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Structural analysis of ABRZ formation at the resin-enamel interface

Research Project

Project/Area Number 15K11105
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Conservative dentistry
Research InstitutionTokyo Medical and Dental University

Principal Investigator

NIKAIDO Toru  東京医科歯科大学, 大学院医歯学総合研究科, 講師 (00251538)

Co-Investigator(Kenkyū-buntansha) 井上 剛  東京医科歯科大学, 大学院医歯学総合研究科, 助教 (40431928)
高垣 智博  東京医科歯科大学, 大学院医歯学総合研究科, 助教 (60516300)
Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,680,000 (Direct Cost: ¥3,600,000、Indirect Cost: ¥1,080,000)
Fiscal Year 2017: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2016: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2015: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Keywordsエナメル質 / ABRZ / 接着 / セルフエッチング接着システム / リン酸エッチング / 電子顕微鏡 / 接着試験 / セルフエッチングシステム / 歯質接着 / エナメル質ABRZ / 機能性モノマー / 化学結合 / フッ素徐放
Outline of Final Research Achievements

A self-etching primer is much milder than phosphoric acid, which is concerned in enamel bonding. The purpose of this study was to evaluate the acid-base resistant zone (ABRZ) at the adhesive/enamel interface of self-etching adhesives with/without prior phosphoric acid etching. After application of self-etching adhesives on enamel surfaces, a flowable composite was placed. For observation of the acid-base resistant zone (ABRZ), the bonded interface was subjected to the acid-base challenge, morphological attributes of the interface were observed using SEM. ABRZ formation was confirmed in all groups, however, the morphology of the ABRZ was adhesive material dependent. The funnel-shaped erosion beneath the interface was present in one-step self-etch adhesives. With phosphoric acid etching, the ABRZs were obviously thicker compared with no phosphoric acid etching. In the case of the one-step self-etching adhesives, enamel etching should be recommended to improve the interfacial quality.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (14 results)

All 2017 2016 2015 Other

All Int'l Joint Research (2 results) Journal Article (3 results) (of which Int'l Joint Research: 3 results,  Peer Reviewed: 3 results,  Open Access: 2 results,  Acknowledgement Compliant: 2 results) Presentation (9 results) (of which Int'l Joint Research: 3 results,  Invited: 2 results)

  • [Int'l Joint Research] 香港大学歯学部(香港)

    • Related Report
      2017 Annual Research Report
  • [Int'l Joint Research] ワシントン大学歯学部(米国)

    • Related Report
      2017 Annual Research Report
  • [Journal Article] Effects of experimental pastes containing surface pre-reacted glass ionomer fillers on inhibition of enamel demineralization2017

    • Author(s)
      Nakamura K, Hamba H, Nakashima S, Sadr A, Nikaido T, Oikawa M, Uo M, Tagami J.
    • Journal Title

      Dental Materials Journal

      Volume: 36 Issue: 4 Pages: 482-490

    • DOI

      10.4012/dmj.2016-303

    • NAID

      130005865133

    • ISSN
      0287-4547, 1881-1361
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Morphological evaluation of adhesive-enamel interface with 2-step self-etching adhesive and multi-mode one-bottle self-etching adhesives.2016

    • Author(s)
      Sato T, Takagaki T, Matsui N, Hamba H, Sadr A, Nikaido T, Tagami J.
    • Journal Title

      J Adhes Dent

      Volume: 18 Pages: 223-229

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] Adsorption Behavior of Methacryloyloxy Decyldihydrogen Phosphate on an Apatite Surface at Neutral pH.2016

    • Author(s)
      1.Bista B. Nakashima S, Nikaido T, Sadr Ali, Takagaki T, Maja Romero, Sato Takaaki, J Tagami.
    • Journal Title

      Eur J Oral Sci.

      Volume: 124 Issue: 2 Pages: 195-203

    • DOI

      10.1111/eos.12254

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Int'l Joint Research / Acknowledgement Compliant
  • [Presentation] Evaluation of the enamel/bond interfaces of multi-mode one-bottle self-etching adhesives2017

    • Author(s)
      Sato T, Takagaki T, Guan R, Nikaido T, Tagami J
    • Organizer
      Brazil-Japan Joint Research Workshop on Adhesive Dentistry
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Acid-Base Resistant Zone (ABRZ) - New concept of adhesive-tooth interface2017

    • Author(s)
      Toru Nikaido
    • Organizer
      Taiwan Academy of Operative Dentistry
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Assessment of adhesive materials for direct composite restorations2017

    • Author(s)
      Nikaido T
    • Organizer
      Brazil-Japan Joint Research Workshop on Adhesive Dentistry
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Office Bleachingがエナメル質接着強さに及ぼす影響2017

    • Author(s)
      スマヤ ハラビ、松井七生子、二階堂徹、田上順次
    • Organizer
      日本歯科保存学会2017年度春季学術大会(146回)
    • Related Report
      2017 Annual Research Report
  • [Presentation] 接着性レジンセメント-エナメル質界面におけるAcid-Base Resistant Zoneの観察.2017

    • Author(s)
      熊谷 薬師神 ローゼ,高垣智博,佐藤隆明,二階堂徹,Rodrigues JA,Reis AF,田上順次
    • Organizer
      日本歯科保存学会2017年度春季学術大会(146回)
    • Related Report
      2017 Annual Research Report
  • [Presentation] 2ステップセルフエッチシステムにおけるボンド中のMDP、NaFがエナメル質接着性能に及ぼす影響2016

    • Author(s)
      柿内裕輔、髙垣智博、池田正臣、佐藤隆明、松井七生子、二階堂徹、田上順次
    • Organizer
      日本歯科保存学会2015年度秋季学術大会(145回)
    • Place of Presentation
      キッセイ文化ホール(松本)
    • Year and Date
      2016-10-27
    • Related Report
      2016 Research-status Report
  • [Presentation] 新規ワンステップセルフエッチングシステムとエナメル質との接着界面におけるABRZ形態の観察2016

    • Author(s)
      佐藤隆明,高垣智博,二階堂徹,田上順次.
    • Organizer
      第35回日本接着歯学会学術大会
    • Place of Presentation
      北海道大学学術交流会館(札幌)
    • Related Report
      2016 Research-status Report
  • [Presentation] ボンド中の機能性モノマー濃度が象牙質浸透性へ及ぼす影響。2015

    • Author(s)
      松井七生子、高垣智博、徐知勲、二階堂徹、由井伸彦、田上順次.
    • Organizer
      日本歯科保存学会2015年度春季学術大会(142回)
    • Place of Presentation
      北九州国際会議場(福岡県)
    • Year and Date
      2015-06-25
    • Related Report
      2015 Research-status Report
  • [Presentation] フッ化物洗口剤がウシ歯根面象牙質の接着に及ぼす影響について2015

    • Author(s)
      中元絢子,佐藤隆明,松井七生子,池田正臣,二階堂徹,宇尾基弘,田上順次
    • Organizer
      日本歯科保存学会2015年度春季学術大会(142回)
    • Place of Presentation
      北九州国際会議場(福岡県)
    • Year and Date
      2015-06-25
    • Related Report
      2015 Research-status Report

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Published: 2015-04-16   Modified: 2022-08-18  

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