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Nano-structural control of iron-based non-equilibrium materials by container-less solidification process

Research Project

Project/Area Number 15K18244
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Material processing/Microstructural control engineering
Research InstitutionTohoku University

Principal Investigator

Yodoshi Noriharu  東北大学, 金属材料研究所, 助教 (60586494)

Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥4,160,000 (Direct Cost: ¥3,200,000、Indirect Cost: ¥960,000)
Fiscal Year 2017: ¥780,000 (Direct Cost: ¥600,000、Indirect Cost: ¥180,000)
Fiscal Year 2016: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Fiscal Year 2015: ¥1,690,000 (Direct Cost: ¥1,300,000、Indirect Cost: ¥390,000)
Keywordsamorphous alloy / metallic glass / soft magnetic material / containerless process / mono-dispersed particle / nanocryatallization / 無容器凝固 / 単分散粒子 / 鉄系金属ガラス / 軟磁性材料 / ナノ結晶
Outline of Final Research Achievements

In this study, we evaluate iron-based non-equilibrium materials from the viewpoint of thermal stability and nucleation generation in supercooled liquid by using a container-less solidification process. The aims of this study were to clarify a possibility of nano-structural control, the relationship between the nano-structure and the magnetic properties.
Among various iron-based alloys, the Fe76Si9B10P5 hetero-amorphous alloy exhibits excellent amorphous forming ability, and the possibility that the high densed clusters are embedded inside is experimentally confirmed. In addition, it was confirmed that nano-crystallization can be achieved by performing an appropriate heat treatment, and excellent soft magnetic properties are exhibited. We also clarified the possibility of nano-structure control by adding minor copper element.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (24 results)

All 2018 2017 2016 2015

All Journal Article (7 results) (of which Peer Reviewed: 7 results,  Open Access: 1 results,  Acknowledgement Compliant: 2 results) Presentation (17 results) (of which Int'l Joint Research: 5 results,  Invited: 1 results)

  • [Journal Article] Effects of nanocrystallisation on saturation magnetisation of amorphous Fe76Si9B10P52018

    • Author(s)
      Yodoshi Noriharu、Ookawa Shunpei、Yamada Rui、Nomura Naoyuki、Kikuchi Keiko、Kawasaki Akira
    • Journal Title

      Materials Research Letters

      Volume: 6 Issue: 1 Pages: 100-105

    • DOI

      10.1080/21663831.2017.1398191

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] 高品位鉄系非晶質粒子の作製とその応用2017

    • Author(s)
      吉年規治
    • Journal Title

      ふぇらむ

      Volume: 22 Pages: 2-9

    • Related Report
      2017 Annual Research Report 2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Micro Viscous Flow Processing of Iron-based Metallic Glasses2016

    • Author(s)
      吉年規治、山田類、川崎亮
    • Journal Title

      Materia Japan

      Volume: 55 Issue: 4 Pages: 152-159

    • DOI

      10.2320/materia.55.152

    • NAID

      130005140505

    • ISSN
      1340-2625, 1884-5843
    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Temperature dependency of viscosity of Fe76Si9B10P5 supercooled liquid and hetero-amorphous structure2016

    • Author(s)
      N. Yodoshi, R. Yamada, A. Kawasaki, A. Makino
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 679 Pages: 164-168

    • DOI

      10.1016/j.jallcom.2016.04.032

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Journal Article] Mechanically strong nanocrystalline Fe-Si-B-P-Cu soft magnetic powder cores utilizing magnetic metallic glass as a binder2016

    • Author(s)
      Jian Luan, Parmanand Sharma, Noriharu Yodoshi, Yan Zhang, Akihiro Makino
    • Journal Title

      AIP Advances

      Volume: 6 Issue: 5 Pages: 55934-55934

    • DOI

      10.1063/1.4944766

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Journal Article] Evaluation of critical cooling rate of Fe76Si9B10P5 metallic glass by containerless solidification process2015

    • Author(s)
      Noriharu Yodoshi, Rui Yamada, Akira Kawasaki, Akihiro Makino
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 643 Pages: S2-S7

    • DOI

      10.1016/j.jallcom.2015.04.088

    • Related Report
      2015 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Production of a magnetic material with the ability to change from very soft to semi-hard magnetic2015

    • Author(s)
      Zhang Y., Sharma P., Yodoshi N., Makino A.
    • Journal Title

      Journal of Applied Physics

      Volume: 117 Issue: 17

    • DOI

      10.1063/1.4916812

    • Related Report
      2015 Research-status Report
    • Peer Reviewed
  • [Presentation] FeCoSiBPアモルファス単粒子のナノ結晶化と磁気特性評価2017

    • Author(s)
      吉年規治、峯岸剛太、山田類、菊池 圭子、野村 直之、川崎 亮
    • Organizer
      粉体粉末冶金協会春季大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Fabrication of mono-dispersed amorphous Fe76Si9B10P5 particles by container-less solidification process and their soft magnetic property2017

