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Growth of low-reisitivity diamond wafers for ultra low-loss power electronics

Research Project

Project/Area Number 15K18043
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Electronic materials/Electric materials
Research InstitutionNational Institute of Advanced Industrial Science and Technology

Principal Investigator

OHMAGARI Shinya  国立研究開発法人産業技術総合研究所, エネルギー・環境領域, 研究員 (40712211)

Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2017: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2016: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2015: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Keywordsダイヤモンド / ホウ素ドープ / 低抵抗 / ウェハ / 化学気相成長法 / 欠陥 / 縦型パワーデバイス / 低抵抗ウェハ / 結晶成長 / 結晶構造 / 厚膜合成 / ドーピング / パワーデバイス / 省エネルギー / 低損失
Outline of Final Research Achievements

Since diamond has superior physical properties than SiC and GaN, it is expected as material for ultra low-loss power electronics. The excellent switching capabilities has been demonstrated for both unipolar and bipolar devices. For practical vertical device structure, low-resistivity wafers are required. However, as for the conventional CVD, the instability of crystal growth such as soot formation, low doping efficiency has been a problem. In this research, heavily boron-doped diamond wafers were fabricated by hot filament CVD method which has advantageous in large area growth. We realized high doping concentration exceeding 1E21 cm-3, and low-resistivity wafer of the few mΩcm. The crystal quality was equivalent to that of commercially available insulating wafers. The high rectifying operation of vertical Schottky barrier diodes was also demonstrated.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (33 results)

All 2018 2017 2016 2015 Other

All Int'l Joint Research (1 results) Journal Article (7 results) (of which Int'l Joint Research: 2 results,  Peer Reviewed: 6 results,  Acknowledgement Compliant: 4 results) Presentation (20 results) (of which Int'l Joint Research: 7 results,  Invited: 5 results) Remarks (1 results) Patent(Industrial Property Rights) (4 results)

  • [Int'l Joint Research] Kohn Kaen University(タイ)

    • Related Report
      2015 Research-status Report
  • [Journal Article] Growth and characterization of freestanding p+ diamond (100) substrates prepared by hot-filament chemical vapor deposition2018

    • Author(s)
      Ohmagari Shinya、Yamada Hideaki、Umezawa Hitoshi、Tsubouchi Nobuteru、Chayahara Akiyoshi、Mokuno Yoshiaki
    • Journal Title

      Diamond and Related Materials

      Volume: 81 Pages: 33-37

    • DOI

      10.1016/j.diamond.2017.11.003

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Lifetime and migration length of B-related admolecules on diamond {1 0 0}-surface: Comparative study of hot-filament and microwave plasma-enhanced chemical vapor deposition2017

    • Author(s)
      Ohmagari Shinya、Ogura Masahiko、Umezawa Hitoshi、Mokuno Yoshiaki
    • Journal Title

      Journal of Crystal Growth

      Volume: 479 Pages: 52-58

    • DOI

      10.1016/j.jcrysgro.2017.09.022

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Ohmic contact formation to heavily boron-doped p+ diamond prepared by hot-filament chemical vapor deposition2016

    • Author(s)
      S. Ohmagari, T. Matsumoto, H. Umezawa, and Y. Mokuno
    • Journal Title

      MRS Advances

      Volume: 1 Issue: 51 Pages: 3489-3489

    • DOI

      10.1557/adv.2016.471

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Submicron-scale diamond selective-area growth by hot-filament chemical vapor deposition2016

    • Author(s)
      S. Ohmagari, T. Matsumoto, H. Umezawa, and Y. Mokuno
    • Journal Title

      Thin Solid Films

      Volume: 615 Pages: 239-239

    • DOI

      10.1016/j.tsf.2016.07.017

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] ダイヤモンド単結晶ウェーハ開発の現状と課題2016

    • Author(s)
      杢野由明、山田英明、茶谷原昭義、大曲新矢
    • Journal Title

      NEW DIAMOND

      Volume: 32 Pages: 30-33

    • Related Report
      2016 Research-status Report
  • [Journal Article] Boron inhomogeneity of HPHT-grown single-crystal diamond substrates: confocal micro-Raman mapping investigations2016

    • Author(s)
      K. Srimongkon, S. Ohmagari, Y. Kato, V. Amornkitbamrung, and S. Shikata
    • Journal Title

      Diamond and Related Materials

      Volume: 63 Pages: 21-25

    • DOI

      10.1016/j.diamond.2015.09.014

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Journal Article] Low resistivity p+ diamond (100) films fabricated by hot-filament chemical vapor deposition2015

    • Author(s)
      S. Ohmagari, K. Srimongkon, H. Yamada, H. Umezawa, N. Tsubouchi, A. Chayahara, S. Shikata, and Y. Mokuno
    • Journal Title

