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Radial XRD methods with stress-strain analysis opening new horizons for high-pressure experiments

Research Project

Project/Area Number 16H04078
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Petrology/Mineralogy/Economic geology
Research InstitutionNational Institute for Materials Science

Principal Investigator

YUSA HITOSHI  国立研究開発法人物質・材料研究機構, 機能性材料研究拠点, 主席研究員 (10343865)

Co-Investigator(Kenkyū-buntansha) 平尾 直久  公益財団法人高輝度光科学研究センター, 利用研究促進部門, 研究員 (70374915)
Project Period (FY) 2016-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥18,200,000 (Direct Cost: ¥14,000,000、Indirect Cost: ¥4,200,000)
Fiscal Year 2018: ¥2,860,000 (Direct Cost: ¥2,200,000、Indirect Cost: ¥660,000)
Fiscal Year 2017: ¥4,810,000 (Direct Cost: ¥3,700,000、Indirect Cost: ¥1,110,000)
Fiscal Year 2016: ¥10,530,000 (Direct Cost: ¥8,100,000、Indirect Cost: ¥2,430,000)
Keywords高圧X線回折 / ダイヤモンドアンビルセル / 応力歪み解析 / 放射光X線 / X線回折 / 高圧 / 差応力 / 鉱物物理 / 高圧力
Outline of Final Research Achievements

The diamond anvil cells (DAC) with laterally wide aperture were developed for high-pressure x-ray diffraction experiments from various angular incident x-ray beam including a radial x-ray diffraction geometry. For analysis under uniaxial stress using the DAC, we installed a newly designed goniometer by remodeling a conventional multi-axis DAC oscillation system at SPring-8 (BL04B2). Analysis of the radial x-ray diffraction profiles under uniaxial compression derives a differential stress of the sample. After the decompression at ambient pressure, a residual stress was also observed. The constructed system can be useful not only for stress analysis of non-hydrostatic pressurized materials but also high-pressure structural analysis for highly oriented two dimensional materials such as molybdenum sulfides.

Academic Significance and Societal Importance of the Research Achievements

従来から、固体圧力は液体における等方的な圧力と同様ではないと考えられてきたが、その差異を解析するための実験的アプローチは、散発的であり、体系的な取り組みに欠けていたといえる。この原因の一つは、専用のダイヤモンドアンビルセルと回折計が放射光施設に整備されていなかったことによると考えられる。本研究により、構築された広方位粉末回折計により、物質の固体圧力下の応力歪み状態の理解が深まり、地球内部のみならず、巨大歪み下での広範な物質創製研究が大きく進展することが期待できる。

Report

(4 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Annual Research Report
  • 2016 Annual Research Report
  • Research Products

    (45 results)

All 2019 2018 2017 2016

All Journal Article (15 results) (of which Int'l Joint Research: 6 results,  Peer Reviewed: 15 results,  Open Access: 3 results) Presentation (26 results) (of which Int'l Joint Research: 5 results,  Invited: 1 results) Book (1 results) Patent(Industrial Property Rights) (3 results)

  • [Journal Article] Phase relations in silicon and germanium nitrides up to 98 GPa and 2400℃2019

    • Author(s)
      Norimasa Nishiyama , Julia Langer , Takeshi Sakai , Youhei Kojima , Astrid Holzheid , Nico A. Gaida , Eleonora Kulik , Naohisa Hirao , Saori I. Kawaguchi , Tetsuo Irifune , Yasuo Ohishi
    • Journal Title

      Journal of American Ceramics Society

      Volume: 102 Issue: 4 Pages: 2195-2202

    • DOI

      10.1111/jace.16063

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] High-pressure Structural Research Using DAC: XRD and XES Measurements of Transition Metal Difluorides under High Pressure2018

