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In-situ TEM observation of nano-dynamics to point defects in crystals by a ultra high-speed CCD camera

Research Project

Project/Area Number 16360310
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Physical properties of metals
Research InstitutionHokkaido University

Principal Investigator

SHIBAYAMA Tamaki  Hokkaido Univ., Center for Advanced Research of Energy Conversion Materials, Assoc Prof., エネルギー変換マテリアル研究センター, 助教授 (10241564)

Co-Investigator(Kenkyū-buntansha) KINOSHITA Hiroshi  Hokkaido Univ., Grad.School of Eng., Inst., 大学院工学研究科, 助手 (40177895)
SAKAGUCHI Norihito  Hokkaido Univ., Center for Advanced Research of Energy Conversion Materials, Assoc Prof, エネルギー変換マテリアル研究センター, 助教授 (70344489)
ETOH Takeharu  Kinki Univ., School of Science and Engineering, Prof., 理工学部, 教授 (20088412)
Project Period (FY) 2004 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥6,900,000 (Direct Cost: ¥6,900,000)
Fiscal Year 2006: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 2005: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 2004: ¥4,700,000 (Direct Cost: ¥4,700,000)
Keywordsultra high speed / TEM / nano sized materials / interface / irradiation effects / joining / point defects / composites / 透過電子顕徴鏡 / TEM / 検出器 / 高速カメラ / 高分解能 / 動的観察 / 時間分解能
Research Abstract

In 2006, We investigated nano dynamics about irradiation defects and crack propagation of SiC/SiC composite material by a high-speed camera. Furthermore, we summarized results of in-situ TEM observation in the past three years. Accomplishment of our original purpose may be reached up to 70%, but it is thought that I clarified the purpose of this study enough. In addition, development of a pulse electron source of light to be based on a new idea by pulsed laser irradiation to a target in Germany, and to generate the electron which was high strength was done. The new electron microscope which they improved this electronic source and changed for electron gun of a normal electron microscope was developed in U.S.A., and it was reported in an international microscope congress held in Sapporo in September, 2006. Because a study was already made about some topics of materials science, and there were word of mouth and announcement with a poster, positioning of international of this study became clear. In this study, we used a general thermo electron source and a field emission electron source, however, for the American device, a pulsed electron source used. We aimed to record a series of events by a high speed CCD camera, but American team aimed to record an each phenomenon by a pulsed electron source as a strobe image to understand a series of high speed phenomena. However, it was advantage in our method to know the initiation of a certain phenomenon, and future development was expected in the above conference. We explored a new research field in this study and we will continue it in future and should be able to go ahead through a new project as mentioned above. In addition, because new issues were found through this study for the past three years, could reflect for the next project.

Report

(4 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • 2004 Annual Research Report
  • Research Products

    (43 results)

All 2007 2006 2005 2004

All Journal Article (39 results) Book (4 results)

  • [Journal Article] Present status of beryllides for fusion and industrial application in Japan2007

    • Author(s)
      Y.Mishima, N.Yoshida, H.Takahashi, K.Ishida, H.Kawamura, T.Iwadachi, T.Shibayama, I.ohnuma, Y.Sato, K.Munakata, H.Iwakiri, M.Uchida
    • Journal Title

      Fusion Engineering and Designe 82

      Pages: 91-97

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Morphological investigations of disaccharide molecules for growth inhibition of ice crystals2007

    • Author(s)
      T.Uchida, M.Nagayama, T.Shibayama, K Gohara
    • Journal Title

      Journal of Crystal Grwoth 299

      Pages: 125-135

    • NAID

      120001117240

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Present status of beryllides for fusion and industrial' application in Japan2007

    • Author(s)
      Y.Mishima, N.Yoshida, H.Takahashi K.Ishida, H.Kawamura, T.Iwadachi, T.Shibayama, I.ohnuma, Y.Sato, K.Munakata, H.Iwakiri, M.Uchida
    • Journal Title

      Fusion Engineering and Design 82

      Pages: 91-97

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Morphological investigations of disaccharide molecules for growth inhibition of ice crystals2007

    • Author(s)
      T.Uchida, M.Nagayama, T.Shibayama, K.Ohara
    • Journal Title

      Journal of Crystal Growth 299

      Pages: 125-135

    • NAID

      120001117240

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Morphological investigations of disaccharide molecules for growth inhibition of ice crystals2007

    • Author(s)
      T.Uchida, M.Nagayama, T.Shibayama, K Gohara
    • Journal Title

      Journal of Crystal Growth 299

      Pages: 125-135

    • NAID

      120001117240

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Growth structure and growth defects in pulsed laser deposited Cr-CrN_x-CrC_xN<1-x> multilayer coatings2006

