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Precise determination of semi-volatile organic compounds with partitioning collection device

Research Project

Project/Area Number 15K17875
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Analytical chemistry
Research InstitutionUniversity of Yamanashi

Principal Investigator

UETA Ikuo  山梨大学, 大学院総合研究部, 助教 (50598688)

Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2017: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2016: ¥2,080,000 (Direct Cost: ¥1,600,000、Indirect Cost: ¥480,000)
Fiscal Year 2015: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Keywords試料前処理 / ガスクロマトグラフィー / 半揮発性有機化合物 / 多環芳香族炭化水素 / 試料濃縮 / セスキテルペン
Outline of Final Research Achievements

This study developed a collection device for precise determination of airborne semi-volatile organic compounds, such as polycyclic aromatic hydrocarbons (PAHs) and sesquiterpenes. First, partition-based collection of SVOC was investigated. As the partition mediums, octadecyl bound silica and poly-dimethyl siloxane coated silica were investigated.
Next, a novel collection device packed with styrene-divinylbenzene polymer particles was developed. The device showed higher collection power for several airborne SVOCs. In addition, the collected SVOCs were completely eluted by just passing of small amount of organic solvent.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (24 results)

All 2018 2017 2016 2015 Other

All Journal Article (9 results) (of which Peer Reviewed: 9 results,  Open Access: 4 results,  Acknowledgement Compliant: 5 results) Presentation (14 results) (of which Int'l Joint Research: 1 results,  Invited: 7 results) Remarks (1 results)

  • [Journal Article] Analysis of Biogenic Volatile Organic Compounds in Air Using a Solid-Phase Extraction-Type Collection Device2018

    • Author(s)
      I. Ueta, H. Fujikawa, K. Fujimura, T. Yoshimura, S. Narukami, S. Mochizuki, T. Sasaki, T. Maeda
    • Journal Title

      CHROMATOGRAPHY

      Volume: 39 Issue: 1 Pages: 27-32

    • DOI

      10.15583/jpchrom.2017.015

    • NAID

      130006464315

    • ISSN
      1342-8284, 1348-3315
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Determination of Aqueous Formic and Acetic Acids by Purge-and-Trap Analysis with a Needle-Type Extraction Device and Gas Chromatography Barrier Discharge Ionization Detector2018

    • Author(s)
      I. Ueta, Y. Nakamura, S. Kawakubo, Y. Saito
    • Journal Title

      Analytical Sciences

      Volume: 34 Issue: 2 Pages: 201-205

    • DOI

      10.2116/analsci.34.201

    • NAID

      130006342070

    • ISSN
      0910-6340, 1348-2246
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] A Newly Designed Solid-Phase Extraction-type Collection Device for Precise Determination of Polycyclic Aromatic Hydrocarbons in Air2017

    • Author(s)
      I. Ueta, M. Onikata, K. Fujimura, T. Yoshimura, S. Narukami, S. Mochizuki, T. Sasaki, T. Maeda
    • Journal Title

      Analytical Sciences

      Volume: 33 Issue: 10 Pages: 1175-1180

    • DOI

      10.2116/analsci.33.1175

    • NAID

      130006163680

    • ISSN
      0910-6340, 1348-2246
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Determination of Gaseous Formic and Acetic Acids by a Needle-Type Extraction Device coupled to a Gas Chromatography-Barrier Discharge Ionization Detector2017

    • Author(s)
      I. Ueta, Y. Nakamura, K. Fujimura, S. Kawakubo and Y. Saito
    • Journal Title

      Chromatographia

      Volume: 80 Issue: 1 Pages: 151-156

    • DOI

      10.1007/s10337-016-3201-2

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Polydimethylsiloxane Coated Partitioning Sample Collection Device for the Precise Quantification of Polycyclic Aromatic Hydrocarbons in Air2016

    • Author(s)
      I. Ueta, M. Onikata, K. Fujimura, T. Yoshimura, S. Narukami, S. Mochizuki, T. Sasaki, T. Maeda
    • Journal Title

      Journal of Separation Science

      Volume: 39 Issue: 21 Pages: 11-14

    • DOI

      10.1002/jssc.201600752

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Determination of Airborne Semi-Volatile Polycyclic Aromatic Hydrocarbons by Partitioning-Type Extraction Device Packed with Octadecyl-Derivatized Macroporous Silica2016

