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Determination of composition and strain for strain released SiGe thin layers on Si with using anomalous x-ray microdiffraction

Research Project

Project/Area Number 16H03913
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Quantum beam science
Research InstitutionJapan Synchrotron Radiation Research Institute

Principal Investigator

Kimura Shigeru  公益財団法人高輝度光科学研究センター, 利用研究促進部門, 主席研究員 (50360821)

Co-Investigator(Kenkyū-buntansha) 今井 康彦  公益財団法人高輝度光科学研究センター, 利用研究促進部門, 主幹研究員 (30416375)
Project Period (FY) 2016-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥16,510,000 (Direct Cost: ¥12,700,000、Indirect Cost: ¥3,810,000)
Fiscal Year 2018: ¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Fiscal Year 2017: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Fiscal Year 2016: ¥11,440,000 (Direct Cost: ¥8,800,000、Indirect Cost: ¥2,640,000)
Keywords放射光 / X線回折 / 薄膜 / 異常散乱 / 半導体物性 / X線回折
Outline of Final Research Achievements

We developed anomalous x-ray microdiffraction method, which can determine composition and strain for strain released SiGe thin layers on Si by compering diffraction intensity measured with x-ray energies of 11.103 keV (Ge k absorption edge) and 11.000 keV. The most important point of this development is to measure microdiffraction intensity precisely. For this purpose, we adopted a hybrid pixel detector (ASI Timepix STPX-65k) as a detector of high-resolution microdiffraction system we used. Accordingly, we succeeded to develop the microdiffraction system which enable us to compere diffraction intensity deference with precision less than 0.2%.

Academic Significance and Societal Importance of the Research Achievements

本研究は,これまでX線回折ピーク位置から求めた格子定数から弾性変形理論とベガード則を利用して決定していたSiGe 層の組成を,放射光がエネルギー可変の光源であることを利用し, Ge原子のK 吸収端およびその近傍で異常散乱による強度変化から上述の仮定なしで求めるものである.本手法は,歪緩和SiGe層の歪と組成を独立に決定することができる唯一の方法である.また,この手法は他の局所領域に形成されるヘテロ薄膜材料(例えばGaInN系レーザ構造等)の組成・歪解析にも応用可能な技術である.

Report

(4 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Annual Research Report
  • 2016 Annual Research Report
  • Research Products

    (7 results)

All 2019 2018 2016 Other

All Journal Article (3 results) (of which Peer Reviewed: 3 results,  Open Access: 3 results,  Acknowledgement Compliant: 1 results) Presentation (3 results) (of which Int'l Joint Research: 2 results) Remarks (1 results)

  • [Journal Article] Current Status of Material Characterization by Synchrotron Radiation Nanobeam X-ray Diffraction2019

    • Author(s)
      •今井康彦,隅谷和嗣,木村 滋
    • Journal Title

      Nihon Kessho Gakkaishi

      Volume: 61 Issue: 1 Pages: 51-55

    • DOI

      10.5940/jcrsj.61.51

    • NAID

      130007606955

    • ISSN
      0369-4585, 1884-5576
    • Year and Date
      2019-02-28
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Current status of nanobeam x-ray diffraction station at SPring-82019

    • Author(s)
      Imai Yasuhiko、Sumitani Kazushi、Kimura Shigeru
    • Journal Title

      AIP Conference Proceedings

      Volume: 2054 Pages: 050004-050004

    • DOI

      10.1063/1.5084622

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] High-resolution Micro- and Nano-beam Diffraction System at BL13XU of the SPring-82016

    • Author(s)
      Shigeru Kimura, Yasuhiko Imai
    • Journal Title

      Material Structure in Chemistry, Biology, Physics and Technology

      Volume: Vol. 23, No. 3 Pages: 317-317

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] ナノビームX線回折装置へのピクセル検出器の導入2019

    • Author(s)
      今井康彦,隅谷和嗣,木村 滋
    • Organizer
      第32回放射光学会年会・放射光科学合同シンポジウム
    • Related Report
      2018 Annual Research Report
  • [Presentation] Current status of nanobeam x-ray diffraction station at SPring-82018

    • Author(s)
      Yasuhiko Imai, Kazyshi Sumitani, and Shigeru Kimura
    • Organizer
      Synchrotron Radiation Instrumentation (SRI 2018)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] High-resolution Micro- and Nano-beam Diffraction System at BL13XU of the SPring-82016

    • Author(s)
      Shigeru Kimura, Yasuhiko Imai
    • Organizer
      13th Biennial Conference on High-Resolution X-Ray Diffraction and Imaging
    • Place of Presentation
      ブルノ(チェコ)
    • Year and Date
      2016-09-04
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Remarks] 利用研究促進部門 メンバー(木村 滋)ホームページ

    • URL

      http://rud.spring8.or.jp/member/0004124.html

    • Related Report
      2016 Annual Research Report

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Published: 2016-04-21   Modified: 2020-03-30  

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