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Syntheis of novel nanomagnets utilizing low dimensionality and extreme environment

Research Project

Project/Area Number 16K13640
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Nanomaterials engineering
Research InstitutionOsaka University

Principal Investigator

Sato Kazuhisa  大阪大学, 超高圧電子顕微鏡センター, 准教授 (70314424)

Co-Investigator(Renkei-kenkyūsha) YASUDA HIDEHIRO  大阪大学, 超高圧電子顕微鏡センター, センター長・教授 (60210259)
Project Period (FY) 2016-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2017: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Fiscal Year 2016: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Keywords低次元性 / 極限環境 / ナノ磁石 / 電子照射 / 規則合金 / FeNi / 照射促進規則化 / 超高圧電子顕微鏡
Outline of Final Research Achievements

L10-type FeNi ordered phase, which was firstly found in a meteorite, is hard to synthesize as a bulk form at a laboratory. We have studied rapid atomic diffusion in FeNi alloy thin films under 1 MeV-electron irradiation in an attempt to largely enhance atomic ordering at low annealing temperatures. In this study, (1) electron irradiation-enhanced ordering of Co-Pt alloy nanoparticles was confirmed, (2) L10-FeNi phase was formed via electron irradiation-enhanced ordering, and (3) effect of 2-MeV-electron irradiation on structural changes of ordered FeNi nanocrystalline alloys was examined. We have demonstrated that radiation-enhanced ordering is a suitable way to promote atomic ordering in FeNi alloy. We proved that L10-FeNi ordered phase is the stable phase at 573 K.

Report

(3 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • Research Products

    (16 results)

All 2018 2017 2016

All Journal Article (4 results) (of which Peer Reviewed: 4 results,  Acknowledgement Compliant: 1 results,  Open Access: 1 results) Presentation (12 results) (of which Int'l Joint Research: 5 results,  Invited: 2 results)

  • [Journal Article] Fluctuation of long-range order in Co-Pt alloy nanoparticles revealed by time-resolved electron microscopy2017

    • Author(s)
      K. Sato and H. Yasuda
    • Journal Title

      Applied Physics Letters

      Volume: 110 Issue: 15 Pages: 1531011-4

    • DOI

      10.1063/1.4980077

    • NAID

      40021254867

    • Related Report
      2017 Annual Research Report 2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Journal Article] Maximum usable thickness revisited: Imaging dislocations in Si by modern high-voltage scanning transmission electron microscopy2017

    • Author(s)
      Kazuhisa Sato, Yuki Yamashita, Hidehiro Yasuda, and Hirotaro Mori
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 56 Issue: 10 Pages: 1003041-4

    • DOI

      10.7567/jjap.56.100304

    • NAID

      210000148310

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Crystallization induced ordering of hard magnetic L10 phase in melt-spun FeNi-based ribbons2016

    • Author(s)
      K. Sato, P. Sharma, Y. Zhang, K. Takenaka, A. Makino,AIP Advances
    • Journal Title

      AIP Advances

      Volume: 6 Issue: 5 Pages: 0552181-9

    • DOI

      10.1063/1.4952968

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Open Access
  • [Journal Article] L1<sub>0</sub>-type Ordered Phase Formation in Fe-Ni-based Nanocrystalline Alloys2016

    • Author(s)
      佐藤和久、Parmanand Sharma、張岩、竹中佳生、牧野彰宏
    • Journal Title

      Materia Japan

      Volume: 55 Issue: 12 Pages: 596-596

    • DOI

      10.2320/materia.55.596

    • NAID

      130005170157

    • ISSN
      1340-2625, 1884-5843
    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Presentation] Fluctuation of long-range order in Co-Pt alloy nanoparticles revealed by time-resolved high-voltage electron microscopy2018

    • Author(s)
      Kazuhisa Sato and Hidehiro Yasuda
    • Organizer
      19th International Microscopy Congress (IMC19)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 合金ナノ粒子における電子照射誘起規則化過程の1/400秒スケール観察2017

