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Development of reemission positron microscope

Research Project

Project/Area Number 16K14015
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Analytical chemistry
Research InstitutionChiba University

Principal Investigator

Fujinami Masanori  千葉大学, 大学院工学研究院, 教授 (50311436)

Research Collaborator CHIARI Luca  千葉大学, 大学院工学研究院, 特任助教
KOMATSU Akari  千葉大学, 大学院工学研究科, 大学院生
NOZAKI Ayaka  千葉大学, 大学院工学研究科, 大学院生
KOIZUMI Kazuki  千葉大学, 大学院工学研究科, 大学院生
SENDA Tomoki  千葉大学, 大学院工学研究科, 大学院生
Project Period (FY) 2016-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2017: ¥1,560,000 (Direct Cost: ¥1,200,000、Indirect Cost: ¥360,000)
Fiscal Year 2016: ¥2,210,000 (Direct Cost: ¥1,700,000、Indirect Cost: ¥510,000)
Keywords格子欠陥 / 放射線 / 量子ビーム / 陽電子 / 水素脆化 / 鉄 / ステンレス鋼 / 二次元分析 / イメージング
Outline of Final Research Achievements

The aim of this work is to clarify the crucial defects related to hydrgen embrittelment (HE) in pure bcc-iron and austenitic stainless steel by positron annihilation lifetime spectroscopy(PALS). Pure bcc-iron specimens were deformed at two different strain rates under a hydrogen environment. These PALS results could be explained by the formation of vacancy-hydrogen complexes, which were considered the dominant defects in HE. The two types of austenitic stainless steels, SUS 304 and SUS 316L, were pre-charged with hydrogen and subjected to tensile straining. The SUS 304 alloy showed HE, whereas the SUS 316L alloy showed low hydrogen susceptibility. The vacancy clusters could be induced in both of the samples, indicating that they were not crucial in the HE process. By comparing the defect behavior in detail using the PALS method, we can clarify the vacancy-hydrogen complexes which are related to HE in fcc iron.

Report

(3 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • Research Products

    (27 results)

All 2018 2017 2016 Other

All Journal Article (1 results) (of which Peer Reviewed: 1 results,  Open Access: 1 results) Presentation (23 results) (of which Int'l Joint Research: 16 results,  Invited: 5 results) Book (2 results) Remarks (1 results)

  • [Journal Article] Significant suppression of Rayleigh scattering loss in silica glass formed by the compression of its melted phase2018

    • Author(s)
      Madoka Ono, Shuhei Aoyama, Masanori Fujinami, Setsuro Ito
    • Journal Title

      Optics Express

      Volume: 26 Issue: 7 Pages: 7942-7948

    • DOI

      10.1364/oe.26.007942

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access
  • [Presentation] 陽電子消滅法を用いたオーステナイト系ステンレス鋼における水素安定化欠陥の検出2017

    • Author(s)
      小松 あかり,小泉 一輝,野﨑 彩花,藤浪 眞紀,秦野 正治,松本 和久
    • Organizer
      日本鉄鋼協会 第173回春季講演大会
    • Place of Presentation
      首都大学東京
    • Year and Date
      2017-03-15
    • Related Report
      2016 Research-status Report
  • [Presentation] 変形したアルミニウムにおける欠陥と相互作用する不純物の同定2017

    • Author(s)
      藤浪眞紀,千田智紀,田中智士,Luca Chiari
    • Organizer
      第77回分析化学討論会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Positron annihilation spectroscopy of the defects induced in bcc- and fcc-iron upon hydrogen embrittlement (HE)2017

    • Author(s)
      Masanori Fujinami
    • Organizer
      The 3rd China-Japan Joint Workshop on Positron Science
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Positron annihilation spectroscopy of various zeolite materials2017

    • Author(s)
      Nagisa Sakata, Ayaka Nozaki, Luca Chiari, Masanori Fujinami
    • Organizer
      The 3rd China-Japan Joint Workshop on Positron Science
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Void structure in silica glass observed with positron annihilation lifetime spectroscopy2017

    • Author(s)
      Madoka Ono, Masanori Fujinami, Setsuro Ito
    • Organizer
      Glass & Optical Materials Division Meeting 2017
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] 各種ゼオライトにおける陽電子消滅2017

    • Author(s)
      坂田渚彩,野﨑彩花,Chiari Luca,藤浪眞紀
    • Organizer
      第53回アイソトープ・放射線研究発表会
    • Related Report
      2017 Annual Research Report
  • [Presentation] Crucial defects induced by hydrogen embrittlement in a-iron and stainless steel by positron annihilation spectroscopy2017

    • Author(s)
      Masanori Fujinami
    • Organizer
      13th International Conference on Diffusion in Solids and Liquids
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Hydrogen-induced defects in α-iron on hydrogen embrittlement by temperature-variable positron annihilation lifetime spectroscopy2017

    • Author(s)
      Ayaka Nozaki, Kazuki Koizumi, Akari Komatsu, Luca Chiari, Masanori Fujinami
    • Organizer
      13th International Conference on Diffusion in Solids and Liquids
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Behavior of hydrogen-stabilized defects in austenitic stainless steel probed by positron annihilation spectroscopy2017

    • Author(s)
      Akari Komatsu, Ayaka Nozaki, Kazuki Koizumi, Luca Chiari, Masanori Fujinami
    • Organizer
      13th International Conference on Diffusion in Solids and Liquids
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] The crucial defects induced in a-iron and stainless steel on hydrogen embrittlement by positron annihilation spectroscopy2017

