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Effect of Single Crystal Nano-Structured Thin Layer on Nano-Surface Integrity

Research Project

Project/Area Number 16206015
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Production engineering/Processing studies
Research InstitutionTokyo University of Agriculture and Technology

Principal Investigator

FURUKAWA Yuji  Tokyo University of Agriculture and Technology, Graduate School of Technology Management, Professor, 大学院技術経営研究科, 教授 (10087190)

Co-Investigator(Kenkyū-buntansha) SASAHARA Hiroyuki  Tokyo University of Agriculture and Technology, Institute of Symbiotic Agriculture and Technology, Associate Professor, 大学院共生科学技術研究院, 助教授 (00205882)
MIN Yan  Tokyo Metropolitan University, Department of Systems Design Engineering, Professor, 大学院工学研究科, 教授 (90240142)
KAKUTA Akira  Tokyo Metropolitan University, Department of Systems Design Engineering, Research Associate, システムデザイン学部, 助手 (60224359)
韓 玉傑  国立大学法人東京農工大学, 大学院・共生科学技術研究部, 助手 (80372457)
Project Period (FY) 2004 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥46,930,000 (Direct Cost: ¥36,100,000、Indirect Cost: ¥10,830,000)
Fiscal Year 2006: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
Fiscal Year 2005: ¥4,940,000 (Direct Cost: ¥3,800,000、Indirect Cost: ¥1,140,000)
Fiscal Year 2004: ¥39,000,000 (Direct Cost: ¥30,000,000、Indirect Cost: ¥9,000,000)
KeywordsSilicon Carbonate (SiC) / thin layer / surface integrity / nano structure / epitaxy / MEMS / indentation / YAG laser / サーフェスインテグリティー / Sic
Research Abstract

Systematization of formation methods of SiC thin layer and SiC nano-structured layer
As a molecule supplying method of Molecular Beam Epitaxy, three kinds for Silicon(Si), namely, Electron Beam gun, Knoodsen Cell and Helicon sputtering, and two kinds for Carbon(C), namely, Acetylene gas and Electron Beam sputtering have been developed respectively. Any two combination of Si and C could generate crystal growth of Silicon Carbonate(SiC), among which the better single crystal SiC could be obtained when supplying C by Acetylene gas and sputtering Si, and firstly, a carbonated layer is prepared on Silicon single crystal substrate under about 900 ℃in order to adjust lattice difference between Si and SiC, then accumulate SiC gradually.
Chemical composition of SiC layer and SiC nano-structured surface
It was clarified by analysis of XPS that the eitaxially grown SiC layer consists of about 50% Si and 50% C, and its basic electric characteristics were verified.
Method to generate micro structure on … More single crystal SiC
Micro grooves in a size of several nm width and several ten nm depth could be formed by applying YAG laser machining systems.
Nano surface integrity of single crystal Silicon layer and nano structured layer
Nano order hardness and adhesive characteristic of the generated SiC layers have been tested by applying Atomic Force Microscope and it was evaluated that these characteristics relate either of tested depth and surface integrity, and these results could be fundamentals of a theoretical analysis. In addition, an effect of nano structure and chemical composition on surface integrity was experimentally clarified and systematized comparing nano structure with its chemical composition of specimen.
Preparation of data file to select an optimal machining condition
Many parameters and data concerned with Si substrate, epitaxy growth conditions of SiC mono-layer, laser machining, and surface nano integrity, etc. have been arranged and systematized so as to correspond to the purpose of application of SiC mono layer and SiC nano structured surface to MEMS/NEMS surfaces. Less

Report

(4 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • 2004 Annual Research Report
  • Research Products

    (43 results)

All 2006 2005 2004

All Journal Article (42 results) Patent(Industrial Property Rights) (1 results)

  • [Journal Article] Principle Factors Affecting on Sub Micro Grooving Mechanism of SiC Thin Layer by 355 nm UV Laser2006

    • Author(s)
      Y.Furukawa, H.Sasahara, A.Kakuta, K.Chuma
    • Journal Title

      Annals of the CIRP 54, No. 1

      Pages: 537-576

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] 炭化による単結晶Si微細構造の表面改質とその応用に関する研究2006

    • Author(s)
      高岡勝則, 諸貫信行, 角田陽
    • Journal Title

      精密工学会春季大会学術講演論文集

      Pages: 389-390

    • NAID

      130005027383

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary 2005 Annual Research Report
  • [Journal Article] UVレーザによる石英ガラスの加工2006