    • Author(s)
      J.M.Lackner, W.Waldhauser, B.Major, J.Morgiel, L.Major, H.Takahashi, T.Shibayama
    • Journal Title

      Surface and Coatings Technology 200・11

      Pages: 3644-3649

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Photochemical fine-Tuning of Luminescent Color of Cadmium Selenide Nanoparticles : Fabricating a Single-Source Multicolor Luminophore2006

    • Author(s)
      T.Torimoto, S.Murakami, M.Sakuraoka, K.Iwasaki, K.Okazaki, T.Shibayama, B.Ohtani
    • Journal Title

      J. Phys. Chem. B 110

      Pages: 13314-13318

    • NAID

      120005228745

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Fabrication of Jingle-Bell-Shaped Core-Shell Nanoparticulate Films and Molecular-Size-Responsive Photoluminescence Quenching of Cadmium Sulfide Cores2006

    • Author(s)
      K.Iwasaki, T.Torimoto, T.Shibayama, T.Nishikawa, B.Ohtani
    • Journal Title

      Small 2

      Pages: 854-858

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Effect of irradiation on microstructural damage in the welded portion of a SUS304 weldment2006

    • Author(s)
      D.S.Bae, S.K.Kim, S.P.Lee, H.Kinoshita, T.Shibayama, H.Takahashi
    • Journal Title

      Fusion Engineering and Design 81

      Pages: 969-974

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Annual Research Report 2006 Final Research Report Summary
  • [Journal Article] Growth structure and growth defects in pulsed laser deposited Cr-CrN_x-CrC_xN_<1-x> multilayer coatings2006

    • Author(s)
      J.M.Lackner, W.Waldhauser, B.Major, J.Morgiel, L.Major, H.Takahashi, T.Shibayama
    • Journal Title

      Surface and Coatings Technology 200(11)

      Pages: 3644-3649

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Photochemical fine-Tuning of Luminescent Color of Cadmium Selenide Nanoparticles : Fabricating a Single-Source Multicolor Luminophore2006

    • Author(s)
      Tsukasa Torimoto, Shin-ya Murakami, Miwa Sakuraoka, Kentaro Iwasaki, Ken-ichi Okazaki, Tamaki Shibayama, Bunsho Ohtani
    • Journal Title

      J.Phys.Chem.B 110

      Pages: 13314-13318

    • NAID

      120005228745

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Effect of irradiation, on microstructural damage in the welded portion of a SUS304 weldment2006

    • Author(s)
      D.S.Bae, S.K.Kim, S.P.Lee, H.Kinoshita, T.Shibayama, H.Takahashi
    • Journal Title

      Fusion Engineering and Design 81

      Pages: 969-974

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Growth structure and growth defects in pulsed laser deposited Cr-CrN_x- CrC_xN_<1-x> multilayer coatings2006

    • Author(s)
      J.M.Lackner, W.Waldhauser, B.Major, J.Morgiel, L.Major, H.Takahashi, T.Shibayama
    • Journal Title

      Surface and Coatings Technology 200・11

      Pages: 3644-3649

    • Related Report
      2006 Annual Research Report
  • [Journal Article] Fabrication of Jingle-Bell-Shaped Core-Shell Nanoparticulate Films and Molecular-Size-Responsive Photoluminescence Quenching of Cadmium Sulfide Cores2006

    • Author(s)
      K.Iwasaki, T.Torimoto, T.Shihayama, T.Nishikawa, B.Ohtani
    • Journal Title

      Small 2

      Pages: 854-858

    • Related Report
      2006 Annual Research Report
  • [Journal Article] An image sensor of 1,000,000 fps, 300,000 pixels, and 144 consecutive frames2005

    • Author(s)
      T.Goji Etoh, Y.Hatsuki, T.Okinaka, H.Ohtake, H.Maruyama, T.Hayashida, M.Yamada, K.Kitamura, T.Arai, K.Tanioka, D.Poggemann, A.Ruckelshausen, H.van Kujik, J.Bosiers, A.Theuwissen
    • Journal Title

      26^<th> International Congress on High-Speed Photography 5580

      Pages: 796-804

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] 「研究成果報告書概要(和文)」より2005

    • Author(s)
      S.T.Thoroddesen, T.G.Etoh, K.Takehara, N.Ootsuka
    • Journal Title

      Physics of Fluids 177

    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] An image sensor of 1,000,000 fps, 3000,000 pixels, and 144 consecutive frames2005

    • Author(s)
      T.Goji Etoh, Y.Hatsuki, T.Okinaka, H.Ohtaka, H.Maruyama, T.Hayashida, M.Yamada, K.Kitamura, T.Arai, K.Tanioka, D.Poggemann, A.Ruckelshausen, H.van Kujik, J.Bosiers, A.Theuwissen
    • Journal Title

