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Development of high-coercivity nanocrystalline NeFeB films deposited by Supersonic Free-Jet PVD

Research Project

Project/Area Number 15K06512
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Material processing/Microstructural control engineering
Research InstitutionShibaura Institute of Technology

Principal Investigator

YUMOTO Atsushi  芝浦工業大学, 工学部, 教授 (20383987)

Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2017: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2016: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2015: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywordsナノ結晶永久磁石 / 保磁力 / 最大エネルギ積 / 成膜速度
Outline of Final Research Achievements

Nd-Fe-B based magnets show the highest maximum energy product among all the permanent magnets. In this work, NdFeB thick films were prepared on substrates by supersonic free-jet physical vapor deposition (SFJ-PVD). The SFJ-PVD has been developed as a new coating method in which a coating film is formed by the deposition of nanoparticles onto a substrate at very high velocity. The SFJ-PVD can deposit almost all the evaporated source material as nanoparticles and produce thick coating film.
Using SFJ-PVD technique, we obtain a uniform high-density NdFeB films. Thickness up to 165 μm of NdFeB films have a poly-nanocrystalline structure with a grain size of 5-30 nm. Coercivities up to 154 kA/m and saturation magnetization of about 50 emu/g were achieved.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (11 results)

All 2018 2017 2016 2015

All Presentation (6 results) (of which Int'l Joint Research: 2 results,  Invited: 3 results) Book (1 results) Patent(Industrial Property Rights) (4 results) (of which Overseas: 1 results)

  • [Presentation] 超音速フリージェットPVDによるナノ結晶厚膜の開発2018

    • Author(s)
      湯本敦史
    • Organizer
      表面技術協会第137回講演大会
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] 熱処理によるNd-Cuキャップ層のNd-Fe-B厚膜への影響2018

    • Author(s)
      田中勇音,湯本敦史
    • Organizer
      表面技術協会第137回講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] ナノ結晶厚膜形成技術としての超音速フリージェットPVDの開発2017

    • Author(s)
      湯本敦史
    • Organizer
      大阪大学接合科学研究所第5回溶射・造形研究集会
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] 新規厚膜形成技術超音速フリージェットPVD2017

    • Author(s)
      湯本敦史
    • Organizer
      日本学術会議若手アカデミー若手科学者ネットワーク分科会第2回若手科学者サミット
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] Understanding of low temperature fabrication process of oxide thin films in eximer laser-assisted metal organic deposition2016

    • Author(s)
      Kentaro Shinoda, Tsukasa Katsuki, Tomohiko Nakajima, Tetsuo Tsuchiya,and Atsushi Yumoto
    • Organizer
      40th International Conference and Expo on Advanced Ceramics and Composites
    • Place of Presentation
      Florida USA
    • Year and Date
      2016-01-24
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] Ultrafast radiation thermometry for monitoring fabrication process of oxide thin films in excimer laser-assisted metal organic deposition2015

    • Author(s)
      Kentaro Shinoda, Tsukasa Katsuki, Atsushi Yumoto, Tomohiko Nakajima and Tetsuo Tsuchiya
    • Organizer
      11th International Conference on Ceramic Materials and Components for Energy and Environmental Applications
    • Place of Presentation
      Canada
    • Year and Date
      2015-06-14
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Book] 溶射工学便覧(改訂版)2017

    • Author(s)
      沖幸男,上野和夫監修(分担湯本敦史)
    • Total Pages
      984
    • Publisher
      一般社団法人日本溶射学会
    • ISBN
      9784990312732
    • Related Report
      2017 Annual Research Report
  • [Patent(Industrial Property Rights)] 超音速フリージェット物理蒸着装置で用いる超音速ノズル,超音速フリージェット物理蒸着装置で用いる超音速ノズルの製造方法,2017

    • Inventor(s)
      湯本敦史
    • Industrial Property Rights Holder
      学校法人芝浦工業大学
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2017-036799
    • Filing Date
      2017
    • Related Report
      2017 Annual Research Report
  • [Patent(Industrial Property Rights)] 窒化アルミニウム膜,窒化アルミニウム膜の製造方法,および高耐電圧部品2016

    • Inventor(s)
      湯本敦史,清水麻里,井上哲夫,日野高志,齋藤秀一
    • Industrial Property Rights Holder
      学校法人芝浦工業大学,東芝マテリアル株式会社
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2016-044525
    • Filing Date
      2016-03-28
    • Related Report
      2015 Research-status Report
  • [Patent(Industrial Property Rights)] 酸化鉄系強磁性膜及び酸化鉄系強磁性膜の製造方法2016

    • Inventor(s)
      大越慎一,湯本敦史,生井飛鳥,吉清まりえ,安部史也,政広泰
    • Industrial Property Rights Holder
      東京大学,芝浦工業大学,田中貴金属工業株式会社
    • Industrial Property Rights Type
      特許
    • Filing Date
      2016-01-28
    • Related Report
      2015 Research-status Report
    • Overseas
  • [Patent(Industrial Property Rights)] 軟磁性金属および磁性部品2015

    • Inventor(s)
      湯本敦史,山本将大,井上哲夫,日野高志,齋藤秀一
    • Industrial Property Rights Holder
      学校法人芝浦工業大学,東芝マテリアル株式会社
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2015-221038
    • Filing Date
      2015-11-11
    • Related Report
      2015 Research-status Report

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Published: 2015-04-16   Modified: 2019-03-29  

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