    • Author(s)
      Yusa Hitoshi
    • Journal Title

      Journal of the Society of Materials Science, Japan

      Volume: 67 Issue: 5 Pages: 527-532

    • DOI

      10.2472/jsms.67.527

    • NAID

      130006742986

    • ISSN
      0514-5163, 1880-7488
    • Year and Date
      2018-05-15
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Journal Article] High pressure generation using double-stage diamond anvil technique: problems and equations of state of rhenium2018

    • Author(s)
      Sakai Takeshi、Yagi Takehiko、Irifune Tetsuo、Kadobayashi Hirokazu、Hirao Naohisa、Kunimoto Takehiro、Ohfuji Hiroaki、Kawaguchi-Imada Saori、Ohishi Yasuo、Tateno Shigehiko、Hirose Kei
    • Journal Title

      High Pressure Research

      Volume: - Issue: 2 Pages: 1-13

    • DOI

      10.1080/08957959.2018.1448082

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Boron-doped diamond as a new heating element for internal-resistive heated diamond-anvil cell2018

    • Author(s)
      Ozawa Haruka、Tateno Shigehiko、Xie Longjian、Nakajima Yoichi、Sakamoto Naoya、Kawaguchi Saori I.、Yoneda Akira、Hirao Naohisa
    • Journal Title

      High Pressure Research

      Volume: 38 Issue: 2 Pages: 120-135

    • DOI

      10.1080/08957959.2018.1441407

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] An Experimental Examination of Thermal Conductivity Anisotropy in hcp Iron2018

    • Author(s)
      Ohta Kenji、Nishihara Yu、Sato Yuki、Hirose Kei、Yagi Takashi、Kawaguchi Saori I.、Hirao Naohisa、Ohishi Yasuo
    • Journal Title

      Frontiers in Earth Science

      Volume: 6 Pages: 1-15

    • DOI

      10.3389/feart.2018.00176

    • NAID

      120006889161

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Synthesis of hexagonal phases of WN and W2.25N3 by high-pressure metathesis reaction2018

    • Author(s)
      F. Kawamura, H. Yusa, T. Taniguchi
    • Journal Title

      J.Am.Ceram.Soc.,

      Volume: 101 Issue: 2 Pages: 949-956

    • DOI

      10.1111/jace.15235

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] An Exceptionally Narrow Band-Gap (~4 eV) Silicate Predicted in the Cubic Perovskite Structure: BaSiO32017

    • Author(s)
      H. Hiramatsu, H. Yusa, R. Igarashi, Y. Ohishi, T. Kamiya, H. Hosono
    • Journal Title

      Inorg. Chem.

      Volume: 56 Issue: 17 Pages: 10535-10542

    • DOI

      10.1021/acs.inorgchem.7b01510

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Lithium polyhydrides synthesized under high pressure and high temperature2017

    • Author(s)
      Matsuoka Takahiro、Kuno Keiji、Ohta Kenji、Sakata Masafumi、Nakamoto Yuki、Hirao Naohisa、Ohishi Yasuo、Shimizu Katsuya、Kume Tetsuji、Sasaki Shigeo
    • Journal Title

      Journal of Raman Spectroscopy

      Volume: 48 Issue: 9 Pages: 1222-1228

    • DOI

      10.1002/jrs.5183

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] High-pressure high-temperature phase relations in FeTiO3 up to 35 GPa and 1600 ºC2017

    • Author(s)
      M. Akaogi, K. Abe, H. Yusa, T. Ishii, T. Tajima, H. Kojitani, D. Mori, Y. Inaguma
    • Journal Title

      Phys. Chem. Minerals

      Volume: 44 Issue: 1 Pages: 63-73

    • DOI

      10.1007/s00269-016-0836-3

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] ダイヤモンドアンビルセルによる高圧下放射光X線回折実験の基礎2017

    • Author(s)
      遊佐斉
    • Journal Title

      放射光

      Volume: 30 Pages: 61-70

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 高圧を用いた5d遷移金属窒化物合成と硬質材料開発2016

