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Microstructure control of L1_2- and B2-type intermetallic alloys by deformation and recrystallization

Research Project

Project/Area Number 16560614
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Structural/Functional materials
Research InstitutionOsaka Prefecture University

Principal Investigator

KANENO Yasuyuki  Osaka Prefecture University, Graduate School of Engineering, Research Associate, 工学研究科, 助手 (50214482)

Project Period (FY) 2004 – 2005
Project Status Completed (Fiscal Year 2005)
Budget Amount *help
¥3,700,000 (Direct Cost: ¥3,700,000)
Fiscal Year 2005: ¥1,100,000 (Direct Cost: ¥1,100,000)
Fiscal Year 2004: ¥2,600,000 (Direct Cost: ¥2,600,000)
Keywordsintermetallics / polycrystalline ingot / cold rolling / foil / high tensile strength / texture / grain boundary character distribution / annealing twin / 熱間圧延 / 薄板 / 耐熱性 / 圧延加工 / 再結晶 / 組織制御 / SEM-EBSD
Research Abstract

Heavily cold-rolled foils of L1_2-type Ni_3(Si,Ti), Ni_3Al and Co_3Ti ordered intermetallic alloys were successfully fabricated by the newly designed thermomechanical processing using conventional polycrystalline ingots. Also, thin sheets of B2-type FeAl, NiAl, CoTi and CoZr intermetallic compounds were fabricated by the two-step hot-rolling. Microstructure including texture and grain boundary character, and mechanical properties of these thin sheets or foils were studied. Main results obtained from the present study are as follows : (i)Texture development during cold rolling of Ni-based L1_2 ordered alloys (i.e., Ni_3(Si,Ti), N_3Al and Ni_3Fe) as well as fcc disordered nickel was investigated by means of the orientation distribution function (ODF). The cold rolling texture of these Ni-based L1_2 ordered alloys was found to be a copper-type with a prominent component of Bs {011}<211> orientation. In addition, intensity of rolling texture of L1_2 alloys was relatively weak in comparison … More that of fcc nickel. These results can be interpreted by consideration of cross slips for superlattice dislocations and ordinary dislocation whose width are estimated by energies of stacking-fault-like defect (SFLD) (i.e., antiphase boundary (APB) in the case of L1_2 ordered structure and stacking fault (SF) in the case of fcc disordered structure). (ii)Grain boundary character distribution (GBCD) of the recrystallized L1_2 ordered alloys and fcc disordered alloys was determined by the electron backscatted diffraction (EBSD) method. A number of annealing twin boundaries (i.e., Σ3 boundaries) were observed in both the L1_2 and fcc alloys. It was suggested that the frequency of Σ3 twin boundary was primarily dominated by the stacking fault energy, regardless of L1_2 ordered or fcc disordered alloys. On the other hand, the difference in the feature of grain boundaries between L1_2 ordered and fcc disordered alloys could be interpreted by the energetic consideration for the grain boundary in which the APB energy (i.e. the ordering energy) due to the wrong bonds is incorporated into. (iii)Mechanical property of the L1_2 thin foils were evaluated by tensile test at room temperature as well as at high temperature. It was found that owing to heavily cold-rolling and proper annealing, these intermetallic foils showed high tensile strength and considerable elongation at room temperature, and also that their high temperature tensile strength was superior to that of conventional metallic materials such as nickel alloys and stainless steels. (iv)Texture evolution during hot-rolling and recrystallization of B2 type FeAl, NiAl and CoTi intermetallic compounds were investigated by means of X-ray pole figure and EBSD methods. The hot-rolling textures of FeAl, NiAl and CoTi are commonly composed of a ND//{111} textural component. The orientations of the recrystallized gains were evolved within the orientation distribution of the deformed matrix, but were more dispersive than those of the deformed grains. It was suggested that the non-selected grain growth was responsible for the observed weak recrystallization textures of the present compounds. (v)B2-type CoZr intermetallic compound was hot-rolled and subsequently recrystallized. Tensile test was revealed that CoZr with recrystallized microstructure exhibited a notable tensile ductility at room temperature as well as at elevated temperature. Furthermore, the recrystallized CoZr was possible to be cold rolled to 70% reduction. These results is strongly suggested that B2 CoZr phase is substantially ductile whereas most of B2-type intermetallic compounds show poor ductility, particularly at room temperature. Less