      26th International Congress on High-Speed Photography 5580

      Pages: 796-804

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] On the coalescence speed of bubbles2005

    • Author(s)
      S.T.Thoroddesen, T.G.Rtoh, K.Takegara, N.Ootsuka
    • Journal Title

      Physics of Fluids 17

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Electron Microscopy of La_<0.7>Ca_<0.3>MnO_32005

    • Author(s)
      M.Arita, K.Hamada, A.Okada, H.Asano, M.Matsui, T.Shibayama
    • Journal Title

      Jpn.J.of Applied Physics 44

      Pages: 304-308

    • NAID

      10014322530

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Synthesis of Meta1-Cadmium Sulfide Nanocomposites Using Jingle-Bell-Shaped Core-She11 Photocatalyst Partides2005

    • Author(s)
      Pal, B., Torimoto, T., Iwasaki, K., Shibayama., Takahashi, H., Ohtani, B.
    • Journal Title

      J.Appl.Electrochem 35

      Pages: 751-756

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Photocatalytic Preparation of Encapsulated Gold Nanoparticles by Jingle-Bell-Shaped Cadmium Sulfide-Silica Nanoparticles2005

    • Author(s)
      Pal, B., Torimoto, T., Ikeda, S., Shibayama, T., Sugawara, K., Takahashi, H., Ohtani, B.
    • Journal Title

      Top.Catal. 35

      Pages: 321-325

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Animage Sensor of 1,000,000fps,3,000,000pixels, and 144 consecutive frames2005

    • Author(s)
      T.Goji Etoh, Y.Hatsuki, T.Okinaka, H.Maruyama, H.Ohtake, T.Hayashiba, M.Yamada, K.Kitamura, T.Arai, K.Tanioka, D.Poggemann, A.Ruckelshausen
    • Journal Title

      Proceedings of 26th International Congress on High Speed Photography and Photonics, SPIE 5580

      Pages: 153-162

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Plane and cross-sectional TEM observation to clarify the effect of damage region by ion implantation in austenitic 301 stainless steel2004

    • Author(s)
      Dwi Gustiono, N.Sakaguchi, T.Shibayama, H.Kinoshita, H.Takahashi
    • Journal Title

      Materials Transaction 45・1

      Pages: 65-68

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Effect of He-injected on Irradiation Damage in Heat Affected Zone of Welded SUS304 Steel2004

    • Author(s)
      Dong-Su Bae, H.Kinoshita, T.Shibayama, H.Takahashi
    • Journal Title

      Materials Transaction 45・1

      Pages: 59-64

    • NAID

      10011981626

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] A study of the formation of nanometer-scale cavities in helium-implanted 4H-SiC2004

    • Author(s)
      C.H.Zhang, S.E.Donnelly, V.M.Vishnyakov, J.H.Evans, T.Shibayama, Y.Sun
    • Journal Title

      Nuclear Instruments and Methods in Physics Research Section B : Beam Interactions With Materials and Atoms B218

      Pages: 53-60

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Preparation and Characterization of Water-Soluble Jingle-Bell-Shaped Silica-Coated Cadmium Sulfide Nanoparticles2004

    • Author(s)
      Kentaro Iwasaki, Tsukasa Torimoto, Tamaki Shibayama, Heishichiro Takahashi, Bunsho Ohtani
    • Journal Title

      The Journal of Physucal Chemistry B 32・108

      Pages: 11946-11952

    • NAID

      120005228747

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Size and Structure-Dependent Photocatalytic Activity of Jingle-Bell-Shaped Silica-Coated Cadmium Sulfide Nanoparticles2004

    • Author(s)
      B.Pal, T.Torimoto, K.Iwasaki, T.Shibayama, H.Takahashi, B.Ohtani
    • Journal Title

      J. Phys. Chem. B 108

      Pages: 18670-18674

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Effect of microstructure on oxidation resistance of MoSi2 fabricated by spark plasma sintering2004

    • Author(s)
      J.Kuchino, K.Kurokawa, T.Shibayama, H.Takahashi
    • Journal Title

      Vacuum 73

      Pages: 623-628

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Plane and cross-sectional TEM observation to clarify the effect of damage region by ion implantation in austenitic2004

    • Author(s)
      Dwi Gustiono, N.sakaguchi, T.Shibayama, H.Kinoshita, H.Takahashi
    • Journal Title

      Materials Transaction 45(1)

      Pages: 65-68

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Effect of He-injected on Irradiation Damage im Heat2004

    • Author(s)
      Dong-Su Bae, H.Kinoshita, T.Shibayama, H.Takahashi
    • Journal Title

      Materials Transaction 45(1)

      Pages: 59-64

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] A Study of the formation of nanometer-scale cavities in helium-implanted 4H-SiC2004