    • Author(s)
      Masanori Fujinami, Akari Komatsu, Ayaka Nozaki, Kazuki Koizumi
    • Organizer
      Gordon Research Conference Hydrogen-Metal Systems
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research
  • [Presentation] Positron Annihilation Spectroscopy of the Defects Induced by Hydrogen Embrittlement in bcc- and fcc-Iron2017

    • Author(s)
      Akari Komatsu, Masanori Fujinami
    • Organizer
      Gordon Research Seminars Hydrogen-Metal Systems
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Pores in highly densified silica glass by positron annihilation spectroscopy2017

    • Author(s)
      Masanori Fujinami, Shuhei Aoyama, Madoka Ono, Setsuro Ito
    • Organizer
      12th International Workshop on Positron and Positronium Chemistry
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] The Critical Defects Induced in fcc-iron on Hydrogen Embrittlement by Positron Annihilation Spectroscopy2017

    • Author(s)
      Masanori Fujinami
    • Organizer
      International Workshop on Positron Studies of Defects 2017
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] 陽電子消滅法による鉄系材料の水素関与欠陥挙動2017

    • Author(s)
      藤浪眞紀,小泉一輝,野﨑彩花,小松あかり
    • Organizer
      日本物理学会 2017年秋季大会
    • Related Report
      2017 Annual Research Report
    • Invited
  • [Presentation] 陽電子消滅法によるオーステナイト系ステンレスSUS316Lにおける水素脆化欠陥2017

    • Author(s)
      藤浪眞紀,小松あかり
    • Organizer
      日本鉄鋼協会 第175回春季講演大会
    • Related Report
      2017 Annual Research Report
  • [Presentation] 陽電子からみた純鉄中水素誘起欠陥の延伸速度依存性2016

    • Author(s)
      藤浪 眞紀
    • Organizer
      日本鉄鋼協会 第172回秋季講演大会
    • Place of Presentation
      大阪大学豊中キャンパス
    • Year and Date
      2016-09-21
    • Related Report
      2016 Research-status Report
  • [Presentation] Characterization of hydrogen-induced defects in metals by positron annihilation spectroscopy2016

    • Author(s)
      Masanori Fujinami
    • Organizer
      The 15th International Symposium on Metal-Hydrogen Systems
    • Place of Presentation
      Interlaken, Switzerland
    • Year and Date
      2016-08-07
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Vacancy-hydrogen complexes in α-iron on hydrogen embrittlement by positron annihilation spectroscopy2016

    • Author(s)
      Ayaka Nozaki, Akari Komatsu, Kazuki Koizumi, Masanori Fujinami
    • Organizer
      The 15th International Symposium on Metal-Hydrogen Systems
    • Place of Presentation
      Interlaken, Switzerland
    • Year and Date
      2016-08-07
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Positron annihilation spectroscopy in hydrogen-stabilized defects in austenitic stainless steels2016

    • Author(s)
      Akari Komatsu, Ayaka Nozaki, Kazuki Koizumi, Kasumi Arai, Masanori Fujinami, Masaharu Hatano
    • Organizer
      The 15th International Symposium on Metal-Hydrogen Systems
    • Place of Presentation
      Interlaken, Switzerland
    • Year and Date
      2016-08-07
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] 温度可変陽電子寿命測定を用いた歪速度変化水素脆化α鉄における水素安定化欠陥挙動の追跡2016

    • Author(s)
      小松あかり,野﨑彩花,小泉一輝,藤浪眞紀
    • Organizer
      第53回アイソトープ・放射線研究発表会
    • Place of Presentation
      東京大学農学部
    • Year and Date
      2016-07-06
    • Related Report
      2016 Research-status Report
  • [Presentation] Positron studies on pores in silica-based glasses2016

    • Author(s)
      Masanori Fujinami, Madoka Ono, Setsuro Ito, Kenji Ito
    • Organizer
      The 14th International Workshop on Positron Beam Techniques & Applications
    • Place of Presentation
      島根,松江くにびきメッセ
    • Year and Date
      2016-05-22
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Positron annihilation spectroscopy in vacancy clusters induced by the electro- and the electroless-deposited Cu films2016

    • Author(s)
      Tomoaki Hyodo, Kagetora Ikeda, Kenji Ito, Masanori Fujinami
    • Organizer
      The 14th International Workshop on Positron Beam Techniques & Applications
    • Place of Presentation
      島根,松江くにびきメッセ
    • Year and Date
      2016-05-22
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Vacancy-hydrogen complexes in α-iron on hydrogen embrittlement by positron annihilation spectroscopy2016

    • Author(s)
      Akari Komatsu, Ayaka Nozaki, Kazuki Koizumi, Masanori Fujinami
    • Organizer
      The 14th International Workshop on Positron Beam Techniques & Applications
    • Place of Presentation
      島根,松江くにびきメッセ
    • Year and Date
      2016-05-22
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Book] 8版2018 放射線取扱の基礎2018

    • Author(s)
      伊藤守弘,勝村庸介,柴田徳思,杉山和幸,鈴木崇彦,桧垣正吾,藤浪眞紀
    • Total Pages
      512
    • Publisher
      丸善
    • ISBN
      9784890732661
    • Related Report
      2017 Annual Research Report
  • [Book] J. of Physics: Conf. Ser. Volume 2172017

    • Author(s)
      M. Fujinami, Y. Nagashima, B.E. O'Rourke
    • Total Pages
      140
    • Publisher
      Institute of Physics
    • Related Report
      2016 Research-status Report
  • [Remarks]

    • URL

      http://chem.tf.chiba-u.jp/gacb11/index.html

    • Related Report
      2017 Annual Research Report

URL: 

Published: 2016-04-21   Modified: 2019-03-29  

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