    • Author(s)
      川村史朗, 遊佐斉, 谷口尚
    • Journal Title

      粉体および粉末冶金

      Volume: 63 Pages: 965-969

    • NAID

      130005277817

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Pressure-induced Isostructural Transition in a Distorted Perovskite via Octahedron Reconfiguration Applied Physics Letters2016

    • Author(s)
      Fang Hong, Binbin Yue, Naohisa Hirao, Guohao Ren, Bin Chen, Ho-kwang Mao
    • Journal Title

      Applied Physics Letters

      Volume: 109 Issue: 24 Pages: 241904-241904

    • DOI

      10.1063/1.4972303

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Phase stability and magnetic behavior of hexagonal phase of N2-O2 system with kagome lattice under high pressure and low temperature2016

    • Author(s)
      Y. Akahama, D. Ishihara, H. Yamashita, H. Fujihisa, N. Hirao, Y. Ohishi
    • Journal Title

      Phys. Rev. B

      Volume: 94 Issue: 6 Pages: 064104-064104

    • DOI

      10.1103/physrevb.94.064104

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Suppression of X-ray-induced dissociation of H2O molecules in dense ice under pressure2016

    • Author(s)
      Hiroshi Fukui, Nozomu Hiraoka, Naohisa Hirao, Katsutoshi Aoki, Yuichi Akahama
    • Journal Title

      Scientific Reports

      Volume: 6 Issue: 1 Pages: 26641-26641

    • DOI

      10.1038/srep26641

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Crystal Structure of the Superconducting Phase of Sulfur Hydride2016

    • Author(s)
      Mari Einaga, Masafumi Sakata, Takahiro Ishikawa, Katsuya Shimizu, Mikhail I. Eremets, Alexander P. Drozdov, Ivan A. Troyan, Naohisa Hirao, and Yasuo Ohishi
    • Journal Title

      Nature Physics

      Volume: 12 Issue: 9 Pages: 835-838

    • DOI

      10.1038/nphys3760

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Presentation] 4d,5d遷移金属窒化物における結晶構造ー体積弾性率相関2019

    • Author(s)
      遊佐 斉
    • Organizer
      2018年度量子ビームサイエンスフェスタ
    • Related Report
      2018 Annual Research Report
  • [Presentation] Latest remolding of multi-axis DAC system for radial XRD experiments2019

    • Author(s)
      H.Yusa, N. Hirao, Y. Mori, Y. Ohishi
    • Organizer
      Joint symposium of Misasa 2019 & CMC
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] BL10XUにおける高エネルギーX線集光ビームを利用した高圧X線回折2019

    • Author(s)
      平尾直久,河口沙織,大石泰生
    • Organizer
      第59回高圧討論会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 窒化物高圧構造探索による新たな超硬質高密度材料開発のための調査研究2018

    • Author(s)
      遊佐斉
    • Organizer
      第2回 TIA かけはし 成果報告会
    • Related Report
      2018 Annual Research Report
  • [Presentation] A multi-axis diamond anvil cell oscillation system for powder X-ray diffraction to improve statistics and analyze deviatoric stress2018

    • Author(s)
      H. Yusa, N. Hirao, Y. Mori, Y. Seto, and Y. Ohishi
    • Organizer
      EHPRG 2018
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 立方晶ペロブスカイト酸化物群から見いだした特異なナローバンドギャップ(~4 eV)を有するシリケート: BaSiO32018

    • Author(s)
      平松秀典 遊佐斉 五十嵐涼 大石泰生 神谷利夫 細野秀雄
    • Organizer
      応用物理学会
    • Related Report
      2018 Annual Research Report
  • [Presentation] BaGeO3における構造対称化とバンドギャップ変化2018

    • Author(s)
      遊佐斉 平松秀典 宮川仁 神谷利夫 細野秀雄 平尾直久 大石泰生 亀卦川卓美
    • Organizer
      第59回高圧討論会
    • Related Report
      2018 Annual Research Report
  • [Presentation] X-ray microfocusing for high-pressure powder x-ray diffraction at BL10XU of SPring-82018

