• Search Research Projects
  • Search Researchers
  • How to Use
  1. Back to previous page

New zirconia by silicon sputter- Invention of resin cement adhesion system

Research Project

Project/Area Number 15K11180
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Prosthodontics/ Dental materials science and
Research InstitutionAsahi University

Principal Investigator

Mitsunori Uno  朝日大学, 歯学部, 講師 (10298424)

Co-Investigator(Kenkyū-buntansha) 川木 晴美  朝日大学, 歯学部, 准教授 (70513670)
土井 豊  朝日大学, 歯学部, 名誉教授 (40116067)
石神 元  朝日大学, 歯学部, 教授 (20168214)
岡 俊男  朝日大学, 歯学部, 准教授 (30185409)
横川 善之  大阪市立大学, 大学院工学研究科, 教授 (20358310)
玉置 幸道  朝日大学, 歯学部, 教授 (80197566)
Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
Fiscal Year 2017: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2016: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2015: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywordsジルコニア / RFマグネトロンスパッタリング / 圧縮せん断接着強さ / 親水性 / シリコン注入 / 接着
Outline of Final Research Achievements

In this study, we made a Si-O coating on the surface of zirconia by RF magnetron sputtering.The Si-O coating on the zirconia surface became superhydrophilic. The contact angle after 21 days on the zirconia surface was 40°or less.Then the specimens were treated with P primer. Cylinder shaped composite resin specimens were prepared, and the following surface treatments for the composite resin core specimens were used porcelain primer. These resin specimens were bonded to the zirconia specimens with resin cement, fixed to universal testing machine, and bond strength was evaluated. Compressive shear bond strength was significantly larger after sputtering (30.86MPa) than no sputtering (9.26MPa).Si sputtering to zirconia took place under the condition of an oxygen volume concentration of 5%. It formed a Si-O coating on the surface of the zirconia. The coating made the surface of the zirconia hydrophilic which enabled chemical bonding with the silane coupling agent.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (5 results)

All 2017 2016

All Presentation (4 results) Patent(Industrial Property Rights) (1 results)

  • [Presentation] シリコンスパッタリングがジルコニアとレジンコア材の接着性におよぼす影響2017

    • Author(s)
      宇野光乗, 川木晴美, 本多 歩,野々垣龍吾,澤田季子,西川元典,倉知正和,石神 元,横川 善之,土井 豊
    • Organizer
      日本歯科理工学会平成29年度春期第69回学術講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Effect of surface treatment on the bond strength between zirconia ceramic and core resin2016

    • Author(s)
      Uno M, Kawaki H, Nonogaki R, Sawada T, Nishikawa M, Kurachi M,Ishigami H, and Doi Y
    • Organizer
      International Dental Materials Congress2016
    • Place of Presentation
      The Stone Hotel-Legian Bali, Legian, Bali, Indonesia
    • Year and Date
      2016-11-04
    • Related Report
      2016 Research-status Report
  • [Presentation] ジルコニアとレジン築造体の接着における表面処理の効果2016

    • Author(s)
      宇野光乗, 川木晴美, 土井 豊, 倉知正和,石神 元
    • Organizer
      日本歯科理工学会平成28年度春期第67回学術講演会
    • Place of Presentation
      九州大学医学部百年講堂
    • Year and Date
      2016-04-16
    • Related Report
      2016 Research-status Report
  • [Presentation] ジルコニアとレジン築造体の接着における表面処理の効果2016

    • Author(s)
      宇野光乗,川木晴美,土井 豊, 倉知正和,石神 元
    • Organizer
      日本歯科理工学会
    • Place of Presentation
      九州大学医学部 百年講堂
    • Year and Date
      2016-04-16
    • Related Report
      2015 Research-status Report
  • [Patent(Industrial Property Rights)] ジルコニア焼結体2016

    • Inventor(s)
      横川善之
    • Industrial Property Rights Holder
      公立大学法人大阪市立大学
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2016-233814
    • Filing Date
      2016-12-01
    • Related Report
      2016 Research-status Report

URL: 

Published: 2015-04-16   Modified: 2019-03-29  

Information User Guide FAQ News Terms of Use Attribution of KAKENHI

Powered by NII kakenhi