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Microscopic toughening mechanism toward the nano-micro hierachical microstructural design for high toughness and high strength

Research Project

Project/Area Number 16K14411
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Structural/Functional materials
Research InstitutionTokyo Institute of Technology

Principal Investigator

Wakai Fumihiro  東京工業大学, 科学技術創成研究院, 教授 (30293062)

Project Period (FY) 2016-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥3,640,000 (Direct Cost: ¥2,800,000、Indirect Cost: ¥840,000)
Fiscal Year 2017: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Fiscal Year 2016: ¥1,820,000 (Direct Cost: ¥1,400,000、Indirect Cost: ¥420,000)
Keywords破壊靱性 / 強度 / ミクロ力学試験 / セラミックス / ナノ結晶材料 / 靱性強化機構 / 構造・機能材料 / 強度・破壊靭性
Outline of Final Research Achievements

The finding of “fracture-induced amorphization” in nanocrystalline SiO2 stishovite lead to a proposal of a new type of transformation toughening by the direct transition from crystal to amorphous state, which is different from the classical martensitic transformation of zirconia. Here, we investigated strength andtoughness of nanocrystalline stishovite by using micro-cantilever beam specimens of different sizes. The maximum strength of 6.3 GPa gave the estimate of the lower bound of critical stress for amorphization,which was much higher than the critical transformation stress of zirconia. The crack growth resistance curve (R-curve) rose steeply with crack extension of only a few micrometers, and reached to a plateau value of10.9 MPa m1/2. The results clearly showed this novel toughening mechanism can achieve both excellent strength and toughness.

Report

(3 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • Research Products

    (14 results)

All 2017 2016 Other

All Int'l Joint Research (3 results) Journal Article (3 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 3 results,  Open Access: 1 results,  Acknowledgement Compliant: 1 results) Presentation (8 results) (of which Int'l Joint Research: 4 results,  Invited: 1 results)

  • [Int'l Joint Research] 南カリフォルニア大学(米国)

    • Related Report
      2017 Annual Research Report
  • [Int'l Joint Research] ドイツ電子エレクトロン(ドイツ)

    • Related Report
      2017 Annual Research Report
  • [Int'l Joint Research] ドイツ電子シンクロトロン(ドイツ)

    • Related Report
      2016 Research-status Report
  • [Journal Article] Evaluation of effects of crack deflection and grain bridging on toughening of nanocrystalline SiO 2 stishovite2017

    • Author(s)
      Yoshida Kimiko、Nishiyama Norimasa、Shinoda Yutaka、Akatsu Takashi、Wakai Fumihiro
    • Journal Title

      Journal of the European Ceramic Society

      Volume: 37 Issue: 15 Pages: 5113-5117

    • DOI

      10.1016/j.jeurceramsoc.2017.06.047

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed
  • [Journal Article] Picosecond amorphization of SiO2 stishovite under tension2017

    • Author(s)
      Misawa Masaaki、Ryuo Emina、Yoshida Kimiko、Kalia Rajiv K.、Nakano Aiichiro、Nishiyama Norimasa、Shimojo Fuyuki、Vashishta Priya、Wakai Fumihiro
    • Journal Title

      Science Advances

      Volume: 3 Issue: 5 Pages: 1-7

    • DOI

      10.1126/sciadv.1602339

    • Related Report
      2017 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research
  • [Journal Article] Strength and toughness of nano crystalline SiO2 stishovite toughened by fracture-induced amorphization2017

    • Author(s)
      Kimiko Yoshida, Norimasa Nishiyama, Masato Sone, Fumihiro Wakai
    • Journal Title

      Acta Materializa

      Volume: 124 Pages: 316-324

    • DOI

      10.1016/j.actamat.2016.11.014

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] Micro-mechanical test method for searching toughening mechanisms operating at nanoscale2017

    • Author(s)
      F. Wakai, K. Yoshida, M. Sone, N. Nishiyama
    • Organizer
      15th Conference and Exhibition of the European Ceramic Society
    • Related Report
      2017 Annual Research Report
    • Int'l Joint Research / Invited
  • [Presentation] Large increase in fracture resistance of nano-crystalline stishovite made from silica glass2016

    • Author(s)
      K. Yoshida, N. Nishiyama, M. Sone, F. Wakai
    • Organizer
      CerSJ-GOMD Joint Symposium on Glass Science and Technologies
    • Place of Presentation
      Kyoto University, Yoshida campus
    • Year and Date
      2016-11-13
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] 高硬度・高靭性ナノ多結晶スティショバイトの微細組織と機械的特性2016

    • Author(s)
      吉田貴美子,西山宣正,若井史博
    • Organizer
      粉体粉末冶金協会平成28年度秋季大会
    • Place of Presentation
      東北大学青葉山キャンパス
    • Year and Date
      2016-11-09
    • Related Report
      2016 Research-status Report
  • [Presentation] ナノメートル領域までのアルミナの破壊靭性の粒径依存性2016

    • Author(s)
      関根 理沙子、吉田 貴美子、篠田 豊、赤津 隆、曽根 正人、明渡 純 、若井 史博
    • Organizer
      日本セラミックス協会第29回秋季シンポジウム
    • Place of Presentation
      広島大学東広島キャンパス
    • Year and Date
      2016-09-07
    • Related Report
      2016 Research-status Report
  • [Presentation] 高圧相SiO2(スティショバイト)の破壊誘起アモルファス化による新奇高靭化機構の解明2016

    • Author(s)
      吉田貴美子,西山宣正,若井史博
    • Organizer
      日本セラミックス協会第29回秋季シンポジウム
    • Place of Presentation
      広島大学東広島キャンパス
    • Year and Date
      2016-09-07
    • Related Report
      2016 Research-status Report
  • [Presentation] Microscopic R-curve behavior and fracture strength of nanocrystalline stishovite toughened by fracture-induced amorphization2016

    • Author(s)
      K. Yoshida, F. Wakai, N. Nishiyama
    • Organizer
      6th International Congress on Ceramics
    • Place of Presentation
      Dresden, Germany
    • Year and Date
      2016-08-21
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] Microscopic R-curve behavior and fracture strength of nanocrystalline stishovite toughened by fracture-induced amorphization,2016

    • Author(s)
      K. Yoshida, F. Wakai, N. Nishiyma
    • Organizer
      Gordon Research Conference, Ceramics, Solid State Studies
    • Place of Presentation
      Mount Holyoke College, South Hadley, MA, USA
    • Year and Date
      2016-07-31
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research
  • [Presentation] マイクロカンチレバー試験片による高硬度・高靭性ナノ多結晶スティショバイトの破壊抵抗及び強度評価2016

    • Author(s)
      吉田貴美子、西山宣正、曽根正人、若井史博
    • Organizer
      マルチスケール材料力学シンポジウム
    • Place of Presentation
      富山大学五福キャンパス
    • Year and Date
      2016-05-27
    • Related Report
      2016 Research-status Report

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Published: 2016-04-21   Modified: 2019-03-29  

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