Report

(3 results)
  • 2005 Annual Research Report   Final Research Report Summary
  • 2004 Annual Research Report
  • Research Products

    (25 results)

All 2006 2005 2004 Other

All Journal Article (21 results) Patent(Industrial Property Rights) (4 results)

  • [Journal Article] Cold rolling texture of Ni-based L1_2 ordered intermetallic alloys2006

    • Author(s)
      Y.Kaneno, A.Takahashi, T.Takasugi
    • Journal Title

      Materials Transactions Vol.47(印刷中)

    • NAID

      10018160363

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Cold rolling texture of Ni-based L1_2 ordered intermetallic alloys2006

    • Author(s)
      Y.Kaneno, A.Takahashi, T.Takasugi
    • Journal Title

      Materials Transactions 47(in press)

    • NAID

      10018160363

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Cold rolling texture of Ni-based L1_2 ordered intermetallic alloys2006

    • Author(s)
      Y.Kaneno, A.Takahashi, T.Takasugi
    • Journal Title

      Materials Transactions 47(印刷中)

    • NAID

      10018160363

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Hot rolling workability, texture and grain boundary character distribution of B2-type FeAl, NiAl and CoTi intermetallic compounds2005

    • Author(s)
      Y.Kaneno, T.Yamaguchi, T.Takasugi
    • Journal Title

      Journal of Materials Science Vol.40

      Pages: 733-740

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary 2004 Annual Research Report
  • [Journal Article] Effects of stacking fault energy and ordering energy on grain boundary character distribution of recrystallized L1_2-type ordered alloys2005

    • Author(s)
      Y.Kaneno, T.Takasugi
    • Journal Title

      Materials Science and Engineering A Vol.393

      Pages: 71-79

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Room-Temperature Tensile Properties and Fracture Behavior of Recrystallized B2-type CoZr Intermetallic Compound2005

    • Author(s)
      T.Yamaguchi, Y.Kaneno, T.Takasugi
    • Journal Title

      Scripta Materialia Vol.52

      Pages: 39-44

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Characterization of Grain Boundaries in Recrystallized L1_2-Type Intermetallic Alloys2005

    • Author(s)
      Y.Kaneno, T.Takasugi
    • Journal Title

      Materials Science Forum Vol.502

      Pages: 151-156

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Hot rolling workability, texture and grain boundary character distribution of B2-type FeAl, NiAl and CoTi intermetallic compounds2005

    • Author(s)
      Y.Kaneno, T.Yamaguchi, T.Takasugi
    • Journal Title

      Journal of Materials Science 40

      Pages: 733-740

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effects of stacking fault energy and ordering energy on grain boundary character distribution of recrystallized L1_2-type ordered alloys2005

    • Author(s)
      Y.Kaneno, T.Takasugi
    • Journal Title

      Materials Science and Engineering A393

      Pages: 71-79

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Room-Temperature Tensile Properties and Fracture Behavior of Recrystallized B2-type CoZr Intermetallic Compound2005

    • Author(s)
      T.Yamaguchi, Y.Kaneno, T.Takasugi
    • Journal Title

      Scripta Materialia 52

      Pages: 39-44

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Characterization of Grain Boundaries in Recrystallized L1_2-Type Intermetallic Alloys2005

    • Author(s)
      Y.Kaneno, T.Takasugi
    • Journal Title

      Materials Science Forum 502

      Pages: 151-156

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effects of stacking fault energy and ordering energy on grain boundary character distribution of recrystallized L1_2-type ordered alloys.2005

    • Author(s)
      Y.Kaneno, T.Takasugi
    • Journal Title

      Materials Science and Engineering A 393

      Pages: 71-79

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Characterization of grain boundaries in recrystallized L1_2-type intermetallic alloys.2005

