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Development of the bicrystal fabrication method which controlled grain boundary character and quantity of grain boundary segregation and elucidation of properties of grain boundaries

Research Project

Project/Area Number 16H04502
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Composite materials/Surface and interface engineering
Research InstitutionHokkaido University

Principal Investigator

Ikeda Ken-ichi  北海道大学, 工学研究院, 准教授 (20335996)

Co-Investigator(Kenkyū-buntansha) 三浦 誠司  北海道大学, 工学研究院, 教授 (50199949)
滝沢 聡  北海道大学, 工学研究院, 助教 (20240632)
Project Period (FY) 2016-04-01 – 2020-03-31
Project Status Completed (Fiscal Year 2019)
Budget Amount *help
¥12,350,000 (Direct Cost: ¥9,500,000、Indirect Cost: ¥2,850,000)
Fiscal Year 2019: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2018: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2017: ¥5,850,000 (Direct Cost: ¥4,500,000、Indirect Cost: ¥1,350,000)
Fiscal Year 2016: ¥2,990,000 (Direct Cost: ¥2,300,000、Indirect Cost: ¥690,000)
Keywords結晶粒界 / 結晶成長 / 再結晶 / 力学特性 / 表面・界面物性 / 局所力学挙動 / 粒界性格 / 表界面・界面物性
Outline of Final Research Achievements

In this study, in order to clarify the influence of elements of grain boundary segregation and solid solution on the mechanical property and the recrystallization behavior of poly crystalline metals, the development of the bicrystal fabrication method and the elucidation of properties of grain boundaries were carried out. The main results are as follows.
(1) We designed the new mold suitable for Bridgeman Method and succeeded in the fabrication of pure aluminum bicrystals. (2) The precipitation and recrystallization behavior of Al-Mn alloys were strongly affected by the temperature of hot working process and the additional elements. (3) In Al-Mg-Si alloys, the grain boundary character affects the aging precipitation behavior and the mechanical properties.

Academic Significance and Societal Importance of the Research Achievements

実用金属材料は多結晶材料であり、多くの結晶粒界が内在する。本研究は、結晶粒界が関与する力学特性などの諸特性が個々の粒界性格に依存することを示した。得られた成果は、学術的のみならず、材料設計指針を検討する上で、粒界性格を考える必要があることを示した点で、社会的意義もある。特にアルミニウム合金の粒界特性を評価するための双結晶作製手法を確立した点は、今後の研究に活かせる成果である。また、自動車用構造部材として使用されるアルミニウム合金の時効熱処理に伴う力学特性の変化に、粒界性格が影響を及ぼすことを示したことは、粒界性格が材料設計に組み込むべきパラメータであることを示した点は特筆すべき成果である。

Report

(5 results)
  • 2019 Annual Research Report   Final Research Report ( PDF )
  • 2018 Annual Research Report
  • 2017 Annual Research Report
  • 2016 Annual Research Report
  • Research Products

    (29 results)

All 2019 2018 2017 2016

All Journal Article (8 results) (of which Int'l Joint Research: 3 results,  Peer Reviewed: 8 results,  Open Access: 4 results,  Acknowledgement Compliant: 1 results) Presentation (21 results) (of which Int'l Joint Research: 4 results,  Invited: 1 results)

  • [Journal Article] Characterisation of structural similarities of precipitates in Mg-Zn and Al-Zn-Mg alloys systems2019

    • Author(s)
      Artenis Bendo, Tomoyoshi Maeda, Kenji Matsuda, Adrian Lervik, Randi Holmestad, Calin D. Marioara, Katsuhiko Nishimura, Norio Nunomura, Hiroyuki Toda, Masatake Yamaguchi, Ken-ichi Ikeda, Tomoyuki Homma
    • Journal Title

      Philosophical Magazine

      Volume: 99 Issue: 21 Pages: 2619-2635

    • DOI

      10.1080/14786435.2019.1637032

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Commencement of ordering in Al-0.69 Mg-0.31 Si alloy2019

    • Author(s)
      J. Mittra, S. Hata, K. Ikeda, A. Arya
    • Journal Title

      Transactions of the Indian Institute of Metals

      Volume: In press Issue: 2 Pages: 301-308

    • DOI

      10.1007/s12666-019-01844-4

    • Related Report
      2019 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Kink boundaries and their role in dynamic recrystallisation of a Mg-Zn-Y alloy2019

    • Author(s)
      Jing Wu, Ken-ichi Ikeda, Q. Shi, YuLung Chiu
    • Journal Title

      Materials Characterization

      Volume: 148 Pages: 233-242

    • DOI

      10.1016/j.matchar.2018.12.027

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Solid Solution Hardening in Supersaturated Al-Mg-Si Alloy2018

    • Author(s)
      Takata Ken、Ushioda Kohsaku、Kaneko Kenji、Akiyoshi Ryutaro、Ikeda Ken-ichi、Hata Satoshi、Nakashima Hideharu
    • Journal Title