    • Author(s)
      古市卓也, 笹原弘之, 古川勇二
    • Journal Title

      2006年度精密工学会春季大会学術講演会講演論文集

      Pages: 1223-1224

    • NAID

      130005027200

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary 2005 Annual Research Report
  • [Journal Article] 355UVレーザによるSiC薄膜層のマイクロチャンネル創成2006

    • Author(s)
      中馬 健一朗, 角田 陽, 笹原 弘之, 古川 勇二
    • Journal Title

      2006年度精密工学会春季大会学術講演会講演論文集

      Pages: 1221-1222

    • NAID

      130005027199

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Single crystal SiC thinfilm produced by epitaxial growth and its application to micro-mechanical devices2006

    • Author(s)
      N.Moronuki, M.Kojima, A.Kakuta
    • Journal Title

      Int. Conf. Precision Engineering Vol. 11

      Pages: 203-207

    • NAID

      120006558394

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Nanometer Deflection Control of AFM Probe by Irradiating Polarized Laser and its Application to Nano-Structuring Process2006

    • Author(s)
      D.Mezaki, K.Chuma, A.Kakuta, Y.Furukawa
    • Journal Title

      Int. Conf. Precision Engineering Vol. 11

      Pages: 203-207

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Principle Factors Affecting on Sub Micro Grooving Mechanism of SiC Thin Layer by 355 nm UV Laser2006

    • Author(s)
      Y.Furukawa, H.Sasahara, A.Kakuta, K.Chuma
    • Journal Title

      Annals of the CIRP 54, No.1

      Pages: 537-576

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Improvement of surface integrity of single crystal Silicon micro structure by carbonization process2006

    • Author(s)
      K.Takaoka, N.Moronuki, A.Kakuta
    • Journal Title

      Proc.Jap.Soc.Prec.Eng.2006(Spring)

      Pages: 389-390

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] A study on precise machining quarts glass assisted by UV laser2006

    • Author(s)
      T.Furuichi, H.Sasahara, Y.Fukukawa
    • Journal Title

      Proc.Jap.Soc.Prec.Eng.2006(Spring)

      Pages: 1223-1224

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Generation of micro channels onto SiC thin layer assisted by 355 nm UV laser2006

    • Author(s)
      K.Chuma, A.Kakuta, H.Sasahara, Y.Furukawa
    • Journal Title

      Proc.Jap.Soc.Prec.Eng.2006(Spring)

      Pages: 1221-1222

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Single crystal SiC thinfilm produced by epitaxial growth and its application to micro-mechanical devices2006

    • Author(s)
      N.Moronuki, M.Kojima, A.Kakuta
    • Journal Title

      Int.Conf.Precision Engineering vol.11

      Pages: 203-207

    • NAID

      120006558394

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Nanometer Deflection Control of AFM Probe by Irradiating Polarized Laser and its Application to Nano-Structuring Process2006

    • Author(s)
      D.Mezaki, K.Chuma, A.Kakukta, Y.Furukawa
    • Journal Title

      Int.Conf.Precision Engineering Vol.11

      Pages: 203-207

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] UVレーザによる石英ガラスの加工2006

    • Author(s)
      古市卓也, 笹原弘之, 古川勇二
    • Journal Title

      精密工学会春季大会学術講演会講演論文集 2006-3

      Pages: 1223-1224

    • NAID

      130005027200

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Single crystal SiC thinfilm produced by epitaxial growth and its application to micro-mechanical devices2006

    • Author(s)
      N.Moronuki, M.Kojima, A.Kakuta
    • Journal Title

      Proc. 3rd International Conference on Technological Advances in Thin Films & Surface Coatings (CD-ROM形式)

    • NAID

      120006558394

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Nanometer Deflection Control of AFM Probe by Irradiating Polarized Laser and its Application to Nano-Structuring Process2006

    • Author(s)
      D.Mezaki, K.Chuma, A.Kakuta, Y.Furukawa
    • Journal Title

      Int. Conf. Precision Engineering Vol.11

      Pages: 203-207

    • Related Report
      2006 Annual Research Report
  • [Journal Article] 355 UVレーザによるSiC薄膜層のマイクロチャンネル創成2006