    • Author(s)
      N. Yodoshi, R. Yamada, A. Kawasaki
    • Organizer
      16th International Conference on Rapidly Quenched and Metastable Materials (RQ16)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Fe-Si-B-P-(Cu)系急冷単分散粒子のナノ結晶化挙動と磁気特性2017

    • Author(s)
      吉年規治、大川 舜平、山田類、野村 直之、菊池 圭子、川崎 亮
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 鉄系金属ガラス粒子マイクロ鍛造加工の粘弾性解析2017

    • Author(s)
      品川一成、吉年規治、山田類、川崎亮
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 金属ガラスの粘性流動成形加工による感圧素子用ダイヤフラムの作製2017

    • Author(s)
      青柳 慶真、吉年規治、菊池圭子、野村直之、川崎 亮
    • Organizer
      粉体粉末冶金協会秋季大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Fe‐Co‐Si‐B‐P系急冷単分散粒子のナノ結晶化挙動と磁気特性のCo濃度依存性2017

    • Author(s)
      峯岸剛太、吉年規治、菊池圭子、野村直之、川崎 亮
    • Organizer
      粉体粉末冶金協会秋季大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Nanocrystallization behavior of rare-metal-free ferrous amorphous mono-dispersed particles prepared by container-less solidification process.2017

    • Author(s)
      N. Yodoshi, R. Yamada, A. Kawasaki
    • Organizer
      MRS Fall Meeting & Exhibit
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] FeSiBP系単分散粒子の磁気特性とその組成依存性2016

    • Author(s)
      大川 舜平、菊池圭子、野村直之、川崎亮、吉年規治、牧野彰宏、山田類
    • Organizer
      粉体粉末冶金協会秋季大会
    • Place of Presentation
      東北大学(仙台)
    • Year and Date
      2016-11-09
    • Related Report
      2016 Research-status Report
  • [Presentation] Fe76Si9B10P5金属ガラス単分散粒子の粘性流動特性および磁気特性2016

    • Author(s)
      吉年規治、山田類、大川 舜平、野村 直之、菊池 圭子、川崎 亮
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Place of Presentation
      大阪大学(大阪)
    • Year and Date
      2016-09-21
    • Related Report
      2016 Research-status Report
  • [Presentation] Glass forming ability, thermal stability and soft magnetic property of Fe76Si9B10P5 metallic glass2016

    • Author(s)
      N. Yodoshi, R. Yamada, A. Makino, A. Kawasaki
    • Organizer
      16th International Conference on Liquid and Amorphous Metals (LAM-16)
    • Place of Presentation
      Bonn, Germany
    • Year and Date
      2016-09-04
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] FeSiBP系アモルファス単分散粒子のナノ結晶化挙動と磁気特性評価2016

    • Author(s)
      大川舜平、吉年規治、山田類、牧野彰宏、川崎亮
    • Organizer
      粉体粉末冶金協会春季大会
    • Place of Presentation
      京都工芸繊維大学(京都)
    • Year and Date
      2016-05-24
    • Related Report
      2016 Research-status Report
  • [Presentation] Fabrication of Iron-based Amorphous Particles by Quenching of Mono-dispersed Droplets2016

    • Author(s)
      N. Yodoshi, R. Yamada, A. Kawasaki
    • Organizer
      EMN droplets 2016
    • Place of Presentation
      San Sebastian, Spain
    • Year and Date
      2016-05-09
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] Fe76Si9B10P5金属ガラスの粘性係数の温度依存性2015

    • Author(s)
      吉年規治、大川舜平、山田類、牧野彰宏、川崎亮、
    • Organizer
      粉体粉末冶金協会秋季大会
    • Place of Presentation
      京都
    • Year and Date
      2015-11-11
    • Related Report
      2015 Research-status Report
  • [Presentation] 鉄系非平衡粉末の液相焼結2015

    • Author(s)
      吉年規治、川崎亮、牧野彰宏
    • Organizer
      第26回傾斜機能材料シンポジウム
    • Place of Presentation
      福岡
    • Year and Date
      2015-09-29
    • Related Report
      2015 Research-status Report
  • [Presentation] Fe76Si9B10P5単分散金属ガラス粒子作製と臨界冷却速度2015

    • Author(s)
      吉年規治、山田類、川崎亮、牧野彰宏
    • Organizer
      日本鉄鋼協会秋季講演大会
    • Place of Presentation
      福岡
    • Year and Date
      2015-09-16
    • Related Report
      2015 Research-status Report
  • [Presentation] 鉄系非晶質粉末の焼結2015

    • Author(s)
      吉年規治
    • Organizer
      第20回焼結研究会
    • Place of Presentation
      八戸
    • Year and Date
      2015-08-21
    • Related Report
      2015 Research-status Report
  • [Presentation] Thermal Stability and Fragility of Fe76Si9B10P5 Super-cooled Liquid and a Hint of Hetero-amorphous Structure2015

    • Author(s)
      Noriharu Yodoshi, Rui Yamada, Akira Kawasaki, AKihiro Makino
    • Organizer
      ISMANAM2015
    • Place of Presentation
      フランス、パリ
    • Year and Date
      2015-07-13
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research

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Published: 2015-04-16   Modified: 2019-03-29  

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