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Comprehensive understanding of light elements solid solution contributing to toughening of pure titanium sintered materials

Research Project

Project/Area Number 16H02408
Research Category

Grant-in-Aid for Scientific Research (A)

Allocation TypeSingle-year Grants
Section一般
Research Field Material processing/Microstructural control engineering
Research InstitutionOsaka University

Principal Investigator

KONDOH KATSUYOSHI  大阪大学, 接合科学研究所, 教授 (50345138)

Co-Investigator(Kenkyū-buntansha) 梅田 純子  大阪大学, 接合科学研究所, 准教授 (50345162)
今井 久志  大阪大学, 接合科学研究所, 講師 (30452379)
Project Period (FY) 2016-04-01 – 2020-03-31
Project Status Completed (Fiscal Year 2019)
Budget Amount *help
¥40,170,000 (Direct Cost: ¥30,900,000、Indirect Cost: ¥9,270,000)
Fiscal Year 2019: ¥9,360,000 (Direct Cost: ¥7,200,000、Indirect Cost: ¥2,160,000)
Fiscal Year 2018: ¥9,880,000 (Direct Cost: ¥7,600,000、Indirect Cost: ¥2,280,000)
Fiscal Year 2017: ¥10,530,000 (Direct Cost: ¥8,100,000、Indirect Cost: ¥2,430,000)
Fiscal Year 2016: ¥10,400,000 (Direct Cost: ¥8,000,000、Indirect Cost: ¥2,400,000)
Keywords粉末冶金 / 粉末プロセス / 純チタン
Outline of Final Research Achievements

Pure titanium (α-Ti) sintered material with light element solutes such as oxygen and nitrogen successfully balanced high strength and enough ductility. To understand the mechanical improvement mechanism, the phase transformation and optimized water-quenching treatment were applied to control the oxygen solution concentration, and resulted in the ductility improvement. After optimizing the processing and heat treatment conditions based on the above results, such heterogeneously oxygen distributed microstructures effectively overcome the strength-ductility trade-off balance of cast titanium materials. Furthermore, it was predicted that the most stable structure of the solid solution oxygen atom in the α-Ti crystal was an octahedral site using first-principles calculation, and the agreement with the X-ray diffraction results was verified.

Academic Significance and Societal Importance of the Research Achievements

チタン焼結材の革新的力学機能発現に向けて,廉価な軽元素である酸素や窒素の有効利用を実現すべく,固溶状態での溶質原子の振舞いを解明することで従前より延性低下を誘発する負の成分とされてきた酸素・窒素が高延性を維持しつつ,高強度発現に作用するといった新たな知見を得た.さらに,このような特異な力学特性の発現に資する加工・熱処理プロセスを提案し,チタン溶解材においても高強度・高延性の両立を実現した.以上の成果は,チタン素材のコスト削減に直結するものであり,チタンをコモンメタルとして幅広い分野で利活用するための重要な基盤技術になり得る.

Report

(5 results)
  • 2019 Annual Research Report   Final Research Report ( PDF )
  • 2018 Annual Research Report
  • 2017 Annual Research Report
  • 2016 Annual Research Report
  • Research Products

    (30 results)

All 2019 2018 2017 2016 Other

All Int'l Joint Research (8 results) Journal Article (10 results) (of which Int'l Joint Research: 7 results,  Peer Reviewed: 10 results,  Open Access: 5 results,  Acknowledgement Compliant: 2 results) Presentation (12 results) (of which Int'l Joint Research: 7 results,  Invited: 5 results)

  • [Int'l Joint Research] メルボルン工科大学(オーストラリア)

    • Related Report
      2019 Annual Research Report
  • [Int'l Joint Research] Northwestern Polytechnical University/中国科学院(中国)

    • Related Report
      2019 Annual Research Report
  • [Int'l Joint Research] KMUTT(タイ)