    • Author(s)
      中馬 健一朗, 角田 陽, 笹原 弘之, 古川 勇二
    • Journal Title

      2006年度精密工学会春季大会学術講演会講演論文集

      Pages: 1221-1222

    • NAID

      130005027199

    • Related Report
      2005 Annual Research Report
  • [Journal Article] The Effect on Fatigue Life of Residual Stress and Surface Hardness resulting from Different Cutting Conditions of 0.45%C Steel2005

    • Author(s)
      Hiroyuki SASAHARA
    • Journal Title

      International Journal of Machine Tools and Manufacture 45, 2

      Pages: 131-136

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Nanopillar formation via defect activation and Coulomb explosion initiated by a 355 nm Nd : YAG laser beam2005

    • Author(s)
      Yujie Han, Yuji Furukawa
    • Journal Title

      The Annals for Micro and Nano Systems 2005-6

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] エピタキシャル成長における3次元島形成を利用したナノテクスチャ創成に関する研究2005

    • Author(s)
      金子新, 藤山孝太郎, 角田陽, 諸貫信行, 古川勇二
    • Journal Title

      精密工学会誌 Vol. 71, No. 6

      Pages: 744-749

    • NAID

      110001824179

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] 単結晶SiC薄膜の製作と微小構造材料への適用2005

    • Author(s)
      諸貫信行, 角田陽, 高岡勝則
    • Journal Title

      精密工学会誌 Vol. 71, No. 9

      Pages: 1146-1150

    • NAID

      110001794643

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] 分子線エピタキシによるSiC/Si多層薄膜構造の創成と応用2005

    • Author(s)
      土井光人, 諸貫信行, 角田陽
    • Journal Title

      精密工学会2005年度春季大会学術講演論文集 2005

      Pages: 103-104

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary 2004 Annual Research Report
  • [Journal Article] A Study on Surface Integrity ofSiC/Si Hybrid Nano-Structured Surfaces2005

    • Author(s)
      Kenichiro CHUMA, Yuji FURUKAWA, Yujie HAN, Akira KAKUTA
    • Journal Title

      Int. Conf. on Leading Edge Manufacturing in 21^<St> century Vol. 1

      Pages: 1199-1204

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] エピタキシャル成長単結晶SiC薄膜の機械的特性に関する研究2005

    • Author(s)
      小島正行, 諸貫信行, 角田陽
    • Journal Title

      精密工学会秋季大会学術講演論文集

      Pages: 107-108

    • NAID

      130004656685

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary 2005 Annual Research Report
  • [Journal Article] Nano texturing process assisted by 3 dimensional growth of micro island in Epitaxy growth2005

    • Author(s)
      S.Kaneko, K.Fujiyama, A.Kakuta, N.Moronuki, Y.Furukawa
    • Journal Title

      Trans.Jap.Soc.Prec.Eng. Vol.71, No.6

      Pages: 744-749

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Fabrication of Single Crystal SiC thinfilm and its application to micro-structure material2005

    • Author(s)
      N.Moronuki, A.Kakuta, K.Takaoka
    • Journal Title

      Trans.Jap.Soc.Prec.Eng. Vol.71, No.9

      Pages: 1146-1150

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Generation of multi thin layers of SiC/Si by Molecular Beam Epitaxy and its application2005

    • Author(s)
      M.Doi, N.Moronuki, A.Kakuta
    • Journal Title

      Proc.Jap.Soc.Prec.Eng.2005(Spring)

      Pages: 103-104

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] A Study of Surface Integrity of SiC/Si Hybrid Nano-Structured Surfaces2005

    • Author(s)
      Kenichiro CHUMA, Yuji FURUKAWA, Yujie HAN. Akira KAKUTA
    • Journal Title

      Int.Conf.on Leading Edge Manufacturing in 21^<st> century vol.1

      Pages: 1199-1204

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Mechanical properties of single crystal Silicon Carbonate thin layer grown by Molecular Beam Epitaxy2005

    • Author(s)
      M.Kojima, N.Moronuki, A.Kakuta
    • Journal Title

      Proc.Jap.Soc.Prec.Eng.2005(Autumn)

      Pages: 107-108

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] エピタキシャル成長における3次元島形成を利用したナノテクスチャ創成に関する研究2005

    • Author(s)
      金子新, 藤山孝太郎, 角田陽, 諸貫信行, 古川勇二
    • Journal Title

      精密工学会誌 Vol.71,No.6

      Pages: 744-749

    • NAID

      110001824179

    • Related Report
      2005 Annual Research Report
  • [Journal Article] 単結晶SiC薄膜の製作と微小構造材料への適用2005