    • Author(s)
      C.H.Zhang, S.E..Donnelly, V.M.Vishnyakov, J.H.Evans, T.Shibayama, Y.Sun
    • Journal Title

      Nuclear Instruments and Methods in Physics Research Section B : Beam Interactions with Materials and Atoms B218

      Pages: 53-60

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Preparation and Characterization of Water-Soluble Jingle-Bell-Shaped silica-Coated Cadmium Sulfide2004

    • Author(s)
      Kentarou Iwasaki, Tsukasa Torimoto, Tamaki Shibayama, Heishichiro Tkahashi, Bunsho Ohtani
    • Journal Title

      The Journal of Physical Chemistry B 32(108)

      Pages: 11946-11952

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Size and Structure-Dependent Photo catalytic Activity of Jingle-Bell-Shaped Silica-Coated cadmium Sulfide2004

    • Author(s)
      B.Pal, T.Torimoto, K.Iwasaki, T.Shibayama, H.Takahashi, B.Ohtani
    • Journal Title

      J.Phys.Chem.B 108

      Pages: 18670-18674

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Nano-scale phase transformation in Ti-implanted austenitic 301 stainless steel2004

    • Author(s)
      Dwi.Gustiono, N.Sakaguchi, T.Shibayama, H.Kinoshita, Takahashi H
    • Journal Title

      Materials Transcation 45(1)

      Pages: 65-68

    • NAID

      10012549808

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Effect of He-injected on Irradiation Damage in Heat Affected Zone of Welded SUS304 Steel2004

    • Author(s)
      Dong-Su Bae, Hiroshi Kinoshita, Tamaki Shibayama, Heishichiro Takahashi
    • Journal Title

      Materials Transcation 45(1)

      Pages: 59-64

    • NAID

      10011981626

    • Related Report
      2004 Annual Research Report
  • [Journal Article] A study of the formation of nanometer-scale cavities in helium-implanted 4H-SiC2004

    • Author(s)
      C.H.Zhang, S.E.Donnelly, V.M.Vishnyakov, J.H.Evans, T.Shibayama, Y.M.Sun
    • Journal Title

      Nuclear Instruments and Methods in Physics Research Section B : Beam Interactions with Materials and Atoms B218

      Pages: 53-60

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Preparation and Characterization of Water-Soluble Jingle-Bell-Shaped Silica-Coated Cadmium Sulfide Nanoparticles2004

    • Author(s)
      Kentaro Iwasaki, Tsukasa Torimoto, Tamaki Shibayama, Heishichiro Takahashi, Bunsho Ohtani
    • Journal Title

      The Journal of Physical Chemistry B 32(108)

      Pages: 11946-11952

    • NAID

      120005228747

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Size and Structure-Dependent Photocatalytic Activity of Jingle-Bell-Shaped Silica-Coated Cadmium Sulfide Nanoparticles2004

    • Author(s)
      Bonamali Pal, Tsukasa Torimoto, Kentaro Iwasaki, Tamaki Shibayama, Heishichiro Takahashi, Bunsho Ohtani
    • Journal Title

      J.Phys.Chem B108

      Pages: 18670-18674

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Effect of microstructure on oxidation resistance of MoSi2 fabricated by spark plasma sintering2004

    • Author(s)
      Jyunichi Kuchino, Kazuya Kurokawa, Tamaki Shibayama, Heishichiro Takahashi
    • Journal Title

      Vacuum 73

      Pages: 623-628

    • Related Report
      2004 Annual Research Report
  • [Book] Introduction of the Advanced Nuclear Energy Technology in Fusion, Fuels and Materials2005

    • Author(s)
      T.Shibayama(分担執筆)
    • Total Pages
      316
    • Publisher
      Atomic Energy Society of Japan
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Book] Introduction of the Advanced Nuclear Energy Technology in Fusion, Fuels and Materials2005

    • Author(s)
      T.Shibayama
    • Total Pages
      316
    • Publisher
      Atomic Energy Society of Japan
    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Book] Introduction to the Advanced Nuclear Energy Technology in Fusion(Fuels and Materials分担執筆)New Electron Microscopy to Materials Science for Energy Related Issues2005

    • Author(s)
      S.Konishi, Y.Tamamoto, A.Kimura, M.S.Yang, B.G.Hong, J.W.Lee編
    • Publisher
      Atomic Energy Society of Japan
    • Related Report
      2005 Annual Research Report
  • [Book] プロフェッショナル英和辞典SPED TERRA/物質・工学編2004

    • Author(s)
      堀内克明ら, 分担執筆
    • Total Pages
      1952
    • Publisher
      小学館
    • Related Report
      2004 Annual Research Report

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Published: 2004-04-01   Modified: 2016-04-21  

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