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Investigation of New Methodology for Provenance Study of Central Anatolian Iron/Steel Objects Using Synchrotron Radiation Methods

Research Project

Project/Area Number 15K21657
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Cultural assets study and museology
Sociology/History of science and technology
Research InstitutionIndependent Administrative Institution National Institutes for Cultural Heritage Tokyo National Research Institute for Cultural Properties

Principal Investigator

Masubuchi Mariya  独立行政法人国立文化財機構東京文化財研究所, 文化遺産国際協力センター, アソシエイトフェロー (50569209)

Research Collaborator SHIKAKU Ryuji  
TSUJI Naruki  
ITO Masayoshi  
UESUGI Kentaro  
HOSHINO Masato  
YAGI Naoto  
Project Period (FY) 2015-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥3,120,000 (Direct Cost: ¥2,400,000、Indirect Cost: ¥720,000)
Fiscal Year 2017: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2016: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Fiscal Year 2015: ¥1,040,000 (Direct Cost: ¥800,000、Indirect Cost: ¥240,000)
Keywords製鉄技術 / 鍛冶技術 / 非破壊分析 / 放射光分析 / 高エネルギー蛍光X線分析 / 放射光X線μCT / 製作地推定 / 放射光蛍光X線マッピング / 微量重元素 / 産地同定 / 放射光高エネルギー蛍光X線分析 / 放射光X線CT / 鉄製考古遺物 / アナトリア / 放射光
Outline of Final Research Achievements

This research has demonstrated technical applicability of synchrotron high-energy X-ray fluorescence (SR-HE-XRF) analysis for possible provenance study of ancient iron/steels and also synchrotron X-ray micro computed tomography (CT) for their non-destructive technical examination using iron/steel objects unearthed at an archaeological site in Central Anatolia, the Hittites' heartland.
The SR-HE-XRF analyses undertaken at BL08W, SPring-8, revealed that the vast majority of iron/steel objects contain heavy metals such as barium and lanthanum. Furthermore, SR-HE-XRF mapping illustrated that the distribution patterns of these heavy metals are not necessarily identical, which indicates they were contained in the objects in a different way. Also, the synchrotron X-ray micro-CT imaging conducted at BL20B2 successfully provided reconstructed images sufficient for the identification of distribution patterns of slag inclusions being important for technical examination especially about forging.

Report

(4 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • 2015 Research-status Report
  • Research Products

    (7 results)

All 2018 2017 2016 2015

All Journal Article (2 results) (of which Peer Reviewed: 1 results,  Open Access: 1 results,  Acknowledgement Compliant: 1 results) Presentation (5 results) (of which Int'l Joint Research: 1 results)

  • [Journal Article] The Chemical Characterization of Iron and Steel Objects from Kaman-Kalehoyuk2017

    • Author(s)
      Mariya Masubuchi
    • Journal Title

      Anatolian Archaeological Studies

      Volume: 20 Pages: 51-62

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] A Study on the Beginning of the Iron Age at Kaman-Kalehöyük2016

    • Author(s)
      Mariya MASUBUCHI
    • Journal Title

      Anatolian Archaeological Studies

      Volume: 19 Pages: 111-122

    • Related Report
      2015 Research-status Report
  • [Presentation] 中央アナトリアにおける製鉄文化解明の試み(9)-カマン・カレホユックでこれまでに発見された炉址・金属工房址について-2018

    • Author(s)
      増渕麻里耶
    • Organizer
      第28回トルコ調査研究会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 中央アナトリアにおける製鉄文化解明の試み(8)-放射光を用いた鉄製品の組成分析と非破壊観察方法の開発-2017

    • Author(s)
      増渕麻里耶
    • Organizer
      第27回トルコ調査研究会
    • Place of Presentation
      学習院大学創立百周年記念会館
    • Year and Date
      2017-03-05
    • Related Report
      2016 Research-status Report
  • [Presentation] An Archaeometallurgical Study of Iron/Steel Objects from Kaman-Kalehoyuk in Central Anatolia2017

    • Author(s)
      Mariya MASUBUCHI
    • Organizer
      The 9th International Conference on the Beginning of the Use of Metals and Alloys (BUMA-IX)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 中央アナトリアにおける製鉄文化解明の試み(7)-鉄製品の化学組成からの考察-2016

    • Author(s)
      増渕麻里耶
    • Organizer
      第26回トルコ調査研究会
    • Place of Presentation
      学習院大学
    • Year and Date
      2016-02-29
    • Related Report
      2015 Research-status Report
  • [Presentation] 中央アナトリア、カマン・カレホユック出土鉄製品に見るヒッタイト崩壊前後の鉄器文化の変容2015

    • Author(s)
      増渕麻里耶、大村幸弘
    • Organizer
      日本西アジア考古学会
    • Place of Presentation
      名古屋大学
    • Year and Date
      2015-06-13
    • Related Report
      2015 Research-status Report

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Published: 2015-04-16   Modified: 2019-03-29  

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