    • Author(s)
      佐藤和久、保田英洋
    • Organizer
      日本物理学会第72回年次大会
    • Place of Presentation
      大阪大学豊中キャンパス (大阪府・豊中市)
    • Year and Date
      2017-03-17
    • Related Report
      2016 Research-status Report
  • [Presentation] Direct imaging of electron irradiation induced atomic ordering in CoPt nanoparticles2017

    • Author(s)
      K. Sato and H. Yasuda
    • Organizer
      5th International Conference on Multifunctional, Hybrid and Nanomaterials
    • Place of Presentation
      Lisboa Congress Centre (Portugal)
    • Year and Date
      2017-03-06
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] In-situ UHVEM observation of atomic ordering in alloy nanoparticles using a direct detection camera2017

    • Author(s)
      K. Sato and H. Yasuda
    • Organizer
      Workshop on High-Resolution Quantitative Measurements (2016年度 日本顕微鏡学会超高分解能顕微鏡法分科会 研究会)
    • Place of Presentation
      マホロバ・マインズ三浦 (神奈川県・三浦市)
    • Year and Date
      2017-02-18
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research / Invited
  • [Presentation] 最新電子顕微鏡法によるナノ磁性材料の原子的構造評価2017

    • Author(s)
      佐藤和久
    • Organizer
      大阪大学超高圧電子顕微鏡センター・材料系共同利用研究報告会
    • Place of Presentation
      大阪大学吹田キャンパス (大阪府・吹田市)
    • Year and Date
      2017-01-16
    • Related Report
      2016 Research-status Report
  • [Presentation] 超高圧電子顕微鏡を用いた1/400秒スケールその場観察と極厚試料における観察可能厚さの定量評価2017

    • Author(s)
      佐藤和久, 保田英洋
    • Organizer
      超顕微科学研究拠点事業平成29年度研究発表会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Electron-irradiation-enhanced atomic ordering in magnetic nanoparticles revealed by high-voltage transmission electron microscopy2017

    • Author(s)
      Kazuhisa Sato and Hidehiro Yasuda
    • Organizer
      The 3rd East-Asia Microscopy Conference (EAMC3)
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Pdナノ粒子の原子的構造と磁気的性質2017

    • Author(s)
      安村駿治, 佐藤和久, 保田英洋
    • Organizer
      日本金属学会2017年秋期(第161回)講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 透過電子顕微鏡によるナノ磁性材料の原子的構造評価2016

    • Author(s)
      佐藤和久
    • Organizer
      日本顕微鏡学会関西支部平成28年度特別講演会
    • Place of Presentation
      京都大学宇治キャンパス (京都府・宇治市)
    • Year and Date
      2016-10-29
    • Related Report
      2016 Research-status Report
    • Invited
  • [Presentation] CoPtナノ粒子規則化過程の超高圧電子顕微鏡その場加熱高速観察2016

    • Author(s)
      佐藤和久、保田英洋
    • Organizer
      日本金属学会2016年秋期(第159回)講演大会
    • Place of Presentation
      大阪大学豊中キャンパス (大阪府・豊中市)
    • Year and Date
      2016-09-21
    • Related Report
      2016 Research-status Report
  • [Presentation] In situ UHVEM observation of atomic ordering in magnetic nanoparticles using a direct detection camera2016

    • Author(s)
      K. Sato and H. Yasuda
    • Organizer
      The 16th European Microscopy Congress (emc2016)
    • Place of Presentation
      Lyon Convention Center (France)
    • Year and Date
      2016-08-28
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] ナノ粒子における規則化過程の超高圧電子顕微鏡その場加熱観察2016

    • Author(s)
      佐藤和久、保田英洋
    • Organizer
      日本顕微鏡学会第72回学術講演会
    • Place of Presentation
      仙台国際センター (宮城県・仙台市)
    • Year and Date
      2016-06-14
    • Related Report
      2016 Research-status Report

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Published: 2016-04-21   Modified: 2019-03-29  

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