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Fabrication of high strength and high ductility titanium via high pressure gas jet milling and its deformation mechanism.

Research Project

Project/Area Number 15K18248
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Material processing/Microstructural control engineering
Research InstitutionRitsumeikan University

Principal Investigator

Ota Mie  立命館大学, 理工学部, 助教 (30710587)

Co-Investigator(Renkei-kenkyūsha) AMEYAMA Kei  立命館大学, 理工学部, 教授 (10184243)
Project Period (FY) 2015-04-01 – 2017-03-31
Project Status Completed (Fiscal Year 2016)
Budget Amount *help
¥4,030,000 (Direct Cost: ¥3,100,000、Indirect Cost: ¥930,000)
Fiscal Year 2016: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2015: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Keywords組織制御 / 高強度高延性 / 超強加工 / 粉末冶金 / 調和組織制御 / 強度延性バランス / チタンおよびチタン合金
Outline of Final Research Achievements

The harmonic structure was successfully created by controlled milling of fine-sized pure Ti powder via jet milling followed by spark plasma sintering. Spark plasma sintering of milled powder resulted in the formation of a “harmonic” structure wherein the severely deformed shell regions of the milled powders transformed to a three dimensional network of equiaxed fine-sized grains, enclosing the coarse-grained “core” areas. The pure Ti compacts with a harmonic structure exhibited a significant enhancement in the strength without compromising the ductility. The improved mechanical properties of the harmonic structure compacts were attributed to the specific topological distribution of high strength fine-grained “shell” and ductile coarse-grained “core” regions; as such a microstructure promotes uniform distribution of strain during plastic deformation and avoids the localized plastic deformation in the early stages of deformation.

Report

(3 results)
  • 2016 Annual Research Report   Final Research Report ( PDF )
  • 2015 Research-status Report
  • Research Products

    (26 results)

All 2017 2016 2015 Other

All Int'l Joint Research (2 results) Journal Article (9 results) (of which Int'l Joint Research: 3 results,  Peer Reviewed: 9 results) Presentation (13 results) (of which Int'l Joint Research: 5 results) Remarks (1 results) Funded Workshop (1 results)

  • [Int'l Joint Research] Paris 13 University/Poitier University/Institute Jean Lamour(フランス)

    • Related Report
      2016 Annual Research Report
  • [Int'l Joint Research] パリ13大学(フランス)

    • Related Report
      2015 Research-status Report
  • [Journal Article] 高強度・高靱性材料創製のための調和組織制御法に関する研究2017

    • Author(s)
      飴山 惠、太田 美絵
    • Journal Title

      粉体粉末冶金協会誌

      Volume: 64 Pages: 3-10

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Three-dimensionally gradient harmonic structure design: an integrated approach for high performance structural materials2016

    • Author(s)
      Sanjay Kumar Vajpai, Mie Ota, Zhe Zhang and Kei Ameyama
    • Journal Title

      Materials Research Letters

      Volume: 4 Issue: 4 Pages: 191-197

    • DOI

      10.1080/21663831.2016.1218965

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] ミリングプロセスによる二相ステンレス鋼の調和組織形成過程2016

    • Author(s)
      太田美絵、澤井貴一、南谷大樹、飴山惠
    • Journal Title

      日本金属学会誌

      Volume: 80 Pages: 379-385

    • NAID

      130005153014

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Application of Al-Si Semi-Solid Reaction for Fabricating Harmonic Structured Al Based Alloy2016

    • Author(s)
      Nur Zalikha KHALIL, Sanjay Kumar VAJPAI, Mie OTA, and Kei AMEYAMA
    • Journal Title

      J. Materials Transactions

      Volume: 57 Pages: 1433-1439

    • NAID

      130005289891

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Bulk Ni-W alloys with a composite-like microstructure processed by spark plasma sintering: Microstructure and mechanical properties2016

    • Author(s)
      Tarik Sadat, Guy Dirras, David Tingaud, Mie Ota, Thierry Chauveau, Damien Faurie, Sanjay Vajpai, Kei Ameyama
    • Journal Title

      Journal of Materials and Design

      Volume: 89 Pages: 1181-1190

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Three-Dimensionally Gradient and Periodic Harmonic Structure for High Performance Advanced Structural Materials2016