    • Related Report
      2019 Annual Research Report
  • [Int'l Joint Research] メルボルン工科大学(オーストラリア)

    • Related Report
      2018 Annual Research Report
  • [Int'l Joint Research] Northwestern Polytechnical University/中国科学院(中国)

    • Related Report
      2018 Annual Research Report
  • [Int'l Joint Research] KMNUTT(タイ)

    • Related Report
      2018 Annual Research Report
  • [Int'l Joint Research] Northwestern Polytechnical University/中国科学院(中国)

    • Related Report
      2017 Annual Research Report
  • [Int'l Joint Research] メルボルン工科大学(オーストラリア)

    • Related Report
      2017 Annual Research Report
  • [Journal Article] Ductility Improvement Mechanism of Pure Titanium with Excessive Oxygen Solid Solution via Rapid Cooling Process2018

    • Author(s)
      刈屋翔太,梅田純子,Ma Qian,近藤勝義
    • Journal Title

      Journal of the Japan Institute of Metals and Materials

      Volume: 82 Issue: 10 Pages: 390-395

    • DOI

      10.2320/jinstmet.JAW201810

    • NAID

      130007488297

    • ISSN
      0021-4876, 1880-6880, 2433-7501
    • Year and Date
      2018-10-01
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Microstructural and mechanical properties of α-titanium sintered material via thermal decomposition of additive chromium oxide particles2018

    • Author(s)
      K. Kondoh, R. Ikemasu, J. Umeda, S. Kariya, A. Khantachawana
    • Journal Title

      Materials Science & Engineering A

      Volume: 739 Pages: 491-498

    • DOI

      10.1016/j.msea.2018.10.081

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Rate sensitivity and work-hardening behavior of an advanced Ti-Al-N alloy under uniaxial tensile loading2018

    • Author(s)
      J. Shen, J. Umeda B. Chen, J. Umeda, J. Zhang, Y.Li, K. Kondoh
    • Journal Title

      Materials Science & Engineering A

      Volume: 744 Pages: 630-637

    • DOI

      10.1016/j.msea.2018.12.066

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Dynamic recrystallization behavior and strengthening-toughening effects in a near-α Ti-xSi alloy processed by hot extrusion2017

    • Author(s)
      X.X. Ye, H. Imai, J.H. Shen, B. Chen, G.Q. Han, J. Umeda, M. Takahashi, K. Kondoh
    • Journal Title

      Materials Science & Engineering A

      Volume: 684 Pages: 165-177

    • DOI

      10.1016/j.msea.2016.12.054

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Microstructure and strengthening mechanism of ultrastrong and ductile Ti-xSn alloy processed by powder metallurgy2017

    • Author(s)
      X.X. Ye, B. Chen, J.H. Shen, J. Umeda, K. Kondoh
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 709 Pages: 381-393

    • DOI

      10.1016/j.jallcom.2017.03.171

    • Related Report
      2017 Annual Research Report 2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Advanced mechanical properties of powder metallurgy commercially pure titanium with a high oxygen concentration2017

    • Author(s)
      B. Chen, J. Shen, X. Ye, J. Umeda, K. Kondoh
    • Journal Title

      Journal of Material Research

      Volume: 32 Issue: 19 Pages: 3769-3776

    • DOI

      10.1557/jmr.2017.338

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] 窒素固溶強化純チタン焼結材の摩擦摺動特性2017

    • Author(s)
      山辺 康宏,梅田純子,近藤勝義
    • Journal Title

      粉体および粉末冶金

      Volume: 64 Pages: 275-280

    • NAID

      130007311751

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Enhanced Homogenization of Vanadium in Spark Plasma Sintering of Ti-10V-2Fe-3Al Alloy from Titanium and V-Fe-Al Master Alloy Powder Blends2017

    • Author(s)
      Y. F. Yang, H, Imai, K. Kondoh, M. Qian
    • Journal Title

      JOM

      Volume: 69 Issue: 4 Pages: 663-668

    • DOI

      10.1007/s11837-017-2271-4

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] The formation of bimodal multilayered grain structure and its effect on the mechanical properties of powder metallurgy pure titanium2017

