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Control of nano-carbon synthesized in liquid phase under high magnetic field

Research Project

Project/Area Number 16510089
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Nanomaterials/Nanobioscience
Research InstitutionToyama Prefectural University

Principal Investigator

YOKOMICHI Haruo  Toyama Prefectural University, 工学部, Associate Professor (30212301)

Co-Investigator(Kenkyū-buntansha) KISHIMOTO Naoki  National Research Institute for Metals, Quantum Beam Center, 量子ビームセンター, Managing Director (40354360)
Project Period (FY) 2004 – 2006
Project Status Completed (Fiscal Year 2006)
Budget Amount *help
¥3,300,000 (Direct Cost: ¥3,300,000)
Fiscal Year 2006: ¥900,000 (Direct Cost: ¥900,000)
Fiscal Year 2005: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 2004: ¥1,300,000 (Direct Cost: ¥1,300,000)
Keywordssupersonic irradiation / room temperature synthesis / liquid phase synthesis / nano-carbon / electrochemical technique / high magnetic field / 超音波合成法 / 磁場中合成 / ナノワイヤー
Research Abstract

Carbon nanotubes have been commonly synthesized using a wide variety of chemical vapor deposition (CVD) methods, arc discharge and laser ablation techniques. These synthesis methods require a high synthesis temperature, at least 500℃. A low-temperature synthesis is important for an application of nanotubes and nanowires to practical devices. Since we have reported the room temperature nano-carbon synthesis by electrochemical techniques, high magnetic fields up to 12 Tesla are applied to electrochemical techniques for carbon nanotube synthesis. The deposits were characterized by scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy dispersive spectroscopy (EDS). An increase in the long carbon nanowires due to magnetic field was observed by TEM. In addition, high magnetic fields up to 12 Tesla are applied to thermal CVD for carbon nanotube synthesis. An increase in the onion-like nano-carbons and due to magnetic field was observed by TEM. Beside these synthesis methods, we have discovered another room temperature synthesis method of carbon nanotubes and carbon nanowires. The new room temperature synthesis has been achieved by a supersonic irradiation into a liquid phase of organic solution with a metal catalyst and metal Na. The temperature increase during the deposition is negligible, because of by a few degrees at most. This low temperature synthesis method has a great advantage to develop carbon-based new materials. In addition, the apparatus used in the present study is simple and is not expensive. Therefore, this technique will make it possible to develop other nanosized new materials.

Report

(4 results)
  • 2006 Annual Research Report   Final Research Report Summary
  • 2005 Annual Research Report
  • 2004 Annual Research Report
  • Research Products

    (6 results)

All 2009 2007 2005

All Journal Article (4 results) (of which Peer Reviewed: 2 results) Presentation (2 results)

  • [Journal Article] Morphology of carbon nanotubes synthesized by thermal CVD under high magnetic field up to 10 T2009

    • Author(s)
      H.Yokomichi, et al
    • Journal Title

      Vacuum 83

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Morphology of carbon nanotubes synthesized by thermal CVD under high magnetic field up to 10 T2009

    • Author(s)
      H.Yokomichi, M.Ichihara, S.Nimori, N.Kishimoto
    • Journal Title

      Vacuum 83

      Pages: 625-628

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Journal Article] Room Temperature Synthesis of Nano-Carbons Usiong an Electrochemical Technique of Organic Solution2005

    • Author(s)
      H.Yokomichi, et al
    • Journal Title

      Nanotecnology 16

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
    • Peer Reviewed
  • [Journal Article] Room Temperature Synthesis of Nano-Carbons Using an Electrochemical Technique of Organic Solution2005

    • Author(s)
      H.Yokomichi, F.Sakai, M.Ichihara, N.Kishimoto
    • Journal Title

      Nanotecnology 16

      Pages: 1204-1207

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2006 Final Research Report Summary 2005 Annual Research Report
  • [Presentation] Attempt to Control Nanocarbons Morphology by High Magnetic Field under Thermal CVD2007

    • Author(s)
      H.Yokomichi
    • Organizer
      The 9th International Symposium on Sputtering & Plasma Processes
    • Place of Presentation
      Kanazawa, Japan
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary
  • [Presentation] Attempt to Synthesize Nano-Carbons by Electrochemical Technique Under High Magnetic Field Up To 12 T at Room Temperature2005

    • Author(s)
      H.Yokomichi
    • Organizer
      Twelve International Conference on Composites/Nano Engineering
    • Place of Presentation
      Tenerife, Spain
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2006 Final Research Report Summary

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Published: 2004-04-01   Modified: 2016-04-21  

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