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Development of atmosphere controlled Tribotester and evaluation of tribological properties of hard thin films nanostructured with femtosecond laser

Research Project

Project/Area Number 16360059
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionFukui National College of Technology

Principal Investigator

KOMAI Kenjiro  Fukui National College of Technology, President, 校長 (70025948)

Co-Investigator(Kenkyū-buntansha) YASUMARU Naoki  Fukui National College of Technology, Mechanical Engineering, Professor, 機械工学科, 教授 (90158006)
KATO Hirotaka  Fukui National College of Technology, Mechanical Engineering, Professor, 機械工学科, 教授 (30311020)
粉川 良平  島津製作所, 分析計測事業部, プロダクトマネージャー
Project Period (FY) 2004 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥15,200,000 (Direct Cost: ¥15,200,000)
Fiscal Year 2006: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 2005: ¥3,800,000 (Direct Cost: ¥3,800,000)
Fiscal Year 2004: ¥10,300,000 (Direct Cost: ¥10,300,000)
Keywordsfemtosecond laser / ablation / hard thin film / DLC / nanostructure / scanning probe microscope / tribology / トライポロジー特性
Research Abstract

We report tribological properties of diamond-like carbon (DLC) film of which surface has been nanostructured with femtosecond (fs) laser pulses. A broad area on the DLC surface was nanostructured using a precise target-scan system developed for the fs-laser processing. In the present experiment we have developed two types of laser scan. One is a parallel scan to produce a uniformly nanostructured surface. The other is a crossed scan along a net-like pattern to form a partially nanostructured area on the surface. The results obtained are summarized as follows.
1)The nanostructure has been formed uniformly on the DLC surface over the area of 15 x 15 mm^2.
2)The structured surface at E = 110 μJ near the ablation threshold is uniformly modified to the GC layer.
3)The friction coefficient of the structured DLC film has shown a small decrease for the steel ball but a small increase for the ceramic WC-Co ball.
4)A large improvement of the friction coefficient of the DLC surface has been achieved by coating the MoS_2 layer on the nanostructured DLC surface. The measured friction coefficients μ of the surface were 0.07 with the steel ball and 0.02 - 0.04 with the WC-Co ball.
5)The net-like patterning of the ablated zone created by the crossed scan produces an effective method to increase μ, maintaining the initial surface flatness.
6)The nano-indentation test and nano-scratch test(100〜2000μN) indicate that the laser-treated surface layer modified to GC becomes soft and its friction coefficient increases as compared with that of the untreated DLC.

Report

(4 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • 2004 Annual Research Report
  • Research Products

    (29 results)

All 2007 2006 2005 2004

All Journal Article (29 results)

  • [Journal Article] Tribological Properties of Diamond-Like Carbon Films with Surface Nano-Structure Formed by Femtosecond Laser Pulses2007

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuchi, K.Komai
    • Journal Title

      J. of Laser Micro/Nanoengineering (to be published)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Tribofilm Formation and Mild Wear by Tribo-Sintering of Nanometer-Sized Oxide Particles on Rubbing Steel Surfaces2007

    • Author(s)
      H.Kato, K.Komai
    • Journal Title

      Wear Vol. 262

      Pages: 36-41

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Tribofilm Formation and Mild Wear by Tribo-Sintering of Nanometer-Sized Oxide Particles on Rubbing Steel Surfaces2007

    • Author(s)
      H.Kato, K.Komai
    • Journal Title

      Wear Vol.262

      Pages: 36-41

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Tribofilm Formation and Mild Wear by Tribo-Sintering of Nanometer-Sized Oxide Particles on Rubbing Steel Surgfaces2007

    • Author(s)
      H.Kato, K.Komai
    • Journal Title

      Wear Vol.262

      Pages: 36-41

    • Related Report
      2006 Annual Research Report
  • [Journal Article] 硬質薄膜のフェムト秒レーザープロセシングとトライボロジー特性2006

    • Author(s)
      駒井謙治郎, 安丸尚樹, 宮崎健創, 木内淳介
    • Journal Title

      日本機械学会2006年度年次大会講演論文集 (1)

      Pages: 531-532

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Wear of Tribofilms Produced by Tribo-Sintering of Nanometer-Sized Particles on Rubbing Surfaces2006

    • Author(s)
      H.Kato, K.Komai
    • Journal Title

      Proc. of Asiatrib 2006

      Pages: 841-842

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] フェムト秒レーザーによる硬質薄膜の微細加工2006

    • Author(s)
      安丸尚樹, 宮崎健創, 木内淳介, 駒井謙治郎
    • Journal Title

      第3回マイクロマテリアルシンポジウム講演論文集

      Pages: 45-49

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] フェムト秒レーザー加工DLC薄膜のトライボロジー特性2006

    • Author(s)
      駒井謙治郎, 山口光弘, 安丸尚樹, 宮崎健創, 木内淳介
    • Journal Title

      日本材料学会2006年度年次大会講演論文集 (1)

      Pages: 417-418

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Femtosecond Laser Processing of Hard Thin Films and Control of Tribological Characteristics2006

    • Author(s)
      K.Komai, N.Yasumaru, K.Miyazaki, J.Kiuchi
    • Journal Title

      Proceed. of the Mechanical Engineering Congress, 2006 Japan (MECJ-06) Vol.1

      Pages: 531-532

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Wear of Tribofilms Produced by Tribo-Sintering of Nanometer-Sized Particles on Rubbing Surfaces2006