    • Author(s)
      Sanjay Kumar Vajpai, Han Yu, Mie Ota, Ikumu Watanabe, Kei Ameyama
    • Journal Title

      Journal of Material Transactions

      Volume: 57 Pages: 1424-1432

    • NAID

      130005289897

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Effect of Harmonic Microstructure on the Corrosion Behavior of SUS304L Austenitic Stainless Steel2016

    • Author(s)
      Prabhat K. Rai, S. Shekhar, M. Nakatani, M. Ota, S. K. Vajpai, K. Ameyama and K. Mondal
    • Journal Title

      Metallurgical and Materials Transaction A

      Volume: 47 Issue: 12 Pages: 6259-6269

    • DOI

      10.1007/s11661-016-3758-2

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] 調和組織を有する工業用純チタンの低温窒化挙動2016

    • Author(s)
      菊池将一、中村悠太、太田美絵、上野明、飴山惠
    • Journal Title

      粉体および粉末冶金協会誌

      Volume: 63 Pages: 731-738

    • NAID

      130005253110

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 高強度構造材料の創製(ヘテロ構造材料)における 50年間の技術動向と最新技術2016

    • Author(s)
      太田美絵、飴山惠
    • Journal Title

      日本学術振興会将来加工技術第136委員会 50周年記念誌

      Volume: 1 Pages: 171-174

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Presentation] Decomposition of α Phase in a Jet Milling Processed Ti-15V-3Cr-3Sn-3Al Alloy2017

    • Author(s)
      Shota Yokoyama, Kaishu Hamasaki, Mie Ota, Kei Ameyama
    • Organizer
      6th International Symposium on Functionalization and Applications of Soft/Hard Materials
    • Place of Presentation
      立命館大学(滋賀県・草津市)
    • Year and Date
      2017-01-21
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 高圧ガスジェットミリング法によるTi-15V-3Cr-3Sn-3Al合金の調和組織形成と機械的特性2016

    • Author(s)
      横山将太、太田美絵、David Tingaud、Guy Dirras、飴山惠
    • Organizer
      日本金属学会2016年秋季講演大会
    • Place of Presentation
      大阪大学(大阪府・豊中市)
    • Year and Date
      2016-09-22
    • Related Report
      2016 Annual Research Report
  • [Presentation] Influence of Thermo-Mechanical Treatments on The Mechanical Behavior Under Tensile and Shear Loadings of Ti-15V-3Cr-3Sn-3Al Alloy Processed by Powder Metallurgy Route2016

    • Author(s)
      Shota Yokoyama , Ryo Maeda, Azziz Hocini, Ota Mie, Sanjay K Vajpai, David Tingaud, Kei Ameyama, Guy Dirras
    • Organizer
      9th Pacific Rim International Conference on Advanced Materials and Processing (PRICM9)
    • Place of Presentation
      立命館大学(滋賀県・草津市)
    • Year and Date
      2016-08-03
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 遊星型ボールミリングならびに高圧ガスジェットミリングにおける粉末加工エネルギーの推定とその比較2016

    • Author(s)
      太田美絵、飴山惠
    • Organizer
      平成28年塑性加工春季講講演会
    • Place of Presentation
      京都工芸繊維大学(京都府・京都市)
    • Year and Date
      2016-05-22
    • Related Report
      2016 Annual Research Report
  • [Presentation] 調和組織制御による革新的力学特性を有する金属材料の創製2016

    • Author(s)
      飴山惠、太田美絵
    • Organizer
      平成28年塑性加工春季講講演会
    • Place of Presentation
      京都工芸繊維大学(京都府・京都市)
    • Year and Date
      2016-05-22
    • Related Report
      2016 Annual Research Report
  • [Presentation] The mechanical properties of heat-treated Ti-15V-3Cr-3Sn-3Al alloy processed by High Pressure Gas Jet Milling2016