    • Author(s)
      諸貫信行, 角田陽, 高岡勝則
    • Journal Title

      精密工学会誌 Vol.71,No.9

      Pages: 1146-1150

    • NAID

      110001794643

    • Related Report
      2005 Annual Research Report
  • [Journal Article] A Study on Surface Integrity of SiC/Si Hybrid Nano-Structured Surfaces2005

    • Author(s)
      Kenichiro CHUMA, Yuji FURUKAWA, Yujie HAN, Akira KAKUTA
    • Journal Title

      Int.Conf.on Leading Edge Manufacturing in 21^<st> century Vol.1

      Pages: 1199-1204

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Nanopillar formation via defect activation and Coulomb explosion initiated by a 355 nm Nd:YAG laser beam2005

    • Author(s)
      Yujie Han, Yuji Furukawa
    • Journal Title

      The Annals for Micro and Nano System 2005-6(未定)

    • Related Report
      2004 Annual Research Report
  • [Journal Article] The Effect on Fatigue Life of Residual Stress and Surface Hardness resulting from Different Cutting Conditions of 0.45%C Steel2005

    • Author(s)
      Hiroyuki SASAHARA
    • Journal Title

      International Journal of Machine Tools and Manufacture 45,2

      Pages: 131-136

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Effect of Chemical Composition upon Mechanical Properties of Thin Layered Mono-Crystal SiC2004

    • Author(s)
      A.KAKUTA, Y.FURUKAWA
    • Journal Title

      Annals of the CIRP 53, No. 1

      Pages: 467-470

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Development of the CAE-assisted Nano-indentation Method for the Evaluation of the Anisotropic Mechanical-properties of Thin Films2004

    • Author(s)
      T.SASAKI, M.YANG, S.FUKUSHIMA, R.TSUKANO
    • Journal Title

      Journal of Materials Processing Technology 151, No. 1-3

      Pages: 263-267

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Measuring the Fatigue Properties of Thin Films2004

    • Author(s)
      J.M.CAIRNEY, R.TSUKANO, M.YANG, M.J.HOFFMAN
    • Journal Title

      Proc. of Thin Films 2004 & Nanotech 2004 2004-1

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Effect of Chemical Composition upon Mechanical Properties of Thin Layered Mono-Crystal SiC2004

    • Author(s)
      A.KAKUTA, Y.FURUKAWA
    • Journal Title

      Annals of the CIRP 53, No.1

      Pages: 467-470

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Development of the CAE-assisted Nano-indentation Method for the Evaluation of the Anisotropic Mechanical-properties of Thin Films2004

    • Author(s)
      T.SASAKI, M.YANG, S.FUKUSHIMA, R.TSUKANO
    • Journal Title

      Journal of Materials Processing Technology 151, No.1-3

      Pages: 263-267

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Measuring the Fatigue Properties of Thin Films2004

    • Author(s)
      J.M.CAIRNEY, R.TSUKANO, M.YANG, M.J.HOFFMAN
    • Journal Title

      Proc.of Thin Films 2004 & Nanotech 2004 2004-1

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Effect of Chemical Composition upon Mechanical Properties of Thin Layered Mono-Crystal SiC2004

    • Author(s)
      A.KAKUTA, Y.FURUKAWA
    • Journal Title

      Annals of the CIRP 53,No.1

      Pages: 467-470

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Measuring the Fatigue Properties of Thin Films2004

    • Author(s)
      J.M.CAIRNEY, R.TSUKANO, M.YANG, M.J.HOFFMAN
    • Journal Title

      Proc.of Thin Films 2004 & Nanotech 2004 2004-1

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Development of the CAE-assisted Nano-indentation Method for the Evaluation of the Anisotropic Mechanical-properties of Thin Films2004

    • Author(s)
      T.SASAKI, M.YANG, S.FUKUSHIMA.R.TSUKANO
    • Journal Title

      Journal of Materials Processing Technology 151,No.1-3

      Pages: 263-267

    • Related Report
      2004 Annual Research Report
  • [Patent(Industrial Property Rights)] マイクロアクチュエーターシステム2006

    • Inventor(s)
      古川勇二, 中馬健一郎, 目崎大輔
    • Industrial Property Rights Holder
      東京農工大学
    • Industrial Property Number
      2006-220513
    • Filing Date
      2006-08-11
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary

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Published: 2004-04-01   Modified: 2016-04-21  

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