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Develpment of measurement based materials science by simultaneous analysis of elastic & inelastic scattering

Research Project

Project/Area Number 16K13660
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Applied materials
Research InstitutionUniversity of Tsukuba

Principal Investigator

NISHIBORI Eiji  筑波大学, 数理物質系, 教授 (10293672)

Project Period (FY) 2016-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥3,510,000 (Direct Cost: ¥2,700,000、Indirect Cost: ¥810,000)
Fiscal Year 2017: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2016: ¥2,600,000 (Direct Cost: ¥2,000,000、Indirect Cost: ¥600,000)
Keywords放射光X線回折 / 弾性散乱 / 非弾性散乱 / 電子密度解析 / フォノン分散 / 熱散漫散乱 / Bragg反射 / コンプトン散乱 / 放射光散乱 / 高エネルギーエックス線 / 結晶構造解析 / 散漫散乱改s系 / コンプトン散乱解析 / 手法開発 / 散漫散乱解析 / 新機能性材料
Outline of Final Research Achievements

In this study, we have developed an analytical method to determine both dynamic and static structure from powder diffraction profiles of simple structure materials such as diamond and pure metals. Bragg intensities, thermal diffuse scattering, and Compton scattering, etc were used for the analysis.
We successfully measured the temperature dependence of thermal diffuse scattering due to phonon for aluminum which shows relatively large amount of diffuse scattering. We also observed very small amounts of electron accumulation in charge density from Bragg intensities. We succeeded to detect weak modulation of charge density by the present developed method.

Report

(3 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • Research Products

    (12 results)

All 2017 2016 Other

All Int'l Joint Research (1 results) Journal Article (5 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 5 results,  Open Access: 1 results,  Acknowledgement Compliant: 1 results) Presentation (6 results) (of which Int'l Joint Research: 4 results)

  • [Int'l Joint Research] オーフス大学/材料結晶学センター(デンマーク)

    • Related Report
      2016 Research-status Report
  • [Journal Article] β-IminoBODIPY oligomers: facilely accessible π-conjugated luminescent BODIPY arrays2017

    • Author(s)
      Tsuchiya Mizuho、Sakamoto Ryota、Shimada Masaki、Yamanoi Yoshinori、Hattori Yohei、Sugimoto Kunihisa、Nishibori Eiji、Nishihara Hiroshi
    • Journal Title

      Chemical Communications

      Volume: 53 Issue: 54 Pages: 7509-7512

    • DOI

      10.1039/c7cc03279j

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Mechano-, thermo-, solvato-, and vapochromism in bis(acetato-κ1O)[4′-(4-(diphenylamino)phenyl)](2,2′:6′,2′′-terpyridine-κ3N,N′,N′′)zinc(ii) and its polymer2017

    • Author(s)
      Tsukamoto Takamasa、Aoki Risa、Sakamoto Ryota、Toyoda Ryojun、Shimada Masaki、Hattori Yohei、Kitagawa Yasutaka、Nishibori Eiji、Nakano Masayoshi、Nishihara Hiroshi
    • Journal Title

      Chemical Communications

      Volume: 53 Issue: 70 Pages: 9805-9808

    • DOI

      10.1039/c7cc05022d

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 2.Spatial distribution of electrons near the Fermi level in the metallic LaB6 through accurate X-ray charge density study.2017

    • Author(s)
      Hidetaka Kasai & Eiji Nishibori
    • Journal Title

      Scientific Reports

      Volume: 7 Issue: 1 Pages: 41375-41375

    • DOI

      10.1038/srep41375

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Open Access / Acknowledgement Compliant
  • [Journal Article] Antiferromagnetic Ordering in the Single-component Molecular Conductor, [Pd(tmdt)2]2016

    • Author(s)
      Ogura Satomi, Idobata Yuki, Zhou, Biao, Kobayashi Akiko, Takagi Rina, Miyagawa Kazuya, Kanoda Kazushi, Kasai Hidetaka, Nishibori Eiji, Satoko Chikatoshi, Delley, Bernard
    • Journal Title

      Inorganic Chemistry

      Volume: 55 Issue: 15 Pages: 7709-7716

    • DOI

      10.1021/acs.inorgchem.6b01166

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Int'l Joint Research
  • [Journal Article] 5.Direct observation of spin-coating process in PS-b-P2VP thin films.2016

    • Author(s)
      Hiroki Ogawa*, Mikihito Takenaka, Tsukasa Miyazaki, Keisuke Shimokita, Akihiko Fujiwara, Eiji Nishibori, Masaki Takata,
    • Journal Title

      Macromolecules

      Volume: 49 Issue: 9 Pages: 3471-3477

    • DOI

      10.1021/acs.macromol.6b00049

    • Related Report
      2016 Research-status Report
    • Peer Reviewed
  • [Presentation] Ultra-high reciprocal resolution X-ray diffraction of Al and Cu2017

    • Author(s)
      Tomoaki Sasaki, Hidetaka Kasai, Eiji Nishibori
    • Organizer
      24th Congress and General Assembly of the International Union of Crystallography
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Accurate structures of diamond under high- pressure and temperature.2017

    • Author(s)
      Yuka Deguchi, Eiji Nishibori, Bo Iversen,
    • Organizer
      24th Congress and General Assembly of the International Union of Crystallography
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 超高分解能放射光粉末法によるアルミニウムの結合電荷密度2017

    • Author(s)
      佐々木友彰・笠井秀隆・西堀英治
    • Organizer
      平成29年度日本結晶学会年会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 量子結晶学によるダイヤモンドの精密構造決定2017

    • Author(s)
      出口裕佳・西堀英治・Bo Iversen
    • Organizer
      平成29年度日本結晶学会年会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Charge density studies of metallic and semiconductor hexaborides2017

    • Author(s)
      Eiji Nishibori, Hidetaka Kasai
    • Organizer
      AnalyiX-2017
    • Place of Presentation
      Hilton Fukuoka Sea Hawk, Fukuoka,Fukuoka
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] X-ray Charge density study of positive electrodes for secondary battery.2016

    • Author(s)
      Eiji Nishibori, Hidetaka Kasai, Takayuki Shibata, Wataru Kobayashi, and Yutaka Moritomo
    • Organizer
      AsCA2016
    • Place of Presentation
      Hanoi University of Science & Technology, Hanoi, Vetnum
    • Year and Date
      2016-12-04
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research

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Published: 2016-04-21   Modified: 2019-03-29  

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