    • Author(s)
      H.Kato, K.Komai
    • Journal Title

      Proceed. of Asiatrib 2006

      Pages: 841-842

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Microstructuring of Hard Thin Films with Femtosecond Laser Pulses2006

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuchi, K.Komai
    • Journal Title

      Proceed. of The 3^<rd> Symposium on Micromaterials

      Pages: 45-49

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Tribology of DLC Films Formed by Femtosecond Laser Pulses2006

    • Author(s)
      K.Komai, M.Yamaguchi, N.Yasumaru, K.Miyazaki, J.Kiuchi
    • Journal Title

      Proceed. of the Annual Congress for The Society of Materials Science, 2006 Japan Vol.1

      Pages: 417-418

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Tribological Properties of Diamond-Like Carbon Films with Surface Nano-Structure Formed by Femtosecond Laser Pulses2006

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuchi, K.Komai
    • Journal Title

      Proceed. of the International Congress on Laser Advanced Materials Processing (LAMP2006) #WeP20

      Pages: 1-4

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] 硬質薄膜のフェムト秒レーザープロセシングとトライボロジー特性2006

    • Author(s)
      駒井謙治郎, 安丸尚樹, 宮崎健創, 木内淳介
    • Journal Title

      日本機械学会2006年度年次大会講演論文集(1)

      Pages: 531-532

    • Related Report
      2006 Annual Research Report
  • [Journal Article] フェムト秒レーザー加工DLC薄膜のトライボロジー特性2006

    • Author(s)
      駒井謙治郎, 山口光弘, 安丸尚樹, 宮崎健創, 木内淳介
    • Journal Title

      日本材料学会2006年度年次大会講演論文集(1)

      Pages: 417-418

    • Related Report
      2006 Annual Research Report
  • [Journal Article] フェムト秒レーザーによりナノ構造が形成されたDLC薄膜のトライボロジー特性2006

    • Author(s)
      山口光弘, 安丸尚樹, 駒井謙治郎, 宮崎健創, 木内 淳介
    • Journal Title

      日本機械学会北陸信越学生会第35回学生員卒業研究発表講演会

      Pages: 187-188

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Fluence dependence on femtosecond-laser-induced nanostructure formed on TiN and CrN2005

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuchi
    • Journal Title

      Appl.Phys.A Vol.81

      Pages: 933-937

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] フェムト秒レーザーによるナノ加工と次世代トライボロジー制御技術2005

    • Author(s)
      安丸尚樹, 宮崎健創, 木内淳介
    • Journal Title

      福井県地域結集型共同研究事業最終成果発表会

      Pages: 13-14

    • Related Report
      2005 Annual Research Report
  • [Journal Article] フェムト秒レーザーによる硬質薄膜表面のナノ構造形成と制御2005

    • Author(s)
      安丸尚樹, 宮崎健創, 木内淳介
    • Journal Title

      レーザー研究(レーザー解説小特集号「フェムト秒レーザーによるナノアブレーション」) 33巻・8号

      Pages: 519-524

    • NAID

      10029621797

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Fluence dependence on femtosecond-laser-induced nanostructure formed on TiN and CrN2005

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuchi
    • Journal Title

      Applied Physics A ; Materials Science & Processing 81巻

      Pages: 933-937

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Production of Tribofilms and Mild Wear by Tribo-Sintering of Nanoparticles on Rubbing Surfaces2005

    • Author(s)
      H.Kato
    • Journal Title

      Synopses of Int.Tribology Conf.

      Pages: 63-63

    • Related Report
      2005 Annual Research Report
  • [Journal Article] 硬質薄膜のフェムト秒レーザープロセシング2005

    • Author(s)
      松村浩司, 安丸尚樹, 駒井謙治郎, 宮崎健創
    • Journal Title

      日本機械学会北陸信越学生会第34回学生員卒業研究発表講演会

      Pages: 39-40

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Fluence dependence on femtosecond-laser-induced nanostructure formed on TiN and CrN2005

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuchi
    • Journal Title

      Applied Physics A ; Materials Science & Processing (印刷中)

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Production of tribofilms and mild wear by tribo-sintering of nanoparticles on rubbing surfaces2005

    • Author(s)
      H.Kato
    • Journal Title

      International Tribology Conference, Kobe, 2005

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Glassy carbon layer formed in diamond-like carbon films with femtosecond laser pulses2004

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuch
    • Journal Title

      Appl.Phys.A Vol.78

      Pages: 425-427

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Influence of water absorption on the pull-out behavior of aramid/epoxy model composite2004

    • Author(s)
      K.Tanaka, K.Minoshima, W.Grela, K.Komai
    • Journal Title

      Proceed. of the 12th International Conf. on Experimental Mechanics (ICEM12)

      Pages: 1-8

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Influence of water absorption on the pull-out behavior of aramid/epoxy model composite2004

    • Author(s)
      K.Tanaka, K.Minoshima, W.Grela, K.Komai
    • Journal Title

      Proced.of the 12^<th> International Conf.on Experimental Mechanics

      Pages: 89-90

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Glassy carbon layer formed in diamond-like carbon films with femtosecond laser pulses2004

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuchi
    • Journal Title

      Applied Physics A ; Materials Science & Processing 78

      Pages: 425-427

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Nanoscale modification of DLC film surfaces with femtosecond laser pulses2004

    • Author(s)
      N.Yasumaru, K.Miyazaki, J.Kiuchi, H.Magara
    • Journal Title

      Proceedings of SPIE 5662

      Pages: 755-759

    • Related Report
      2004 Annual Research Report

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Published: 2004-04-01   Modified: 2016-04-21  

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