    • Author(s)
      Shota Yokoyama, Ryo Maeda, Azziz Hocini, Mie Ota, Sanjay K. Vajpai, David Tingaud, Kei Ameyama, Guy Dirras
    • Organizer
      エネルギーイノベーション材料研究センター第2回シンポジウム
    • Place of Presentation
      立命館大学びわこ・くさつキャンパス(滋賀県草津市)
    • Year and Date
      2016-03-11
    • Related Report
      2015 Research-status Report
  • [Presentation] Effect of the strain rate Sensitivity on Harmonic Structure Designed Ti-6Al-4V Alloy2016

    • Author(s)
      Hidenori Maezawa, Ryo Maeda, M. Ota, S. K. Vajpai and Kei Ameyama
    • Organizer
      エネルギーイノベーション材料研究センター第2回シンポジウム
    • Place of Presentation
      立命館大学びわこ・くさつキャンパス(滋賀県草津市)
    • Year and Date
      2016-03-11
    • Related Report
      2015 Research-status Report
  • [Presentation] Ti-6Al-4V合金の高圧ガスジェットミリング法による調和組織制御2015

    • Author(s)
      前田亮、渡邊智之、渡守貴大、太田美絵、飴山惠
    • Organizer
      粉体粉末冶金協会 平成27年度秋季講演大会
    • Place of Presentation
      京都大学百周年時計台記念館(京都府京都市)
    • Year and Date
      2015-11-12
    • Related Report
      2015 Research-status Report
  • [Presentation] Unique mechanical properties of Harmonic Structure Designed Ti-6Al-4V compact produced by High Pressure Gas Milling2015

    • Author(s)
      R. Maeda, T. Watanabe,Syouta Yokoyama, M. Ota, S. K. Vajpai, K. Ameyama
    • Organizer
      The 3rd International Conference on Powder Metallurgy in Asia, APMA2015
    • Place of Presentation
      Kyoto University, Japan(京都府京都市)
    • Year and Date
      2015-11-08
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] Innovative Microstructural Designing and Powder Metallurgy Processing Strategies to Develop High Performance Structural and Functional Materials2015

    • Author(s)
      Sanjay Kumar Vajpai, Mie Ota, Kei Ameyama
    • Organizer
      The 3rd International Conference on Powder Metallurgy in Asia, APMA2015
    • Place of Presentation
      Kyoto University, Japan(京都府京都市)
    • Year and Date
      2015-11-08
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] Innovative Materials Design for High Performance Pure Titanium2015

    • Author(s)
      Mie Ota, Sanjay Kumar Vajpai, Hikaru Kawabata, Hidenori Maezawa and Kei Ameyama
    • Organizer
      The 13th World conference on Titanium
    • Place of Presentation
      San Diego, USA
    • Year and Date
      2015-08-20
    • Related Report
      2015 Research-status Report
    • Int'l Joint Research
  • [Presentation] 高圧ガスジェットミリング法により調和組織制御されたTi-6Al-4V合金の変形挙動2015

    • Author(s)
      横山 将太、前田 亮、渡邊 智之、太田 美絵、Sanjay Kumar Vajpai、飴山 惠
    • Organizer
      粉体粉末冶金協会 平成27年度春季講演大会
    • Place of Presentation
      早稲田大学国際会議場(東京都新宿区)
    • Year and Date
      2015-05-28
    • Related Report
      2015 Research-status Report
  • [Presentation] 工業用純チタン粉末を用いた高圧ガスジェットミリング法による調和組織制御2015

    • Author(s)
      前沢 英典、川畑 光、黒川 和晃、太田 美絵、Sanjay Kumar Vajpai、飴山 惠
    • Organizer
      粉体粉末冶金協会 平成27年度春季講演大会
    • Place of Presentation
      早稲田大学国際会議場(東京都新宿区)
    • Year and Date
      2015-05-28
    • Related Report
      2015 Research-status Report
  • [Remarks] 立命館大学理工学部機械システム系機械工学科飴山研究室

    • URL

      http://www.amelab.se.ritsumei.ac.jp/

    • Related Report
      2015 Research-status Report
  • [Funded Workshop] 6th International Symposium on Functionalization and Applications of Soft/Hard Materials2017

    • Place of Presentation
      立命館大学(滋賀県・草津市)
    • Year and Date
      2017-01-20
    • Related Report
      2016 Annual Research Report

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Published: 2015-04-16   Modified: 2018-03-22  

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