    • Author(s)
      I. Ueta, M. Onikata, K. Fujimura, T. Sasaki, T. Yoshimura, S. Mochizuki, T. Maeda
    • Journal Title

      CHROMATOGRAPHY

      Volume: 37 Issue: 1 Pages: 9-13

    • DOI

      10.15583/jpchrom.2015.038

    • NAID

      130005133693

    • ISSN
      1342-8284, 1348-3315
    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] I. Ueta, T. Mitsumori, Y. Suzuki, S. Kawakubo and Y. Saito Determination of Very Volatile Organic Compounds in Water Samples by Purge and Trap Analysis with a Needle-Type Extraction Device2015

    • Author(s)
      I. Ueta, T. Mitsumori, Y. Suzuki, S. Kawakubo and Y. Saito
    • Journal Title

      Journal of Chromatography A

      Volume: 印刷中 Pages: 27-31

    • DOI

      10.1016/j.chroma.2015.04.016

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Partitioning Sample Collection/Solvent Extraction Cartridge Packed with Octadecyl-Derivatized Macroporous Silica Particles for the Analysis of Sesquiterpenes in Air Samples2015

    • Author(s)
      l. Ueta, M. Onikata, S. Mochizuki, K. Fuiimura, T. Sasaki, J. Aoki, T. Maeda
    • Journal Title

      Journal of Separation Science

      Volume: 38 Issue: 22 Pages: 3891-3896

    • DOI

      10.1002/jssc.201500629

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Purge-and-Trap Analysis of Flavor Compounds inAqueous Samples by a Needle-Type Extraction Device2015

    • Author(s)
      I. Ueta, T Mitsumori, Y Suzuki, S. Kawakubo and Y. Saito
    • Journal Title

      CHROMATOGRAPHY

      Volume: 36 Issue: 3 Pages: 99-104

    • DOI

      10.15583/jpchrom.2015.031

    • NAID

      130005118197

    • ISSN
      1342-8284, 1348-3315
    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] 試料濃縮針を用いた溶液中のギ酸及び酢酸のパージトラップ・GC-BID分析2017

    • Author(s)
      中村 陽平, 植田 郁生, 川久保 進, 齊戸 美弘
    • Organizer
      第24回クロマトグラフィーシンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] 固相抽出型デバイスを用いるSVOC捕集法の新展開2017

    • Author(s)
      植田 郁生
    • Organizer
      2017JAIMAセミナー
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] Quantitative Determination of Airborne Semi-Volatile Organic Compounds by Solid-Phase Extraction-Type Collection Device2017

    • Author(s)
      Ikuo Ueta, Koji Fujimura, Tomotaka Yoshimura, Shoji Narukami, Suguru Mochizuki, Tomohiro Sasaki, Tsuneaki Maeda
    • Organizer
      Asia/ CJK symposium on analytical science 2017
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 固相抽出型SVOC捕集デバイスを用いた大気中テルペン類の分析2017

    • Author(s)
      藤川 尋斗, 植田 郁生, 藤村 耕治, 芳村 智孝, 鳴上 翔士, 望月 賢, 佐々木 智啓, 前田 恒昭
    • Organizer
      日本分析化学会第65年会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 新規スチレン-ジビニルベンゼン粒子捕集デバイスを用いた大気中の多環芳香族炭化水素の分析2016

    • Author(s)
      鬼形 萌, 植田 郁生, 藤村 耕治, 芳村 智孝, 鳴上 翔士, 望月 賢, 佐々木 智啓, 前田 恒昭
    • Organizer
      第27回クロマトグラフィー科学会議
    • Place of Presentation
      慶應義塾大学(東京都・港区)
    • Year and Date
      2016-11-16
    • Related Report
      2016 Research-status Report
  • [Presentation] 大気中の多環芳香族炭化水素測定のための新規デバイスの開発2016

