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Evaluation of hydrogen distribution at vicinity of a crack employing a local strain measurement

Research Project

Project/Area Number 15K17930
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Materials/Mechanics of materials
Research InstitutionKyushu University (2016)
Tohoku University (2015)

Principal Investigator

Takakuwa Osamu  九州大学, 水素材料先端科学研究センター, 特任准教授 (60633518)

Project Period (FY) 2015-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2016: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2015: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Keywords水素脆化 / 亀裂 / 応力拡大係数
Outline of Final Research Achievements

Hydrogen concentrating around a crack tip significantly accelerates crack propagation, i.e., hydrogen embrittlement. In order to clarify the mechanism leading to this, the local hydrogen concentration behavior, i.e., at a crack tip, was evaluated by numerical analysis and experimental measurements. Although thermal desorption analysis can be used to evaluate the total hydrogen content in metals, it cannot be applied to local areas. Microprint methods, which use chemical reactions between hydrogen and coated elements cannot quantitatively evaluate the hydrogen content. The present study takes account of hydrogen-induced strain, and X-ray diffraction in a confined area was employed to detect variations in lattice spacing before and after hydrogen charging. Using X-ray diffraction applied to a small area, it was demonstrated that the hydrogen concentrates in the vicinity of the crack, i.e., at the elastic-plastic boundary.

Report

(3 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • Research Products

    (7 results)

All 2016 2015

All Journal Article (2 results) (of which Peer Reviewed: 2 results,  Acknowledgement Compliant: 2 results) Presentation (5 results) (of which Int'l Joint Research: 3 results)

  • [Journal Article] Experimental verification of the hydrogen concentration around a crack tip using spot X-ray diffraction2016

    • Author(s)
      Osamu Takakuwa, Takuya Fujisawa, Hitoshi Soyama
    • Journal Title

      International Journal of Hydrogen Energy

      Volume: 41 Issue: 48 Pages: 23188-23195

    • DOI

      10.1016/j.ijhydene.2016.10.083

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Improvement of delayed fracture resistance on chrome molybdenum steel bolt by cavitation peening2016

    • Author(s)
      熊谷直輝,高桑脩,祖山均
    • Journal Title

      Transactions of the JSME (in Japanese)

      Volume: 82 Issue: 842 Pages: 16-00111-16-00111

    • DOI

      10.1299/transjsme.16-00111

    • NAID

      130005433191

    • ISSN
      2187-9761
    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Improvement of the Resistance to Delayed Fracture in High-Strength Bolt Made of Cr-Mo Steel by Means of Cavitation Peening2016

    • Author(s)
      Osamu Takakuwa, Naoki Kumagai, Hitoshi Soyama
    • Organizer
      International Conference on Laser Peening and Related Phenomena
    • Place of Presentation
      Skukuza, Kruger National Park
    • Year and Date
      2016-11-06
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Prevention of hydrogen entry in stainless steel using a surface modification2016

    • Author(s)
      Osamu Takakuwa
    • Organizer
      M&M International Symposium for Young Researchers
    • Place of Presentation
      Stony Brook University
    • Year and Date
      2016-08-10
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] An Experimental Evaluation of the Hydrogen Concentration around a Notch Using an X-ray Diffraction Analysis2016

    • Author(s)
      髙桑 脩,星野 柊,祖山 均
    • Organizer
      2016 M&M International Symposium for Young Researchers
    • Place of Presentation
      Stony Brool University
    • Year and Date
      2016-08-10
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 微小部ひずみ測定を用いたき裂先端部への水素凝集挙動の実験的評価2015

    • Author(s)
      髙桑 脩,藤沢 拓弥,祖山 均
    • Organizer
      日本鉄鋼協会第170回秋季講演大会
    • Place of Presentation
      九州大学,福岡県福岡市
    • Year and Date
      2015-09-16
    • Related Report
      2015 Research-status Report
  • [Presentation] 微小部X線回折測定によるき裂先端部への局所的水素凝集挙動の評価2015

    • Author(s)
      髙桑 脩,藤沢 拓弥,祖山 均
    • Organizer
      日本機械学会2015年度年次大会
    • Place of Presentation
      北海道大学,北海道札幌市
    • Year and Date
      2015-09-14
    • Related Report
      2015 Research-status Report

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Published: 2015-04-16   Modified: 2018-03-22  

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