      Journal of the Japan Institute of Metals and Materials

      Volume: 82 Issue: 8 Pages: 314-318

    • DOI

      10.2320/jinstmet.J2018015

    • NAID

      130007419049

    • ISSN
      0021-4876, 1880-6880, 2433-7501
    • Year and Date
      2018-08-01
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effects of Scandium and Zirconium Addition on Recrystallization Behavior of Al–Mg–Si Alloy2018

    • Author(s)
      Ken-ichi Ikeda, Takuya Takashita, Ryutaro Akiyoshi, Satoshi Hata, Hideharu Nakashima, Kazuhiro Yamada, Kenji Kaneko
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 59 Issue: 4 Pages: 590-597

    • DOI

      10.2320/matertrans.L-M2018802

    • NAID

      130006549523

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Infiltration behavior of molten Mg and its influence on microstructural evolution in SiC-doped MgB2 wires prepared by internal Mg diffusion2018

    • Author(s)
      Yusuke Shimada, Satoshi Hata, Ken-ichi Ikeda, Hideharu Nakashima, Akiyoshi Matsumoto, Kazumasa Togano, Hiroaki Kumakura
    • Journal Title

      Journal of Alloys and Compounds

      Volume: 740 Pages: 305-311

    • DOI

      10.1016/j.jallcom.2018.01.012

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Improvement of Strength–Elongation Balance of Al–Mg–Si Sheet Alloy by Utilising Mg–Si Cluster and Its Proposed Mechanism2017

    • Author(s)
      Ken Takata, Kohsaku Ushioda, Ryutaro Akiyoshi, Ken-ichi Ikeda, Jun Takahashi, Satoshi Hata, Kenji Kaneko
    • Journal Title

      MATERIALS TRANSACTIONS

      Volume: 58 Issue: 5 Pages: 728-733

    • DOI

      10.2320/matertrans.M2016258

    • NAID

      130005621141

    • ISSN
      1345-9678, 1347-5320
    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] Effects of Scandium and Zirconium addition on recrystallization behavior of Al–Mg–Si alloy2016

    • Author(s)
      池田賢一, 高下拓也, 秋吉竜太郎, 波多聰, 中島英治, 山田和広, 金子賢治
    • Journal Title

      Journal of Japan Institute of Light Metals

      Volume: 66 Issue: 11 Pages: 609-616

    • DOI

      10.2464/jilm.66.609

    • NAID

      130007314761

    • ISSN
      0451-5994, 1880-8018
    • Related Report
      2016 Annual Research Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Presentation] Al-1.0mass%Mg2Si合金の時効生成物に及ぼす添加元素の影響2019

    • Author(s)
      池田賢一, 孫天航, 嶋田雄介, 李昇原, 土屋大樹, 松田健二, 本間智之
    • Organizer
      軽金属学会第136回春期大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 熱間圧延を施したAl-1%Mn合金に形成される微細組織とその熱的安定性2019

    • Author(s)
      池田賢一, 長船裕樹, 三浦誠司, 井本浩史, 佐藤馨, 名越正泰
    • Organizer
      軽金属学会第136回春期大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] Al-Mg-Si系合金の時効析出に伴う粒界近傍の力学特性変化の粒界性格依存性2019

    • Author(s)
      橋本拓也, 池田賢一, 三浦誠司
    • Organizer
      令和元年度日本鉄鋼協会・日本金属学会両支部合同サマーセッション
    • Related Report
      2019 Annual Research Report
  • [Presentation] Al-Mg-Si系合金の時効生成物に及ぼす添加元素の影響2019

    • Author(s)
      池田賢一, 孫天航, 嶋田雄介, 李昇原, 土屋大樹, 松田健二, 本間智之
    • Organizer
      日本金属学会2019年秋期(第165回)講演大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 低炭素鋼の引張延性挙動に及ぼすTi添加と時効温度の影響2019

    • Author(s)
      安原颯人, 池田賢一, 三浦誠司, 豊田武
    • Organizer
      日本鉄鋼協会 第178回秋期講演大会 学生ポスターセッション
    • Related Report
      2019 Annual Research Report
  • [Presentation] Al-0.62mass%Mg-0.34mass%Si合金における粒界近傍の力学特性と時効析出挙動の関係2019

    • Author(s)
      橋本拓也, 池田賢一, 三浦誠司
    • Organizer
      軽金属学会第137回秋期大会
    • Related Report
      2019 Annual Research Report
  • [Presentation] 微小硬さ試験によるAl-Mg-Si系合金の局所力学挙動に及ぼす粒界性格の影響2019

    • Author(s)
      橋本拓也, 池田賢一, 三浦誠司
    • Organizer
      日本金属学会 微小領域の力学特性評価とマルチスケールモデリング 第一回研究会
    • Related Report
      2019 Annual Research Report
  • [Presentation] アルミニウム合金の加工熱処理工程における組織形成機構の解明2019