    • Author(s)
      鬼形 萌, 植田 郁生, 藤村 耕治, 芳村 智孝, 鳴上 翔士, 望月 賢, 佐々木 智啓, 前田 恒昭
    • Organizer
      日本分析化学会第65年会
    • Place of Presentation
      北海道大学(北海道・札幌市)
    • Year and Date
      2016-09-14
    • Related Report
      2016 Research-status Report
  • [Presentation] 大気中半揮発性有機化合物捕集用デバイスの開発2016

    • Author(s)
      植田 郁生, 鬼形 萌, 藤村 耕次, 芳村 智孝, 鳴上 翔士, 望月 賢, 佐々木 智啓, 前田 恒昭
    • Organizer
      日本分析化学会第65年会
    • Place of Presentation
      北海道大学(北海道・札幌市)
    • Year and Date
      2016-09-14
    • Related Report
      2016 Research-status Report
    • Invited
  • [Presentation] 試料濃縮針とガスクロマトグラフ‐バリア放電イオン化検出器を用いた空気中のギ酸及び酢酸の分析2016

    • Author(s)
      中村 陽平, 植田 郁生, 川久保 進, 齊戸 美弘
    • Organizer
      第23回クロマトグラフィーシンポジウム
    • Place of Presentation
      山梨県立図書館(山梨県・甲府市)
    • Year and Date
      2016-06-15
    • Related Report
      2016 Research-status Report
  • [Presentation] 小型濃縮デバイスを用いたVOCの分析2016

    • Author(s)
      植田 郁生
    • Organizer
      平成27年度標準ガスクラブ講演会
    • Place of Presentation
      TKP東京駅前会議室 (東京都・中央区)
    • Year and Date
      2016-02-05
    • Related Report
      2015 Research-status Report
    • Invited
  • [Presentation] 針型抽出デバイスを用いる新規パージ・トラップ法による揮発性有機化合物の迅速・高感度分析法の確立2016

    • Author(s)
      植田 郁生
    • Organizer
      2016年度クリタ水・環境科学財団研究助成金贈呈式
    • Place of Presentation
      京王プラザホテル(東京都・新宿区)
    • Related Report
      2016 Research-status Report
    • Invited
  • [Presentation] 分配型捕集デバイスを用いた大気中の半揮発性有機化合物の分析2015

    • Author(s)
      植田 郁生, 鬼形 萌, 藤村 耕治, 佐々木 智啓, 芳村 智孝, 望月 賢, 前田 恒昭
    • Organizer
      第26回クロマトグラフィー科学会議
    • Place of Presentation
      九州大学 (福岡県・福岡市)
    • Year and Date
      2015-11-11
    • Related Report
      2015 Research-status Report
    • Invited
  • [Presentation] 針型濃縮デバイスを用いる揮発性有機化合物の分析2015

    • Author(s)
      植田 郁生
    • Organizer
      日本分析化学会第64年会
    • Place of Presentation
      九州大学 (福岡県・福岡市)
    • Year and Date
      2015-09-09
    • Related Report
      2015 Research-status Report
    • Invited
  • [Presentation] 揮発性有機化合物捕集用新規分配型デバイスの開発2015

    • Author(s)
      鬼形 萌, 植田 郁生, 望月 賢, 藤村 耕治, 佐々木 智啓, 青木 潤次, 前田 恒昭
    • Organizer
      第22回クロマトグラフィーシンポジウム
    • Place of Presentation
      近畿大学 (大阪府・東大阪市)
    • Year and Date
      2015-05-28
    • Related Report
      2015 Research-status Report
  • [Presentation] オクタデシル基修飾シリカ粒子を用い空気中半揮発性有機化合物の分配捕集2015

    • Author(s)
      鬼形 萌, 植田 郁生, 望月 賢, 藤村 耕治, 佐々木 智啓, 青木 潤次, 前田 恒昭
    • Organizer
      第75回分析化学討論会
    • Place of Presentation
      山梨大学 (山梨県・甲府市)
    • Year and Date
      2015-05-23
    • Related Report
      2015 Research-status Report
  • [Remarks] 研究室webページ

    • URL

      http://www.ccn.yamanashi.ac.jp/~iueta/Index.html

    • Related Report
      2017 Annual Research Report 2016 Research-status Report 2015 Research-status Report

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Published: 2015-04-16   Modified: 2019-03-29  

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