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Multiscale microstructral analysis of functional materials by TEM

Research Project

Project/Area Number 15K13306
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Nanomaterials engineering
Research InstitutionOsaka Prefecture University

Principal Investigator

MORI SHIGEO  大阪府立大学, 工学(系)研究科(研究院), 教授 (20251613)

Research Collaborator HARADA Ken  理化学研究所, 上席研究員
Project Period (FY) 2015-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2016: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2015: ¥2,340,000 (Direct Cost: ¥1,800,000、Indirect Cost: ¥540,000)
Keywords微細構造解析 / 電子回折 / ローレンツTEM / 透過型電子顕微鏡 / 機能性材料 / 微細構造観察 / ローレンツ顕微鏡 / 磁気的微細構造
Outline of Final Research Achievements

A method of electron diffraction with the objective lens turned off is developed by using three intermediate lenses as compound lenses. A crossover which is adjusted on the selected-are aperture plane is projected on the fluorescent with the compound lenses using a camera length from 0.8 to 4.5 m. Magnetic dependence of electron diffraction patterns is able to be observed in the electron optical system with the objective lens under weak excitation condition. The optical system is switched to a small-angle electron diffraction mode without changing the illumination system. Electron diffraction as a function of a magnetic field as well as small-angle electron diffraction and a dark-field image is obtained to observe magnetic domain structures in hexaferrites using the developed method.

Report

(3 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • Research Products

    (13 results)

All 2017 2016 2015 Other

All Journal Article (4 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 4 results,  Acknowledgement Compliant: 4 results,  Open Access: 1 results) Presentation (8 results) (of which Int'l Joint Research: 5 results,  Invited: 1 results) Remarks (1 results)

  • [Journal Article] Field-temperature phase diagram of magnetic bubbles spanning charge/orbital ordered and metallic phases in La1-xSrxMnO3 (x = 0.125)2017

    • Author(s)
      A. Kotani, H. Nakajima, K. Harada, Y. Ishii and S. Mori
    • Journal Title

      Physical Review B

      Volume: 95 Pages: 1444031-6

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Lorentz microscopy and small-angle electron diffraction study of magnetic textures in La1-xSrxMnO3 (0.15<x<0.30): The role of magnetic anisotropy2016

    • Author(s)
      A. Kotani, H. Nakajima, K. Harada, Y. Ishii and S. Mori
    • Journal Title

      Physical Review B

      Volume: 024407 Pages: 024407-024407

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Foucault imaging and small-angle electron diffraction in controlled external magnetic fields2016

    • Author(s)
      H. Nakajima, A. Kotani, K. Harada, Y. Ishii, and S. Mori
    • Journal Title

      Microscopy

      Volume: 65 Pages: 473-473

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Observation of spin textures in La1-xSrxMnO3 (x=0.175)2016

    • Author(s)
      A.Kotani, H. Nakajima, Y. Ishii, K. Harada and S. Mori
    • Journal Title

      AIP Advances

      Volume: 6 Issue: 5 Pages: 056403-056403

    • DOI

      10.1063/1.4943611

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Int'l Joint Research / Acknowledgement Compliant
  • [Presentation] Formation of Magnetic Textures in the Ferromagnetic Phase of La0.825Sr0.175MnO3.2016

    • Author(s)
      A. Kotani, H. Nakajima, K. Harada, Y. Ishii and S. Mori
    • Organizer
      Microscopy & Microanalysis 2016 Meeting,
    • Place of Presentation
      米国・オハイオ
    • Year and Date
      2016-07-24
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Observation of spin textures in manganites2016

    • Author(s)
      A. Kotani, H. Nakajima, Y. Ishii, K. Harada and S. Mori
    • Organizer
      日本顕微鏡学会第72回学術講演会
    • Place of Presentation
      仙台
    • Year and Date
      2016-06-14
    • Related Report
      2016 Annual Research Report
  • [Presentation] 間接型強誘電体(Ca,Sr)3Ti2O7の電荷ドメイン壁の局所構造解析2016

    • Author(s)
      久留島康輔、吉本航、塚崎裕文、石井悠衣、森茂生
    • Organizer
      日本顕微鏡学会第72回学術講演会
    • Place of Presentation
      仙台
    • Year and Date
      2016-06-14
    • Related Report
      2016 Annual Research Report
  • [Presentation] 透過型電子顕微鏡によるLi2S-P2S5系ガラス電解質の結晶化挙動の評価2016

    • Author(s)
      塚崎裕文、森要太、杉中優介、森茂生、林晃敏、辰巳砂昌弘
    • Organizer
      日本顕微鏡学会第72回学術講演会
    • Place of Presentation
      仙台
    • Year and Date
      2016-06-14
    • Related Report
      2016 Annual Research Report
  • [Presentation] Observation of spin textures in manganites2016

    • Author(s)
      Atsuhiro Kotani, HiroshiNakajima, Yui Ishii, Ken Harada, Shigeo Mori
    • Organizer
      13th Joint MMM-Intermag Conference
    • Place of Presentation
      the Hilton San Diego Bayfront in San Diego, California USA
    • Year and Date
      2016-01-11
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] Microstructures in Improper Ferroelectric Compounds Revealed by Electron Microscopy2015

    • Author(s)
      S. Mori, H. Tsukasaki, Y. Ishii, K. Kurushima
    • Organizer
      The 2rd East-Asia Microscopy Conference
    • Place of Presentation
      The Himeji Chamber of Commerce and Industry (HCCI) 兵庫県姫路市
    • Year and Date
      2015-11-24
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Lorentz TEM Observation of Magnetic Bubbles in Manganites2015

    • Author(s)
      A. Kotani1, H. Nakajima, K. Harada, Y. Ishii, S. Mori
    • Organizer
      The 2rd East-Asia Microscopy Conference
    • Place of Presentation
      The Himeji Chamber of Commerce and Industry (HCCI) 兵庫県姫路市
    • Year and Date
      2015-11-24
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] Simultaneous Realization of Foucault Imaging and Small Angle Electron Diffraction by Conventional TEM2015

    • Author(s)
      Hiroshi Nakajima, Atsuhiro Kotani, Yui Ishii,Ken Harada, Shigeo Mori
    • Organizer
      The 2rd East-Asia Microscopy Conference
    • Place of Presentation
      The Himeji Chamber of Commerce and Industry (HCCI) 兵庫県姫路市
    • Year and Date
      2015-11-24
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Remarks]

    • URL

      http://mori-lab.mtr.osakafu-u.ac.jp/

    • Related Report
      2016 Annual Research Report

URL: 

Published: 2015-04-16   Modified: 2018-03-22  

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