      Diamond and Related Materials

      Volume: 58 Pages: 110-114

    • DOI

      10.1016/j.diamond.2015.06.011

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Int'l Joint Research / Acknowledgement Compliant
  • [Presentation] 異原子導入によるダイヤモンド貫通転位の伝搬抑制効果2018

    • Author(s)
      大曲新矢、山田英明、坪内信輝、田中真悟、茶谷原昭義、梅沢仁、杢野由明
    • Organizer
      第65回応用物理学会春季学術講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Hot-filament CVD growth of low-resistivity diamond for power device applications2017

    • Author(s)
      S. Ohmagari
    • Organizer
      化学工学会 第82年会
    • Place of Presentation
      芝浦工業大学豊洲キャンパス,東京都江東区
    • Year and Date
      2017-03-06
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] 高出力縦型パワーデバイス用ダイヤモンド低抵抗ウェハ開発2017

    • Author(s)
      大曲新矢
    • Organizer
      第66回CVD研究会
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] 熱フィラメントCVD法によるパワーデバイス用ダイヤモンド結晶成長2017

    • Author(s)
      大曲新矢
    • Organizer
      Cat-CVD研究会
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] Structural and Chemical Bonding Analysis of Diamond Semiconductors using Synchrotron Radiation2017

    • Author(s)
      Shinya Ohmagari
    • Organizer
      ASEAN Workshop on Photoemission Electron Spectroscopy and Microscopy (AWPESM2017)
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] 熱フィラメントCVD法で合成した低抵抗ダイヤモンド自立基板評価2017

    • Author(s)
      大曲新矢、山田英明、梅沢仁、坪内信輝、茶谷原昭義、杢野由明
    • Organizer
      第78回応用物理学会秋季学術講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] ダイヤモンド選択成長: フィラメントCVDとメタルマスク併用による微細パターニング2016

    • Author(s)
      大曲 新矢,松本 猛,梅沢 仁,杢野 由明
    • Organizer
      第30回ダイヤモンドシンポジウム
    • Place of Presentation
      東京大学駒場リサーチキャンパス,東京都目黒区
    • Year and Date
      2016-11-16
    • Related Report
      2016 Research-status Report
  • [Presentation] Strategy to grow high-quality p+ diamond substrates: doping efficiency, lattice mismatch, and resistivity controls2016

    • Author(s)
      S. Ohmagari, H. Yamada, H. Umezawa, N. Tsubouchi, A. Chayahara, and Y. Mokuno
    • Organizer
      European Materials Research Society (E-MRS)
    • Place of Presentation
      ワルシャワ工科大学,ワルシャワ,ポーランド
    • Year and Date
      2016-09-19
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Selective-Area Growth of Single-Crystal Diamond Films by Hot-Filament CVD Using Metal Masks2016

    • Author(s)
      S. Ohmagari, T. Matsumoto, H. Umezawa, and Y. Mokuno
    • Organizer
      HWCVD9
    • Place of Presentation
      Chemical Heritage Foundation,フィラデルフィア,アメリカ
    • Year and Date
      2016-09-06
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Homoepitaxial Diamond Growth by Hot-Filament CVD For Future Diamond Power Devices2016

    • Author(s)
      S. Ohmagari, H. Yamada, H. Umezawa, N. Tsubouchi, A. Chayahara, and Y. Mokuno
    • Organizer
      HWCVD9
    • Place of Presentation
      Chemical Heritage Foundation,フィラデルフィア,アメリカ
    • Year and Date
      2016-09-06
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Low Resistivity P+ Single-Crystal Diamond Prepared by Hot-Filament CVD2016

    • Author(s)
      S. Ohmagari, and Y. Mokuno
    • Organizer
      2016 MRS Spring Meeting & Exhibit
    • Place of Presentation
      Phoenix, Arizona
    • Year and Date
      2016-03-28
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 超低損失パワーデバイス用途ダイヤモンド低抵抗ウェハの開発2016

    • Author(s)
      大曲 新矢、山田 英明、梅沢 仁、坪内 信輝、茶谷原 昭義、 杢野 由明
    • Organizer
      応用物理学会関西支部平成28年度第1回講演会
    • Place of Presentation
      産業技術総合研究所関西センター,大阪府池田市
    • Related Report
      2016 Research-status Report
  • [Presentation] 逆格子空間マッピング法による高濃度ホウ素ドープダイヤモンド (100) 薄膜の歪み評価2015

    • Author(s)
      竹市悟志, 大曲新矢, 杢野由明,吉武剛
    • Organizer
      平成27年度応用物理学会九州支部学術講演会
    • Place of Presentation
      琉球大学工学部
    • Year and Date
      2015-12-05
    • Related Report
      2015 Research-status Report
  • [Presentation] フィラメントCVD 法による高濃度ホウ素ドープダイヤモンド(100) 薄膜の 擬似格子整合成長2015

