

      Volume: 51 Pages: 31-35

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] Microstructure Formation of Al2O3-HfO2 Eutectic2015

    • Author(s)
      K. Seya, B-K Jang and S. Ueno
    • Journal Title

      Journal of the Ceramic Society of Japan

      Volume: 123 Pages: 433-436

    • NAID

      130005068648

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] An Oxide Eutectic EBC for Silicon Carbide Ceramics2015

    • Author(s)
      K. Seya, S. Ueno and B-K Jang
    • Journal Title

      Journal of Nanomaterials

      Volume: 2015 Pages: 318278-318278

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Presentation] 遊星型ボールミルで調製したY2Si2O7-mullite共晶組成ナノ粒子の結晶化過程2018

    • Author(s)
      蔦木新也,上野俊吉
    • Organizer
      日本セラミックス協会2018年年会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Microstructure Formation of Oxide Composite by Crystallization, Phase Separation and Precipitation of Its Glass2017

    • Author(s)
      S. Ueno, N. Kanno, S. Yamada, H. Iwano, B.K. Jang, and T. Sekino
    • Organizer
      The 15th International Conference on Advanced Materials (IUMRS-ICAM 2017)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Thermo-Chemical Properties of Y2SiO5 Environmental Barrier Coatings2017

    • Author(s)
      B.K. Jang, N. Nagashima, S. Ueno, K.S.Lee and H.T. Kim
    • Organizer
      The 15th International Conference on Advanced Materials (IUMRS-ICAM 2017)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Ln2Si2O7-mullite(Ln=Y, La, Yb, Lu)共晶組成を有するガラスの結晶化2017

    • Author(s)
      菅野直登,上野俊吉
    • Organizer
      第60回日本大学工学部学術研究報告会
    • Related Report
      2017 Annual Research Report
  • [Presentation] ゾル-ゲル法により調製したRE2Si2O7-Al6Si2O13(RE=Y,Yb)共晶組成アモルファスの結晶化2017

    • Author(s)
      大島卓巳,上野俊吉
    • Organizer
      第60回日本大学工学部学術研究報告会
    • Related Report
      2017 Annual Research Report
  • [Presentation] CMAS融液の高温挙動およびムライト相の溶解性2017

    • Author(s)
      富田悠志,上野俊吉
    • Organizer
      第60回日本大学工学部学術研究報告会
    • Related Report
      2017 Annual Research Report
  • [Presentation] ゾル-ゲル法により調製したY2Si2O7-mullite共晶組成ガラスの結晶化と溶融挙動2017

    • Author(s)
      大島卓巳,菅野貴裕,上野俊吉
    • Organizer
      平成29年度 日本セラミックス協会東北北海道支部研究発表会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 溶融-固化により調製したLn2Si2O7-mullite(Ln=希土類)共晶組成ガラスの組織形成と皮膜への応用2017

    • Author(s)
      菅野直登,會澤耕平,鈴木洋平,上野俊吉
    • Organizer
      平成29年度 日本セラミックス協会東北北海道支部研究発表会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Yb2Si2O7-Al6Si2O13共晶組成ガラスの熱安定性2017

    • Author(s)
      菅野直登,上野俊吉
    • Organizer
      2017年度 日本セラミックス協会東北北海道支部郡山地区セミナー
    • Related Report
      2017 Annual Research Report
  • [Presentation] Y2Si2O7-SiC複合材料の酸化挙動2017

    • Author(s)
      箭内哲也,上野俊吉
    • Organizer
      2017年度 日本セラミックス協会東北北海道支部郡山地区セミナー
    • Related Report
      2017 Annual Research Report
  • [Presentation] ムライト相のCMAS腐食挙動2017

    • Author(s)
      富田悠志,大島卓己,魚住知加,佐藤和也,上野俊吉
    • Organizer
      2017年度 日本セラミックス協会東北北海道支部郡山地区セミナー
    • Related Report
      2017 Annual Research Report
  • [Presentation] ゾル-ゲル法で調製したAl2O3-YAG組成アモルファスの結晶化挙動2017

    • Author(s)
      瀬藤兼太,大島卓巳,上野俊吉
    • Organizer
      2017年度 日本セラミックス協会東北北海道支部郡山地区セミナー,
    • Related Report
      2017 Annual Research Report
  • [Presentation] 遊星ボールミルで調製したY2Si2O7-mullite共晶組成ナノ粒子の結晶化過程2017

    • Author(s)
      蔦木新也,上野俊吉
    • Organizer
      2017年度 日本セラミックス協会東北北海道支部郡山地区セミナー,
    • Related Report
      2017 Annual Research Report
  • [Presentation] ゾル-ゲル法により調製したLn2Si2O7-Al6Si2O13共晶組成ガラスの結晶化2017

    • Author(s)
      大島卓巳,菅野貴裕,上野俊吉
    • Organizer
      2017年度 日本セラミックス協会東北北海道支部郡山地区セミナー
    • Related Report
      2017 Annual Research Report
  • [Presentation] La2Si2O7- Al6Si2O13共晶組成を有するガラスの結晶化2017

    • Author(s)
      菅野直登,會澤耕平,上野俊吉
    • Organizer
      日本材料科学会第24回若手研究者討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] ムライトセラミックスのCMAS腐食2017

    • Author(s)
      富田悠志,佐藤和也,上野俊吉,張炳國
    • Organizer
      日本材料科学会第24回若手研究者討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Yb2Si2O7-Al6Si2O13共晶組成ガラスの結晶化と組織形成2017

