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Mechanism of stress-induced exothermic reaction in Ti/Si multilayer films and development of novel reactive bonding technique

Research Project

Project/Area Number 16H04510
Research Category

Grant-in-Aid for Scientific Research (B)

Allocation TypeSingle-year Grants
Section一般
Research Field Composite materials/Surface and interface engineering
Research InstitutionAichi Institute of Technology

Principal Investigator

NAMAZU Takahiro  愛知工業大学, 工学部, 教授 (90347526)

Research Collaborator MIYAKE shugo  
Project Period (FY) 2016-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥18,330,000 (Direct Cost: ¥14,100,000、Indirect Cost: ¥4,230,000)
Fiscal Year 2018: ¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Fiscal Year 2017: ¥2,730,000 (Direct Cost: ¥2,100,000、Indirect Cost: ¥630,000)
Fiscal Year 2016: ¥13,000,000 (Direct Cost: ¥10,000,000、Indirect Cost: ¥3,000,000)
Keywords自己伝播発熱材料 / 接合 / デバイス / 機械刺激 / 自己伝播発熱素材 / 瞬間ハンダ接合 / 機械刺激反応誘起 / 自己伝播発熱多層膜 / Ti/Si / 瞬間接合 / 新規接合技術 / 機能材料 / 薄膜 / 自己伝播発熱 / マイクロ・ナノデバイス
Outline of Final Research Achievements

In this work, we succeeded quantitative evaluation of the threshold energy for exothermic reaction in Ti/Si multilayer films by means of mechanical shock test. We found that Ti/Si film with thinner bilayer thickness could react by smaller external energy for exothermic reaction. Differential scanning calorimetry demonstrated that Ti/Si film with thinner bilayer thickness showed the first exothermic peak at lower temperature. Based on these experimental facts, we successfully fabricated reactively-soldered Si chips with Ti/Si exothermic reactive film by only single mechanical shock.

Academic Significance and Societal Importance of the Research Achievements

機械刺激で2種類の金属の化合物生成に伴う発熱反応を誘起できる現象の力学的考察の一端を行うことができた.今後,原子レベルまで掘り下げて発熱反応誘起ならびに反応伝播のメカニズムを解明することが課題である.この機能性素材を用いてSiウェハを1秒未満で瞬間的にはんだ接着することに成功した.既存のはんだ接合が本提案技術に置き換われば,工程短縮・コスト削減とともに省エネ・ゼロエミッション化にも貢献できる可能性があり,環境問題にも貢献できる.

Report

(4 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Annual Research Report
  • 2016 Annual Research Report
  • Research Products

    (16 results)

All 2019 2018 2017 2016 Other

All Journal Article (7 results) (of which Int'l Joint Research: 3 results,  Peer Reviewed: 7 results,  Open Access: 1 results) Presentation (7 results) (of which Int'l Joint Research: 4 results) Remarks (2 results)

  • [Journal Article] Effect of Free-standing Al/Ni Exothermic Film on Thermal Resistance of Reactively Bonded Solder Joint2019

    • Author(s)
      Kanetsuki Shunsuke、Miyake Shugo、Namazu Takahiro
    • Journal Title

      Sensors and Materials

      Volume: 31 Issue: 3 Pages: 729

    • DOI

      10.18494/SAM.2019.2076

    • ISSN
      0914-4935, 2435-0869
    • Year and Date
      2019-03-08
    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access
  • [Journal Article] New local joining technique for metal materials using exothermic heat of Al/Ni multilayer powder2018

    • Author(s)
      Izumi Taisei、Kametani Nagamasa、Miyake Shugo、Kanetsuki Shunsuke、Namazu Takahiro
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 57 Issue: 6S1 Pages: 06HJ10-06HJ10

    • DOI

      10.7567/jjap.57.06hj10

    • NAID

      210000149185

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Size effect in self-propagating exothermic reaction of Al/Ni multilayer block on a Si wafer2017

    • Author(s)
      Namazu Takahiro、Ito Shun、Kanetsuki Shunsuke、Miyake Shugo
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 56 Issue: 6S1 Pages: 06GN11-06GN11

    • DOI

      10.7567/jjap.56.06gn11

    • NAID

      210000147936

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Effect of thickening outermost layers in Al/Ni multilayer film on thermal resistance of reactively bonded solder joints2017

    • Author(s)
      Kanetsuki Shunsuke、Kuwahara Koichi、Egawa Shouichi、Miyake Shugo、Namazu Takahiro
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 56 Issue: 6S1 Pages: 06GN16-06GN16

