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Development of evaluation method for ductile damage in a single crystal using synchrotron white X-rays

Research Project

Project/Area Number 16K05961
Research Category

Grant-in-Aid for Scientific Research (C)

Allocation TypeMulti-year Fund
Section一般
Research Field Materials/Mechanics of materials
Research InstitutionKitami Institute of Technology

Principal Investigator

Shibano Junichi  北見工業大学, 工学部, 教授 (60206141)

Co-Investigator(Kenkyū-buntansha) 吉田 裕  北見工業大学, 工学部, 准教授 (30626122)
Project Period (FY) 2016-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥4,550,000 (Direct Cost: ¥3,500,000、Indirect Cost: ¥1,050,000)
Fiscal Year 2018: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2017: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2016: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Keywords延性損傷 / 単結晶 / 転位密度 / プロファイル解析 / 装置関数 / 白色X線 / 放射光 / 機械材料・材料力学 / 放射光白色X線 / 非破壊検査
Outline of Final Research Achievements

In this study, we presented the profile analysis method to evaluate dislocation cell size, non-uniform strain and dislocation density in a single crystal by using a transmitted diffracted X-ray of synchrotron white X-rays. The aluminum single crystal which received ductile damage with tension load was measured at synchrotron radiation facilities SPring-8. The X-ray measurement area of the specimen was observed by transmission electron microscope TEM. The observations by TEM were compared with the estimate results by this method. As a result, although the dislocation cell size obtained by this method was evaluated more largely than the observations by TEM, the dislocation density indicated almost same value. It confirmed that this method is useful for the ductile damage evaluation in a single crystal.

Academic Significance and Societal Importance of the Research Achievements

機械や構造物の破壊の原因となるき裂の発生・進展を非破壊で高精度に推定・評価する手法の開発が産業界から強く望まれている。本研究では、これまで検討してきた放射光白色X線によるプロファイル解析手法を基に、単結晶内部の特定された結晶方位から得られる単一の回折X線プロファイルから、延性損傷パラメータとして転位セルサイズ、不均一ひずみ、転位密度の情報を得るための手法を開発した。本手法は材料破壊の原因究明や材料工学研究においても有効な測定技術として活用できる。

Report

(4 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Research-status Report
  • 2016 Research-status Report
  • Research Products

    (8 results)

All 2018 2017 2016

All Journal Article (3 results) (of which Peer Reviewed: 3 results) Presentation (5 results)

  • [Journal Article] Crystal rotation and microstructures in an aluminum single-slip system under tensile loading2018

    • Author(s)
      Y.Yoshida, J. Shibano, K. Fukuda, K. Terabayashi, M. Eguchi, K. Kajiwara, T. Shobu , A. Shiro
    • Journal Title

      Materials Characterization

      Volume: 146 Pages: 121-126

    • DOI

      10.1016/j.matchar.2018.10.001

    • NAID

      120006951245

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Journal Article] チタンと骨組織の接触界面近傍の放射光白色X線を用いたひずみ測定2017

    • Author(s)
      柴野純一、清谷真平、越村瑞樹、梶原堅太郎、菖蒲敬久
    • Journal Title

      非破壊検査

      Volume: 66 Pages: 261-265

    • NAID

      130007342635

    • Related Report
      2017 Research-status Report
    • Peer Reviewed
  • [Journal Article] Acoustic emission response of magnesium alloy during cyclic and creep tests2016

    • Author(s)
      S. Kawai, Y. Yoshida, H. Asano, S. Miura, M. Kobayashi, J. Shibano
    • Journal Title

      Materials Science and Engineering: A

      Volume: 668 Pages: 120-124

    • DOI

      10.1016/j.msea.2016.05.057

    • NAID

      120006695780

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Presentation] 回折X線による極薄板内部の応力評価2018

    • Author(s)
      立石優河, 吉田裕, 蓮本翔, 柴野純一
    • Organizer
      日本設計工学会 秋季研究発表講演会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 放射光白色X線を利用したアルミニウム単結晶の延性損傷評価及び検討2018

    • Author(s)
      吉田裕, 寺林賢吾, 柴野純一, 梶原堅太郎, 城鮎美, 菖蒲敬久
    • Organizer
      第52回X線材料強度に関するシンポジウム
    • Related Report
      2018 Annual Research Report
  • [Presentation] 引張破壊試験片の転位密度評価2018

    • Author(s)
      菖蒲敬久, 安田良, 城鮎美, 吉田裕, 徳田奨, 柴野純一, 熊谷正芳
    • Organizer
      第31回日本放射光学会放射光科学合同シンポジウム
    • Related Report
      2017 Research-status Report
  • [Presentation] 透過X線回折による引張負荷中の純マグネシウムの損傷評価2017

    • Author(s)
      江口雅人, 本間与主愛, 宇佐美翔也, 吉田裕, 柴野純一
    • Organizer
      日本金属学会第160回春期大会
    • Place of Presentation
      首都大学東京(東京都八王子市)
    • Year and Date
      2017-03-15
    • Related Report
      2016 Research-status Report
  • [Presentation] 放射光を用いたラインプロファイル解析法による鉄鋼材料転位密度評価2017

    • Author(s)
      菖蒲敬久、城鮎美、吉田裕、徳田奨、柴野純一、熊谷正芳
    • Organizer
      第51回X線材料強度に関するシンポジウム
    • Related Report
      2017 Research-status Report

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Published: 2016-04-21   Modified: 2020-03-30  

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