    • Author(s)
      池田賢一
    • Organizer
      日本金属学会2019年(第164回)春期講演大会
    • Related Report
      2018 Annual Research Report
    • Invited
  • [Presentation] 予ひずみを与えたAl-Mg-Si合金の時効硬化挙動とその力学特性2018

    • Author(s)
      池田賢一, 佐藤翔悟, 三浦誠司, 高田健
    • Organizer
      軽金属学会第134回春期大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Effect of Cold Rolling on Age Hardening in Al-0.62mass%Mg-0.32mass%Si Alloy2018

    • Author(s)
      Ken-ichi IKEDA, Shogo SATO, Seiji MIURA, Ken TAKATA
    • Organizer
      International Conference on Aluminum Alloys (ICAA16)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 低炭素鋼の時効析出挙動に及ぼすTi添加の影響2018

    • Author(s)
      安原颯人, 池田賢一, 三浦誠司, 豊田武
    • Organizer
      平成30年度日本金属学会・日本鉄鋼協会両支部合同サマーセッション
    • Related Report
      2018 Annual Research Report
  • [Presentation] The effect of natural aging combine with prestrain on bake hardening response in Al-Mg-Si alloy2018

    • Author(s)
      Tianhang SUN, Ken-ichi IKEDA, Seiji MIURA, Ken TAKATA
    • Organizer
      軽金属学会第135回秋期大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Al-0.62mass%Mg-0.32mass%Si合金の二段時効挙動に及ぼす予ひずみの影響2018

    • Author(s)
      池田賢一, 佐藤翔悟, 孫天航, 三浦誠司, 高田健
    • Organizer
      軽金属学会第135回秋期大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Al-0.62mass%Mg-0.32mass%Si合金の時効硬化に及ぼす予ひずみの影響2017

    • Author(s)
      池田賢一, 佐藤翔悟, 三浦誠司, 高田健
    • Organizer
      日本顕微鏡学会 第73回学術講演会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Al-Mg-Si系合金における微細組織と機械的性質の関係2017

    • Author(s)
      佐藤翔悟, 池田賢一, 三浦誠司, 高田健
    • Organizer
      日本金属学会2017年(第161回)秋期講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Al-Mg-Si合金の時効析出挙動に及ぼす冷間加工の影響2017

    • Author(s)
      池田賢一, 佐藤翔悟, 三浦誠司, 高田健
    • Organizer
      日本金属学会 高温変形の組織ダイナミクス研究会 「平成29年度夏の学校」
    • Related Report
      2017 Annual Research Report
  • [Presentation] Effect of Sc and Zr Addition on Recrystallization Behavior and Texture formation in Al-Mg-Si alloy2017

    • Author(s)
      Ken-ichi IKEDA, Seiji MIURA
    • Organizer
      18th International Conference on Texture of Materials (ICOTOM18)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Al-Mg-Si系合金の再結晶集合組織に及ぼす熱的安定な析出物の影響2016

    • Author(s)
      池田賢一
    • Organizer
      軽金属学会 第99回シンポジウム「加工と熱処理による優先方位制御」
    • Place of Presentation
      日本大学 駿河台キャンパス, 東京都
    • Year and Date
      2016-11-28
    • Related Report
      2016 Annual Research Report
  • [Presentation] 熱的安定な析出物がAl-Mg-Si系合金の再結晶挙動に及ぼす影響2016

    • Author(s)
      池田賢一, 秋吉竜太郎, 高下拓也, 波多聰, 中島英治, 山田和広, 金子賢治
    • Organizer
      軽金属学会 平成28年度加工と熱処理による優先方位制御研究部会 公開講演会
    • Place of Presentation
      福山市鞆公民館, 福山市
    • Year and Date
      2016-10-06
    • Related Report
      2016 Annual Research Report
  • [Presentation] Effect of Thermo-Mechanical Treatment on Recrystallization Behavior in Al-Mg-Si-Sc-Zr Alloys2016

    • Author(s)
      Ken-ichi Ikeda, Ryutaro Akiyoshi, Satoshi Hata, Hideharu Nakashima, Kazuhiro Yamada, Kenji Kaneko
    • Organizer
      9th Pacific Rim International Conference on Advanced Materials and Processing (PRICM9)
    • Place of Presentation
      Kyoto International Conference Center, Kyoto
    • Year and Date
      2016-08-01
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Effect of Sc and Zr Addition on Recrystallization Behavior in Al-Mg-Si Alloy2016

    • Author(s)
      Ken-ichi Ikeda, Ryutaro Akiyoshi, Satoshi Hata, Hideharu Nakashima, Kazuhiro Yamada, Kenji Kaneko
    • Organizer
      6th International Conference on Recrystallization and Grain Growth (ReX&GG2016)
    • Place of Presentation
      Pittsburgh, USA
    • Year and Date
      2016-07-17
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research

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Published: 2016-04-21   Modified: 2021-02-19  

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