    • Author(s)
      N. Hirao, Y. Ohishi, S. kawaguchi
    • Organizer
      XXII Meeting of the International Mineralogical Association
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 広開口型DACによるAGeO3(A=Sr,Ba)の高圧下X線回折実験2018

    • Author(s)
      遊佐斉
    • Organizer
      第7回名古屋大学シンクロトロン光研究センターシンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] 超高圧物質科学:新奇高密度相の探索から材料応用へ2018

    • Author(s)
      遊佐斉, 川村史朗, 谷口尚, 亀卦川卓美, 若林大祐
    • Organizer
      第3回TIA光・量子計測シンポジウム
    • Related Report
      2017 Annual Research Report
  • [Presentation] スピネル類似組成化合物の高圧相転移:実験と計算による検証2018

    • Author(s)
      遊佐斉, 村田秀信, 亀卦川卓美
    • Organizer
      2017年度量子ビームサイエンスフェスタ
    • Related Report
      2017 Annual Research Report
  • [Presentation] 硫化水素の高温超伝導相の生成過程2017

    • Author(s)
      榮永茉利,坂田雅文,益田明宜,清水克哉,平尾直久,河口沙織,大石泰生
    • Organizer
      日本物理学会第72回年次大会
    • Place of Presentation
      大阪
    • Year and Date
      2017-03-17
    • Related Report
      2016 Annual Research Report
  • [Presentation] W-N系における超硬物質探索2017

    • Author(s)
      遊佐斉, 川村史朗, 谷口尚, 亀卦川卓美, 平尾直久
    • Organizer
      2016年度量子ビームサイエンスフェスタ
    • Place of Presentation
      つくば
    • Year and Date
      2017-03-14
    • Related Report
      2016 Annual Research Report
  • [Presentation] High-pressure syntheses and compression measurements of 5d transition metal nitrides2017

    • Author(s)
      H. Yusa, F. kawamura, T. Taniguchi
    • Organizer
      ISNT2017 & ISSNOX5
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] III族元素を含むMg, Znスピネル高圧相転移の系統性:実験と計算による検証 / III族元素を含むMg, Znスピネル高圧相転移の系統性:実験と計算による検証2017

    • Author(s)
      遊佐斉, 村田秀信, 平尾直久, 大石泰生, 亀卦川卓美
    • Organizer
      第58回高圧討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 多方向広開口DAC粉末X線回折計の開発2017

    • Author(s)
      遊佐斉, 森嘉久, 平尾直久, 大石泰生
    • Organizer
      第58回高圧討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] BL10XUにおけるX線マイクロビームを利用した低温高圧X線回折測定2017

    • Author(s)
      平尾直久,大石泰生,河口沙織,松岡岳洋
    • Organizer
      第58回高圧討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] High pressure and low temperature micro-beam X-ray diffraction system in beamline BL10XU at SPring-82017

    • Author(s)
      N. Hirao, Y. Ohishi, S. kawaguchi
    • Organizer
      AIRAPT 26 & ACHPR 8 & CHPC 19
    • Related Report
      2017 Annual Research Report
  • [Presentation] 遷移金属フッ化物の高圧下X線発光とX線回折実験2016

    • Author(s)
      遊佐斉, 石井啓文, 平岡望, 平尾直久, 大石泰生
    • Organizer
      第57回高圧討論会
    • Place of Presentation
      つくば
    • Year and Date
      2016-10-26
    • Related Report
      2016 Annual Research Report
  • [Presentation] SPring-8の高圧ビームラインの現状と将来展望2016

    • Author(s)
      大石泰生,平尾直久,肥後祐司,丹下慶範,今田沙織
    • Organizer
      第57回高圧討論会
    • Place of Presentation
      つくば
    • Year and Date
      2016-10-26
    • Related Report
      2016 Annual Research Report
  • [Presentation] 金の結晶弾性の圧力位依存性測定: 低圧領域での体積弾性率異常と絶対圧力スケールの検討2016

