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Development of Consistent Measuring Procedure to Detect Hydrogen Damage by Acoustic Emission Method

Research Project

Project/Area Number 16560635
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/treatments
Research InstitutionThe University of Tokushima

Principal Investigator

YOSHIDA Kenichi  The University of Tokushima, Faculty of Engineering, Professor, 工学部, 教授 (50200986)

Co-Investigator(Kenkyū-buntansha) NISHINO Hideo  The University of Tokushima, Faculty of Engineering, Associate Professor, 工学部, 助教授 (50316890)
Project Period (FY) 2004 – 2005
Project Status Completed (Fiscal Year 2005)
Budget Amount *help
¥3,600,000 (Direct Cost: ¥3,600,000)
Fiscal Year 2005: ¥1,500,000 (Direct Cost: ¥1,500,000)
Fiscal Year 2004: ¥2,100,000 (Direct Cost: ¥2,100,000)
KeywordsAcoustic Emission / Gas Leak / Aluminum Alloys / Hydrogen Micro-Print Method / Hydrogen Embrittlement / アコースティック・エミッション(AE) / 疲労損傷 / AE波形解析
Research Abstract

A consistent measuring procedure to sequentially detect the generation and growth of micro-cracks due to hydrogen embrittlement and macro-cracks with gas leak by acoustic emission (AE) method has been investigated using a steel for pipe material and aluminum alloys for hydrogen cylinder (5000 and 6000 series alloys). New knowledge and results obtained are as follows :
1.Hydrogen damages were revealed to concentrate along slip lines and grain boundaries by hydrogen microprint method. Grain boundaries easy to make these damages were identified using electron back scattering pattern (EBSP) analysis. The generation and growth of the micro-cracks due to hydrogen damages was closely related to the detected AE signals.
2.New method was proposed to contract the characteristics of the AE waveforms because the elastic wave propagating in finite body shows velocity dispersion and mode transform. It was recognized that the analytical method was useful to analyze the AE waveforms detected during plastic deformation and micro-cracking due to the hydrogen damage.
3.Characteristic AE waveforms could be obtained during the gas leak from artificial pinholes similar to the macro-cracks due to hydrogen damage. Application to hydro-dynamical noise evaluation was made clear to be possible using the peak frequency of the AE waveforms

Report

(3 results)
  • 2005 Annual Research Report   Final Research Report Summary
  • 2004 Annual Research Report
  • Research Products

    (23 results)

All 2006 2005 2004

All Journal Article (23 results)

  • [Journal Article] Propagation phenomena of wideband guided waves in a bended pip2006

    • Author(s)
      Hideo Nishino
    • Journal Title

      ULTRASONICS (to be published)

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Propagation phenomena of wideband guided waves in a bended pipe2006

    • Author(s)
      Nishino Hideo
    • Journal Title

      ULTRASONICS (to be published)

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Propagation phenomena of wideband guided waves in a bended pipe2006

    • Author(s)
      Hideo Nishino
    • Journal Title

      ULTRASONICS to be published

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Boron Effects of AE Event Rate Peaks during Tensile Deformatio of Ni_3Al Intermetallic Compound2005

    • Author(s)
      Kenichi Yoshida
    • Journal Title

      Journal of Acoustic Emission 23

      Pages: 189-195

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] ガスリーク中に検出されるAE特性におよぼすスリット人工孔の形状およびその方向の影響2005

    • Author(s)
      吉田憲一
    • Journal Title

      第15回アコースティック・エミッション総合コンファレンス論文集 15

      Pages: 55-58

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Boron Effects of AE Event Rate Peaks during Tensile Deformation of Ni_3Al Intermetallic Compound2005

    • Author(s)
      Yoshida Kenichi
    • Journal Title

      Journal of Acoustic Emission Vol.23

      Pages: 189-195

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effect of Artificial Slit Shapes and Directions on AE Characteristics Detected during Gas Leak2005

    • Author(s)
      Yoshida Kenichi
    • Journal Title

      Proceedings of 15^<th> AE General Conference Vol.15

      Pages: 55-58

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Boron Effects of AE Event Rate Peaks during Tensile Deformation of Ni_3Al Intermetallic Compound2005

    • Author(s)
      Kenichi Yoshida
    • Journal Title

      Journal of Acoustic Emission 23

      Pages: 189-195

    • Related Report
      2005 Annual Research Report
  • [Journal Article] ガスリーク中に検出されるAE特性およぼすスリット人工孔およびその方向の影響2005

    • Author(s)
      吉田憲一
    • Journal Title

      第15回アコースティック・エミッション総合コンファレンス論文集 15

      Pages: 55-58

    • Related Report
      2005 Annual Research Report
  • [Journal Article] Acoustic Emission Behavior of Martensitic Transformation in Early Stage during Deformation of Cu-Al-Ni Shape Memory Alloy Single Crystals2004