    • Author(s)
      菅野直登,張炳國,上野俊吉
    • Organizer
      日本材料科学会平成29年度学術講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] ゾル-ゲル法により調製したY2Si2O7-Al6Si2O13共晶組成ガラスの結晶化2017

    • Author(s)
      大島卓巳,鈴木洋平,上野俊吉
    • Organizer
      日本材料科学会平成29年度学術講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Ln2Si2O7(Ln=希土類)-mullite共晶組成を有するガラスの溶融凝固による共晶構造の形成2017

    • Author(s)
      菅野直登,鈴木洋平,居城菜々美,上野俊吉
    • Organizer
      日本セラミックス協会2017年年会
    • Related Report
      2017 Annual Research Report
  • [Presentation] ゾル‐ゲル法により調製したCaZrO3-ZrO2(CaO)共晶組成物の結晶化2017

    • Author(s)
      大島卓巳,仙波友貴,上野俊吉
    • Organizer
      日本セラミックス協会2017年年会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Al2O3-ZrO2共晶皮膜の作製と問題点2016

    • Author(s)
      古川裕貴,箭内哲也,瀬谷恭佑,上野俊吉,張炳國
    • Organizer
      日本材料科学会平成28年度学術講演会
    • Place of Presentation
      産業技術総合研究所(東京)
    • Related Report
      2016 Research-status Report
    • Invited
  • [Presentation] Fabrication of Oxide Eutectic EBC Layer without Boundary Glassy phase2015

    • Author(s)
      S. Ueno, K. Seya, N. Ishiro and B-K. Jang
    • Organizer
      The 32nd International Japan-Korea Seminar on Ceramics
    • Place of Presentation
      Nagaoka, Japan
    • Year and Date
      2015-11-18
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Al2O3‐HfO2共晶構造を有する耐環境皮膜の形成メカニズム2015

    • Author(s)
      瀬谷恭佑,張炳國,上野俊吉
    • Organizer
      平成27年度日本セラミックス協会東北北海道支部発表研究会
    • Place of Presentation
      米沢市市民文化会館
    • Year and Date
      2015-10-16
    • Related Report
      2015 Research-status Report
  • [Presentation] 高温における還元反応を利用した共晶系耐環境皮膜の作製2015

    • Author(s)
      古川裕貴, 瀬谷恭佑, 張炳國, 上野俊吉
    • Organizer
      平成27年度日本セラミックス協会東北北海道支部郡山地区セミナー
    • Place of Presentation
      日本大学
    • Year and Date
      2015-10-03
    • Related Report
      2015 Research-status Report
  • [Presentation] 集光加熱法による共晶系多層皮膜の作製2015

    • Author(s)
      瀬谷恭佑, 張炳國, 上野俊吉
    • Organizer
      平成27年度日本セラミックス協会東北北海道支部郡山地区セミナー
    • Place of Presentation
      郡山
    • Year and Date
      2015-10-03
    • Related Report
      2015 Research-status Report
  • [Presentation] Formation of Multi-layered EBC with Oxides Eutectic Structure by Solidification Process at High Temperature2015

    • Author(s)
      S. Ueno, K. Seya, Y. Furukawa and B-K. Jang
    • Organizer
      11th Pacific Rim Conference of Ceramics Societies
    • Place of Presentation
      Jeju, Korea
    • Year and Date
      2015-08-31
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Development of EBC with oxide Eutectic Structure Layer2015

    • Author(s)
      Shunkichi Ueno, Kyosuke Seya and Byung-Koog Jang
    • Organizer
      Japan-Korea International Symposium on Materials Science and Technology 2015
    • Place of Presentation
      Tokyo, Japan
    • Year and Date
      2015-08-26
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] 皮膜組成物の高温反応を利用した耐環境皮膜の作製に関する問題点2015

    • Author(s)
      古川裕貴,瀬谷恭佑,上野俊吉,張炳國
    • Organizer
      日本材料科学会第22回若手研究者討論会
    • Place of Presentation
      日本大学
    • Year and Date
      2015-08-26
    • Related Report
      2015 Research-status Report
  • [Presentation] A New EBC System for Silicon Carbide Ceramics with Al2O3/HfO2 Eutectic Structure Layer2015

    • Author(s)
      S. Ueno and K. Seya
    • Organizer
      11th International Conference on Ceramic Materials and Components for Energy and Environmental Applications
    • Place of Presentation
      Vancouver, Canada.
    • Year and Date
      2015-06-14
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Al2O3-HfO2共晶系耐環境皮膜の作製2015

    • Author(s)
      瀬谷恭佑,張炳國,上野俊吉
    • Organizer
      日本材料科学会平成27年度学術講演会
    • Place of Presentation
      工学院大学
    • Year and Date
      2015-06-05
    • Related Report
      2015 Research-status Report
  • [Patent(Industrial Property Rights)] 耐熱耐食皮膜、耐熱耐食部材及び耐熱耐食皮膜の製造方法2017

    • Inventor(s)
      上野俊吉, 菅野直登, 中村康介
    • Industrial Property Rights Holder
      上野俊吉, 菅野直登, 中村康介
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2017-143689
    • Filing Date
      2017
    • Related Report
      2017 Annual Research Report
  • [Patent(Industrial Property Rights)] 耐水蒸気腐食性多層皮膜、およびその製造方法2015

    • Inventor(s)
      上野俊吉, 瀬谷恭佑, 古川裕貴
    • Industrial Property Rights Holder
      上野俊吉, 瀬谷恭佑, 古川裕貴
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2014-200781
    • Filing Date
      2015-09-30
    • Related Report
      2015 Research-status Report

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Published: 2015-04-16   Modified: 2019-03-29  

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