    • Author(s)
      大曲新矢,山田英明,茶谷原昭義,鹿田真一,杢野由明
    • Organizer
      第29回ダイヤモンドシンポジウム
    • Place of Presentation
      東京理科大学
    • Year and Date
      2015-11-17
    • Related Report
      2015 Research-status Report
  • [Presentation] HPHT 製p+ダイヤモンド (100) 基板の共焦点ラマンマッピング評価2015

    • Author(s)
      大曲新矢,K.Srimongkon, V.Amornkitbamrung,加藤有香子,鹿田真一
    • Organizer
      第29回ダイヤモンドシンポジウム
    • Place of Presentation
      東京理科大学
    • Year and Date
      2015-11-17
    • Related Report
      2015 Research-status Report
  • [Presentation] cTLM法によるダイヤモンドp-/p++界面の接触抵抗評価2015

    • Author(s)
      大曲 新矢,梅沢 仁,松本 猛, 杢野 由明
    • Organizer
      先進パワー半導体分科会 第2回講演会
    • Place of Presentation
      大阪国際交流センター
    • Year and Date
      2015-11-09
    • Related Report
      2015 Research-status Report
  • [Presentation] フィラメントCVD法による低抵抗 (1 mΩcm) ダイヤモンドの合成2015

    • Author(s)
      大曲新矢,山田英明,梅沢仁,茶谷原昭義,鹿田真一,杢野由明
    • Organizer
      第76回応用物理学会秋季学術講演会
    • Place of Presentation
      名古屋国際会議場
    • Year and Date
      2015-09-13
    • Related Report
      2015 Research-status Report
  • [Presentation] Characterization of low-resistivity diamond (100) films fabricated by hot-filament chemical vapor deposition2015

    • Author(s)
      S. Ohmagari, K. Srimongkon, H. Yamada, H. Umezawa, N. Tsubouchi, A. Chayahara, S. Shikata, and Y. Mokuno
    • Organizer
      The 35th Electron Materials Symposium
    • Place of Presentation
      ラフォーレ琵琶湖
    • Year and Date
      2015-07-06
    • Related Report
      2015 Research-status Report
  • [Presentation] Heavily boron-doped single-crystal diamond (100) films prepared by hotfilament CVD2015

    • Author(s)
      S. Ohmagari, K. Srimongkon, H. Yamada, H. Umezawa, N. Tsubouchi, A. Chayahara, and S. Shikata
    • Organizer
      International Conference on New Diamond & Nano Carbon 2015
    • Place of Presentation
      Shizuoka GRANSHIP, Japan
    • Year and Date
      2015-05-25
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] Defects analysis of HPHT-grown heavily boron-doped diamond (100) by dry etching technique2015

    • Author(s)
      K. Srimongkon, S. Ohmagari, N. Tsubouchi, Y. Kato, V. Amornkitbamrung, and S. Shikata
    • Organizer
      International Conference on New Diamond & Nano Carbon 2015
    • Place of Presentation
      Shizuoka GRANSHIP, Japan
    • Year and Date
      2015-05-25
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Remarks] Diamond Research -Shinya Ohmagari-

    • URL

      https://staff.aist.go.jp/shinya.ohmagari/

    • Related Report
      2015 Research-status Report
  • [Patent(Industrial Property Rights)] 単結晶ダイヤモンドおよびそれを用いた半導体素子2017

    • Inventor(s)
      大曲新矢,山田英明,茶谷原昭義,杢野由明
    • Industrial Property Rights Holder
      国立研究開発法人 産業技術総合研究所
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2017-243965
    • Filing Date
      2017
    • Related Report
      2017 Annual Research Report
  • [Patent(Industrial Property Rights)] 不純物ドープダイヤモンド2016

    • Inventor(s)
      大曲新矢、山田英明、梅沢仁、茶谷原昭義、杢野由明
    • Industrial Property Rights Holder
      大曲新矢、山田英明、梅沢仁、茶谷原昭義、杢野由明
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2016-141305
    • Filing Date
      2016-07-19
    • Related Report
      2016 Research-status Report
  • [Patent(Industrial Property Rights)] ホウ素ドープダイヤモンド2016

    • Inventor(s)
      大曲新矢、梅沢仁、山田英明、茶谷原昭義、杢野由明
    • Industrial Property Rights Holder
      大曲新矢、梅沢仁、山田英明、茶谷原昭義、杢野由明
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2016-141306
    • Filing Date
      2016-07-19
    • Related Report
      2016 Research-status Report
  • [Patent(Industrial Property Rights)] 不純物ドープダイヤモンド及びその製造方法2015

    • Inventor(s)
      大曲新矢,山田英明,茶谷原昭義,鹿田真一,杢野由明
    • Industrial Property Rights Holder
      大曲新矢,山田英明,茶谷原昭義,鹿田真一,杢野由明
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2015-098261
    • Filing Date
      2015-05-13
    • Related Report
      2015 Research-status Report

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Published: 2015-04-16   Modified: 2022-02-16  

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