    • Author(s)
      Kenichi Yoshida
    • Journal Title

      Journal of Acoustic Emission 22

      Pages: 159-168

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] 水素マイクロプリント法とEBSP解析に基づく引張変形を与えたAl-5%Mg合金中の水素集積の可視化2004

    • Author(s)
      吉田憲一
    • Journal Title

      日本金属学会誌 68・12

      Pages: 1043-1046

    • NAID

      10014238757

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effect of Pinhole Shape with Divergent Exit on AE Characteristics during Gas Leak2004

    • Author(s)
      Kenichi Yoshida
    • Journal Title

      Journal of Acoustic Emission 22

      Pages: 223-229

    • Description
      「研究成果報告書概要(和文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Acoustic Emission Behavior of Martensitic Transformation in Early Stage during Deformation of Cu-Al-Ni Shape Memory Alloy Single Crystals2004

    • Author(s)
      Yoshida Kenichi
    • Journal Title

      Journal of Acoustic Emission Vol.22

      Pages: 159-168

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Visualization of Hydrogen Distribution in Tensile-Deformed Al-5%Mg Alloy Investigated by means of Hydrogen Microprint Technique with EBSP Analysis2004

    • Author(s)
      Yoshida Kenichi
    • Journal Title

      Materials Transaction Vol.45, No.2

      Pages: 315-318

    • NAID

      10014238757

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] Effect of Pinhole Shape with Divergent Exit on AE Characteristics during Gas Leak2004

    • Author(s)
      Yoshida Kenichi
    • Journal Title

      Journal of Acoustic Emission Vol.22

      Pages: 223-229

    • Description
      「研究成果報告書概要(欧文)」より
    • Related Report
      2005 Final Research Report Summary
  • [Journal Article] 水素マイクロプリント法とEBSP解析に基づく引張変形をAL-5%Mg合金中の水素集積の可視化2004

    • Author(s)
      吉田憲一
    • Journal Title

      日本金属学会誌 12

      Pages: 1043-1045

    • Related Report
      2004 Annual Research Report
  • [Journal Article] EFFECT OF PINHOLE SHAPE WITH DIVERGENT EXIT ON AE CHARACTERISTICS DURING GAS LEAK2004

    • Author(s)
      K.Yoshida et al.
    • Journal Title

      Journal of Acoustic Emission 21

      Pages: 223-229

    • Related Report
      2004 Annual Research Report
  • [Journal Article] ACOUSTIC EMISSION CAUSED BY ENVIRONMENTAL EMBRITTLEMENT OF AN Al-Mg-Si ALLOY2004

    • Author(s)
      K.Yoshida et al.
    • Journal Title

      Journal of Acoustic Emission 21

      Pages: 206-212

    • Related Report
      2004 Annual Research Report
  • [Journal Article] A Novel Method of Estimating the Aspect Ratio of Pipe Wall Thickness to Diameter Utilizing the Characteristics of Hollow Cylindrical Guided Wave2004

    • Author(s)
      H.Nishino et al.
    • Journal Title

      Proceedings of American Society of Mechanical Engineering, PVP2004-2806 484

      Pages: 1-6

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Effect of Boron Additives on Two Peaks of AE Event Rate during Tensile Deformation of Ni3Al Intermetallic Compound2004

    • Author(s)
      K.Yoshida et al.
    • Journal Title

      Progress in Acoustic Emission XII (Proc.of The 16th International Acoustic Emission Symposium) 12

      Pages: 225-232

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Acoustic Emission Behavior of Martensitic Transformation in Early Stage during Deformation of CuAl-Ni Shape Memory Alloy Single Crystals2004

    • Author(s)
      K.Yoshida et al.
    • Journal Title

      Proc.of the 26th European Conference on Acoustic Emission Testing (EWGAE-2004) 1

      Pages: 283-291

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Frequency Characteristics of Acoustic Emission Waveforms during Gas Leak2004

    • Author(s)
      K.Yoshida et al.
    • Journal Title

      Proc.of the 26th European Conference on Acoustic Emission Testing (EWGAE-2004) 1

      Pages: 371-379

    • Related Report
      2004 Annual Research Report
  • [Journal Article] Acoustic emission of Fatigue-Deformed Aluminum Alloys for Automotive Panels2004

    • Author(s)
      K.Yoshida et al.
    • Journal Title

      Proc.of the 26th European Conference on Acoustic Emission Testing (EWGAE-2004) 1

      Pages: 323-330

    • Related Report
      2004 Annual Research Report

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Published: 2004-04-01   Modified: 2016-04-21  

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