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Development of in-situ XAFS technique for the flow-type reactor and its application to hydrothermal synthesis of metal oxide nanoparticles

Research Project

Project/Area Number 15K14212
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Reaction engineering/Process system
Research InstitutionTohoku University

Principal Investigator

Takami Seiichi  東北大学, 多元物質科学研究所, 准教授 (40311550)

Co-Investigator(Kenkyū-buntansha) 沼子 千弥  千葉大学, 大学院理学研究科, 准教授 (80284280)
佐藤 和好  群馬大学, 大学院理工学府, 助教 (40437299)
Project Period (FY) 2015-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2016: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2015: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Keywords水熱合成 / 反応速度 / ナノ粒子 / 金属酸化物 / in situ XAFS / 高温高圧 / 流通式装置 / 表面修飾
Outline of Final Research Achievements

In order to study reaction process and reaction rate of metal ion in water during hydrothermal synthesis using a flow-type reactor, X-ray absorption fine edge structure (XAFS) was measured with the high temperature XAFS cell developed in this study. The results showed that the XAFS cell can be used to measure XAFS spectra of liquid reactants at high temperature and high pressure. However, a part of the produced metal oxides deposited on the windows of the XAFS cell. Therefore, different type of XAFS cell without stagnant flow was proposed to realize in-situ XAFS measurement using flow-type configuration.

Report

(3 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • Research Products

    (3 results)

All 2016

All Presentation (3 results) (of which Invited: 3 results)

  • [Presentation] 有機分子修飾酸化物ナノ粒子の合成と高熱伝導コンポジット材料への応用2016

    • Author(s)
      高見誠一
    • Organizer
      北関東地区化学技術懇話会 「次世代熱マネージメント技術のための材料/界面/流体プロセス」に関する研修懇親会
    • Place of Presentation
      ホテル丸治(宇都宮市)
    • Year and Date
      2016-03-17
    • Related Report
      2015 Research-status Report
    • Invited
  • [Presentation] 表面修飾金属酸化物ナノ粒子の合成手法とその利用2016

    • Author(s)
      高見誠一、阿尻雅文
    • Organizer
      『ナノマテリアルの新展開』 in ナノマテリアルコロキウム
    • Place of Presentation
      秋田大学ベンチャー・ビジネス・ラボラトリー2階大セミナー室(秋田市)
    • Year and Date
      2016-01-12
    • Related Report
      2015 Research-status Report
    • Invited
  • [Presentation] 超臨界技術を使ったナノ粒子、ナノ構造の作製2016

    • Author(s)
      高見 誠一
    • Organizer
      日本セラミックス協会 資源・環境関連材料部会 講演会
    • Place of Presentation
      東京都立産業技術センター(東京都江東区)
    • Related Report
      2016 Annual Research Report
    • Invited

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Published: 2015-04-16   Modified: 2018-03-22  

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