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Flow visualization of heavy oil in supercritical water atmosphere by neutron radiography

Research Project

Project/Area Number 16K14454
Research Category

Grant-in-Aid for Challenging Exploratory Research

Allocation TypeMulti-year Fund
Research Field Properties in chemical engineering process/Transfer operation/Unit operation
Research InstitutionTohoku University

Principal Investigator

Tsukada Takao  東北大学, 工学研究科, 教授 (10171969)

Co-Investigator(Kenkyū-buntansha) 高見 誠一  名古屋大学, 工学研究科, 教授 (40311550)
竹中 信幸  神戸大学, 工学研究科, 教授 (50171658)
齊藤 泰司  京都大学, 原子炉実験所, 教授 (40283684)
杉本 勝美  神戸大学, 先端融合研究環, 助教 (40420468)
Co-Investigator(Renkei-kenkyūsha) KUBO MASAKI  東北大学, 大学院工学研究科, 准教授 (50323069)
Project Period (FY) 2016-04-01 – 2018-03-31
Project Status Completed (Fiscal Year 2017)
Budget Amount *help
¥3,770,000 (Direct Cost: ¥2,900,000、Indirect Cost: ¥870,000)
Fiscal Year 2017: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Fiscal Year 2016: ¥2,470,000 (Direct Cost: ¥1,900,000、Indirect Cost: ¥570,000)
Keywords超重質油 / 超臨界水改質 / 中性子ラジオグラフィ / 充填層型反応器 / 流動挙動 / 流通式反応器 / 流動・混合状態
Outline of Final Research Achievements

For a packed bed reactor, which consists of a 1/2-inch stainless steel tube filled with alumina particles having the diameter of 3 mm, the flow behavior of heavy oil in the reactor under the atmosphere of nitrogen gas or supercritical water was observed by neutron radiography. In the heavy oil/nitrogen gas system, the effect of reactor temperature on the flow behavior at atmospheric pressure was clarified. Particularly, the flow channeling was observed in the reactor at a relatively high temperature. In the heavy oil/supercritical water system, the effect of flow rate of heavy oil on the flow behavior was investigated at 400℃ and 25 MPa. Through this work, it was revealed that neutron radiography is a useful technique to visualize the flow behavior of heavy oil in a packed bed reactor, whose wall was made of metal, at high temperature and high pressure.

Report

(3 results)
  • 2017 Annual Research Report   Final Research Report ( PDF )
  • 2016 Research-status Report
  • Research Products

    (1 results)

All 2018

All Presentation (1 results)

  • [Presentation] 中性子ラジオグラフィを用いた充填層反応器内の重質油の流動挙動の可視化2018

    • Author(s)
      山際幸士郎,庄司衛太,久保正樹,塚田隆夫,髙見誠一,杉本勝美,齊藤泰司,伊藤大介
    • Organizer
      化学工学会第83年会
    • Related Report
      2017 Annual Research Report

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Published: 2016-04-21   Modified: 2019-03-29  

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