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Multi-dimensional single crystal formation by pulsed laser melting in liquid

Research Project

Project/Area Number 15K14141
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Composite materials/Surface and interface engineering
Research InstitutionTohoku University

Principal Investigator

Nakamura Takahiro  東北大学, 多元物質科学研究所, 准教授 (50400429)

Co-Investigator(Kenkyū-buntansha) 越崎 直人  北海道大学, 工学研究院, 教授 (40344197)
Project Period (FY) 2015-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2016: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Fiscal Year 2015: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Keywordsパルスレーザー溶融法 / 電子後方散乱回折 / サブミクロン球状粒子 / バルク金属ガラス / 再結晶化 / 液中レーザー溶融法 / レーザープロセッシング / 表面処理 / 組織観察 / 球状粒子
Outline of Final Research Achievements

Pulsed laser melting in liquid (PLML) is a novel technique to produce submicron spherical particles (SSPs) of various materials. In the process, SSPs is formed by irradiation of laser pulses into a colloidal dispersion. Inner structure of Ag SSPs was evaluated by electron backscattering diffraction (EBSD) using a bulk metallic glass with no EBSD as a substrate for the measurement. Local structure of silver SSPs is crystalline although the feature of SSPs is totally spherical. It is considered that this fascinating materials are produced through nonlinear melting and cooling processes. It was assumed that multidimensional single crystal bulk materials could be formed from those of polycrystal by applying PLML. However no effects were confirmed in the process. Accordingly, it is considered that small crystalline size of raw materials is important for the recrystallization through PLML.

Report

(3 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • Research Products

    (6 results)

All 2016 2015

All Presentation (5 results) (of which Int'l Joint Research: 1 results) Patent(Industrial Property Rights) (1 results)

  • [Presentation] 後方散乱電子回折法による銀サブミクロン球状粒子の内部構造解析とその形成メカニズム2016

    • Author(s)
      中村 貴宏,真柄 英之,榊 祥太,越崎 直人,佐藤 俊一
    • Organizer
      日本金属学会2016年秋季(第159回)大会
    • Place of Presentation
      大阪大学豊中キャンパス(大阪府豊中市)
    • Year and Date
      2016-09-21
    • Related Report
      2016 Annual Research Report
  • [Presentation] 液中レーザー溶融法で作製した銀サブミクロン球状粒子の内部構造解析とその形成メカニズム2016

    • Author(s)
      中村 貴宏,真柄 英之,榊 祥太,越崎 直人,佐藤 俊一
    • Organizer
      日本セラミックス協会 第29回秋季シンポジウム
    • Place of Presentation
      広島大学東広島キャンパス (広島県東広島市)
    • Year and Date
      2016-09-07
    • Related Report
      2016 Annual Research Report
  • [Presentation] Inner structural analysis of silver submicron spherical particles fabricated by pulsed laser melting in liquid2016

    • Author(s)
      Takahiro Nakamura, Hideyuki Magara, Shota Sakaki, Naoto Koshizaki, Shunichi Sato
    • Organizer
      4th Conference on Advanced Nanoparticle Generation and Excitation by Lasers in Liquids (ANGEL)
    • Place of Presentation
      Germany (Essen)
    • Year and Date
      2016-05-09
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 液中レーザー溶融法により作製した銀サブミクロン球状粒子の内部構造と照射時間による影響2016

    • Author(s)
      中村貴宏,真柄英之,榊祥太,越崎直人,佐藤俊一
    • Organizer
      第63回応用物理学会春季学術講演会
    • Place of Presentation
      東京工業大学大岡山キャンパス(目黒区)
    • Year and Date
      2016-03-11
    • Related Report
      2015 Research-status Report
  • [Presentation] 液中レーザー溶融法で作製した銀サブミクロン球状粒子の内部構造2015

    • Author(s)
      中村貴宏,真柄英之,榊祥太,越崎直人,佐藤俊一
    • Organizer
      第76回応用物理学会秋季学術講演会
    • Place of Presentation
      名古屋国際会議場(名古屋市)
    • Year and Date
      2015-09-13
    • Related Report
      2015 Research-status Report
  • [Patent(Industrial Property Rights)] 非晶質合金基板を用いた微小金属粒子の結晶構造解析方法2016

    • Inventor(s)
      中村貴宏,真柄英之,福田奉行,真壁英一
    • Industrial Property Rights Holder
      中村貴宏,真柄英之,福田奉行,真壁英一
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2016-038421
    • Filing Date
      2016-03-15
    • Related Report
      2015 Research-status Report

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Published: 2015-04-16   Modified: 2018-03-22  

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