    • Author(s)
      Y.Kaneno, T.Takasugi
    • Journal Title

      Materials Science Forum 502

      Pages: 151-156

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Microstructure and texture evolution during cold rolling and annealing of Ni_3Fe alloy2005

    • Author(s)
      Y.Kaneno, A.Takahashi, T.Takasugi
    • Journal Title

      Materials Science and Engineering A 393

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Hot-Rolling and Recrystallization Behavior of B2-Type Intermetallic Compounds2004

    • Author(s)
      Y.Kaneno, T.Yamaguchi, T.Takasugi
    • Journal Title

      Proc.of Int.Conf.on New Frontiers of Process Science and Engineering in Advanced Materials (PSEA'04)

      Pages: 203-208

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Microstructure and texture evolution during cold rolling and annealing of Ni_3Fe alloy

    • Author(s)
      Y.Kaneno, A.Takahashi, T.Takasugi
    • Journal Title

      Materials Science and Engineering A (投稿中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Texture evolution during hot-rolling and recrystallization in B2-type FeAl, NiAl and CoTi intermetallic compounds

    • Author(s)
      Y.Kaneno, T.Yamaguchi, T.Takasugi
    • Journal Title

      Journal of Materials Science (印刷中)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Microstructure and texture evolution during cold rolling and annealing of Ni_3Fe alloy

    • Author(s)
      Y.Kaneno, A.Takahashi, T.Takasugi
    • Journal Title

      Materials Science and Engineering A (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Texture evolution during hot-rolling and recrystallization in B2-type FeAl, NiAl and CoTi intermetallic compounds

    • Author(s)
      Y.Kaneno, T.Yamaguchi, T.Takasugi
    • Journal Title

      Journal of Materials Science (in press)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Texture evolution during hot-rolling and recrystallization in B2-type FeAl, NiAl and CoTi intermetallic compounds

    • Author(s)
      Y.Kaneno, T.Yamaguchi, T.Takasugi
    • Journal Title

      Journal of Materials Science (印刷中)

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Effects of stacking fault energy and ordering energy on grain boundary character distribution of recrystallized L1-2-type ordered alloys

    • Author(s)
      Y.Kaneno, T.Takasugi
    • Journal Title

      Materials Science and Engineering A (印刷中)

    • Related Report
      2004 Annual Research Report
  • [Patent(Industrial Property Rights)] CoZr金属間化合物薄板,その製造方法,水素透過フィルター2006

    • Inventor(s)
      高杉 隆幸, 金野 泰幸
    • Industrial Property Rights Holder
      公立大学法人 大阪府立大学
    • Industrial Property Number
      2006-075214
    • Filing Date
      2006-03-17
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Annual Research Report 2005 Final Research Report Summary
  • [Patent(Industrial Property Rights)] Co_3Ti薄板の製造方法,Co_3Ti薄板2005

    • Inventor(s)
      高杉 隆幸, 金野 泰幸
    • Industrial Property Rights Holder
      公立大学法人 大阪府立大学
    • Industrial Property Number
      2005-238880
    • Filing Date
      2005-08-19
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Patent(Industrial Property Rights)] 高強度と室温延性を兼備する耐熱性Ni_3(Si,Ti)金属間化合物箔の製造方法および高強度と室温延性を兼備する耐熱性Ni_3(Si,Ti)金属間化合物箔2005

    • Inventor(s)
      高杉 隆幸, 金野 泰幸
    • Industrial Property Rights Holder
      財団法人大阪産業振興機構
    • Industrial Property Number
      2005-278049
    • Filing Date
      2005-09-26
    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Annual Research Report 2005 Final Research Report Summary
  • [Patent(Industrial Property Rights)] Co_3Ti薄板の製造方法, Co_3Ti薄板2005

    • Inventor(s)
      高杉 隆幸, 金野 泰幸
    • Industrial Property Rights Holder
      公立大学法人 大阪府立大学
    • Industrial Property Number
      2005-238880
    • Filing Date
      2005-08-19
    • Related Report
      2005 Annual Research Report

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Published: 2004-04-01   Modified: 2016-04-21  

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