    • Author(s)
      J. Shen, B. Chen, X. Ye, H. Imai, J. Umeda, K. Kondoh
    • Journal Title

      Materials and Design

      Volume: 116 Pages: 99-108

    • DOI

      10.1016/j.matdes.2016.12.004

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Study of twinning behavior of powder metallurgy Ti-Si alloy by interrupted in-situ tensile tests2017

    • Author(s)
      X.X. Ye, H. Imai, J.H. Shen, B. Chen, G.Q. Han, J. Umeda, K. Kondoh
    • Journal Title

      Materials Science & Engineering A

      Volume: 679 Pages: 543-553

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] Rare Metals Free Titanium Alloys Enhancing High Strength and Ductility by Atomic-Scale Microstructures Control2019

    • Author(s)
      K. Kondoh, S. Kariya, T. Tanaka, J. Umeda
    • Organizer
      ICMAT2019
    • Related Report
      2019 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Zr固溶Ti-Fe合金の針状組織形成挙動と強度解析2019

    • Author(s)
      寺前拓馬,田中貴之,福生瑞希,設樂一希,梅田純子,近藤勝義
    • Organizer
      粉体粉末冶金協会2019年度春季大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Strengthening Mechanism of α+β Type Ti-Fe Alloy by Powder Metallurgy2018

    • Author(s)
      T. Tanaka, S. Kariya, J. Shen, J. Umeda, K. Kondoh
    • Organizer
      ASMP2018
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 鉄・酸素固溶チタン焼結材における相変態挙動と力学特性2018

    • Author(s)
      田中貴之,刈屋翔太,SHEN Jianghua,梅田純子,近藤勝義
    • Organizer
      粉体粉末冶金協会平成30年度秋季大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Novel titanium materials with atomic/nano-scale microstructures by powder metallurgy process2018

    • Author(s)
      K. Kondoh
    • Organizer
      IWAMSN 2018
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 鉄・酸素固溶チタン焼結材における相変態挙動と力学特性2018

    • Author(s)
      田中貴之,刈屋翔太,J. Shen,梅田純子,近藤勝義
    • Organizer
      日本金属学会2018年秋期講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] State-of-The-Art Titanium Alloys by Powder Metallurgy Process2018

    • Author(s)
      K. Kondoh
    • Organizer
      MSAT-10
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] State-of-the-art powder metallurgy light metals and their composites with atomic/nano-scale microstructures2018

    • Author(s)
      K. Kondoh
    • Organizer
      ICMMP2018
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Solid solution strengthening mechanisms of PM α-Ti materials with zirconium and oxygen atoms via thermal decomposition of ZrO2 additives in sintering2017

    • Author(s)
      M. Fukuo, S. Kariya, J. Umeda, K. Kondoh
    • Organizer
      JSPM International Conference on Powder and Powder Metallurgy
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 軽元素固溶強化を利用した希少金属フリーα型チタン粉末焼結材の高強度化2017

    • Author(s)
      近藤勝義,山辺康宏,梅田純子
    • Organizer
      粉体粉末冶金協会平成29年度春季大会
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] 焼結過程での熱分解を利用したジルコニウムと酸素の複合固溶による純チタン粉末押出材の強化機構の解明2017

    • Author(s)
      福生瑞希,刈屋翔太,梅田純子,近藤勝義
    • Organizer
      粉体粉末冶金協会平成29年度春季大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Cost-effective, high strength and ductility titanium materials by powder metallurgy process2016

    • Author(s)
      Katsuyoshi Kondoh
    • Organizer
      AeroMat 2016
    • Place of Presentation
      アメリカ・シアトル
    • Year and Date
      2016-05-23
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research

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Published: 2016-04-21   Modified: 2021-02-19  

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