    • DOI

      10.7567/jjap.56.06gn16

    • NAID

      210000147941

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Temperature behavior of exothermic reaction of Al/Ni multilayer powder materials based on cold-rolling and pulverizing method2017

    • Author(s)
      Kametani Nagamasa、Izumi Taisei、Miyake Shugo、Kanetsuki Shunsuke、Namazu Takahiro
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 56 Issue: 6S1 Pages: 06GN07-06GN07

    • DOI

      10.7567/jjap.56.06gn07

    • NAID

      210000147932

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] Influence of Bonding Pressure on Thermal Resistance in Reactively-bonded Solder Joints2016

    • Author(s)
      S. Kanetsuki, S. Miyake, K. Kuwahara, and T. Namazu
    • Journal Title

      JJAP

      Volume: 55 Issue: 6S1 Pages: 06GP17-06GP17

    • DOI

      10.7567/jjap.55.06gp17

    • NAID

      210000146697

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Mechanical Reliability of Reactively Alloyed NiAl as a Structural Material2016

    • Author(s)
      T. Namazu, K. Kuwahara, M. Fujii, S. Kanetsuki, S. Miyake, and S. Inoue
    • Journal Title

      Sensors and Materials

      Volume: 28 Pages: 141-152

    • Related Report
      2016 Annual Research Report
    • Peer Reviewed
  • [Presentation] Time-resolved X-ray diffraction study of formation of intermetallic compounds in Al/Ni multilayer materials2018

    • Author(s)
      Rino Yamamoto, Taisei Izumi, Sho Nagata, Ryota Wakatsuki, Kai Uozaki, Shugo Miyake, Takahiro Namazu, Shunsuke Kanetsuki, Daiki Goto, Yasuhiro Kuntani, Takumi Nomura, Tomoyuki Koganezawa
    • Organizer
      International Symposium on Advanced Science and Technology in Experimental Mechanics, ISEM’18
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Time-Resolved X-ray Diffraction Measurement during Exothermic Reaction of Al/Ni Multilayer Powder by synchrotron radiation with high-speed two-dimensional detector2018

    • Author(s)
      Shugo Miyake, Rino Yamamoto, Shunsuke Kanetsuki, Takahiro Namazu and Tomoyuki Koganezawa
    • Organizer
      International Microprocesses and Nanotechnology Conference, MNC2018
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 自己伝播発熱多層膜の瞬間接合応用2018

    • Author(s)
      生津資大, 金築俊介, 神谷亮太, 松尾彰大
    • Organizer
      日本機械学会東海支部第67期総会・講演会
    • Related Report
      2018 Annual Research Report
  • [Presentation] Al/Ni多層粉末材料における圧延率が化合物形成と発熱特性に及ぼす影響2018

    • Author(s)
      山本梨乃, 三宅修吾, 金築俊介, 生津資大
    • Organizer
      日本金属学会2018年春期講演大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 機械刺激で発熱反応誘起できるTi/Si多層膜2018

    • Author(s)
      訓谷保広, 金築俊介, 三宅修吾, 生津資大
    • Organizer
      2018年度日本機械学会年次大会
    • Related Report
      2018 Annual Research Report
  • [Presentation] A Novel Joining Technique for Aluminum Foils by Using Al/Ni Exothermic Materials as Saving Heat Source2017

    • Author(s)
      Taisei Izumi, Nagamasa Kametani, Shugo Miyake, Shunsuke Kanetsuki, and Takahiro Namazu
    • Organizer
      30th International Microprocesses and Nanotechnology Conference, MNC2017
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Influence of Solder Thickness on Fracture Behavior of Al/Ni Reactively-Bonded Solder Joints for Reliability of MEMS2016

    • Author(s)
      K. Kuwahara, S. Kanetsuki, S. Miyake, S. Inoue, and T. Namazu
    • Organizer
      Proc. of the Eighth Asia-Pacific Conference on Transducers and Micro/Nano Technologies
    • Place of Presentation
      金沢文化ホール(石川県金沢市)
    • Year and Date
      2016-06-26
    • Related Report
      2016 Annual Research Report
    • Int'l Joint Research
  • [Remarks] 生津研究室ホームページ

    • URL

      https://aitech.ac.jp/~namazu/home.html

    • Related Report
      2018 Annual Research Report
  • [Remarks] 愛知工業大学工学部機械学科 ナノテク研究室(生津研究室)ホームページ

    • URL

      http://aitech.ac.jp/~namazu/home.html

    • Related Report
      2016 Annual Research Report

URL: 

Published: 2016-04-21   Modified: 2020-03-30  

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