    • Author(s)
      米田明,福井宏之,鎌田誠司,謝龍剣,平尾直久,内山裕士,BARON Alfred.Q.R.,筒井智嗣
    • Organizer
      第57回高圧討論会
    • Place of Presentation
      つくば
    • Year and Date
      2016-10-26
    • Related Report
      2016 Annual Research Report
  • [Presentation] 低温高圧下の硫化水素の結晶構造2016

    • Author(s)
      榮永茉利,坂田雅文,益田明宜,中尾敏臣,清水克哉,平尾直久,今田沙織,大石泰生
    • Organizer
      第57回高圧討論会
    • Place of Presentation
      つくば
    • Year and Date
      2016-10-26
    • Related Report
      2016 Annual Research Report
  • [Presentation] 新奇ベリリウム水素化物BeHxの結晶構造I2016

    • Author(s)
      松岡岳洋,中河貴也,久野敬司,平尾直久,大石泰生,清水克哉,久米徹二,佐々木重雄,藤久裕司
    • Organizer
      第57回高圧討論会
    • Place of Presentation
      つくば
    • Year and Date
      2016-10-26
    • Related Report
      2016 Annual Research Report
  • [Presentation] 固体酸素における空間反転対称性の破れ2016

    • Author(s)
      青山拓也,永井正也,三宅厚志,平尾直久,大石泰生,清水克哉,芦田昌明,木村剛
    • Organizer
      第57回高圧討論会
    • Place of Presentation
      つくば
    • Year and Date
      2016-10-26
    • Related Report
      2016 Annual Research Report
  • [Presentation] Current status of the high pressure research beamline BL10XU at SPring-82016

    • Author(s)
      N. Hirao, Y. Ohishi, S. Kawaguchi
    • Organizer
      International Union of Crystallography High Pressure workshop (IUCr-HP)
    • Place of Presentation
      Pohang, Korea
    • Year and Date
      2016-09-20
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 硫化水素の低温高圧における結晶構造2016

    • Author(s)
      榮永茉利,坂田雅文,石河孝洋,清水克哉, A.P. Drozdov, M.I. Eremets, I.A. Troyan,平尾直久,今田沙織,大石泰生
    • Organizer
      日本物理学会2016秋季大会
    • Place of Presentation
      金沢
    • Year and Date
      2016-09-13
    • Related Report
      2016 Annual Research Report
  • [Book] Nanoinfomatics, Chapter 122018

    • Author(s)
      H. Yusa, (Isao Tanaka, Editor)
    • Total Pages
      298
    • Publisher
      Springer
    • ISBN
      9789811076169
    • Related Report
      2017 Annual Research Report
  • [Patent(Industrial Property Rights)] 六方晶系6H型バリウムゲルマニウム酸化物、および、その製造方法2018

    • Inventor(s)
      遊佐斉、宮川仁
    • Industrial Property Rights Holder
      国立研究開発法人物質・材料研究機構
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2018-076475
    • Filing Date
      2018
    • Related Report
      2018 Annual Research Report
  • [Patent(Industrial Property Rights)] 窒化レニウムを含有する硬質材料、その製造方法およびそれを用いた切削工具2017

    • Inventor(s)
      遊佐斉、川村史朗、谷口尚
    • Industrial Property Rights Holder
      物質・材料研究機構
    • Industrial Property Rights Type
      特許
    • Industrial Property Number
      2017-194126
    • Filing Date
      2017
    • Related Report
      2017 Annual Research Report
  • [Patent(Industrial Property Rights)] 高圧相WC型TaN焼結体の製造方法2016

    • Inventor(s)
      遊佐斉、川村史朗、谷口尚
    • Industrial Property Rights Holder
      国立研究開発法人物質・材料研究機構
    • Industrial Property Rights Type
      特許
    • Filing Date
      2016
    • Acquisition Date
      2018
    • Related Report
      2018 Annual Research Report

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Published: 2016-04-21   Modified: 2020-03-30  

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