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Development of dislocation propagation tracking method in nitride semiconductors by synchrotron micro-beam X-rays

Research Project

Project/Area Number 16K17522
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Thin film/Surface and interfacial physical properties
Research InstitutionNational Institutes for Quantum and Radiological Science and Technology

Principal Investigator

Sasaki Takuo  国立研究開発法人量子科学技術研究開発機構, 関西光科学研究所 放射光科学研究センター, 主任研究員(定常) (90586190)

Research Collaborator Takahasi Masamitu  
Project Period (FY) 2016-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥4,290,000 (Direct Cost: ¥3,300,000、Indirect Cost: ¥990,000)
Fiscal Year 2018: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2017: ¥910,000 (Direct Cost: ¥700,000、Indirect Cost: ¥210,000)
Fiscal Year 2016: ¥1,950,000 (Direct Cost: ¥1,500,000、Indirect Cost: ¥450,000)
Keywords放射光X線 / 窒化物半導体 / ナノ構造 / 分子線エピタキシー / X線回折 / 転位 / 格子欠陥 / X線 / MBE
Outline of Final Research Achievements

A detection technique of a single dislocation in semiconductor materials was developed using synchrotron X-rays for new in situ observation technique of lattice defects during crystal growth. The X-rays focused to 1 micrometer by the Fresnel Zone Plate (FZP) were scanned on samples with dislocations, and it was checked whether a single crystal disorder could be detected. As a result, the single threading dislocation in the bulk crystal, as well as the misfit dislocation in the heteroepitaxial film, were successfully detected. Besides, the evolution of strain and crystal structure during hetero-structured nanowire growth was investigated.

Academic Significance and Societal Importance of the Research Achievements

本研究成果である放射光マイクロビームを用いた単一転位の可視化技術の確立は、単一転位が結晶成長中にどのような挙動を示すのかその場観察手法を開発する上で必須の技術であり、転位の発生や運動、転位間相互作用といった学術的に意義の高い転位挙動の解明において重要である。また、同研究成果は、バルク結晶およびヘテロエピタキシャル薄膜の結晶品質の向上に将来的に寄与するものと期待され、窒化物半導体を用いた電子デバイスの高性能化、高機能化にも資するものであり、社会的にも意義のある成果と考える。

Report

(4 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Research-status Report
  • 2016 Research-status Report
  • Research Products

    (16 results)

All 2019 2018 2017 2016

All Journal Article (4 results) (of which Peer Reviewed: 2 results,  Open Access: 1 results,  Acknowledgement Compliant: 1 results) Presentation (12 results) (of which Int'l Joint Research: 2 results,  Invited: 2 results)

  • [Journal Article] Real-time structural analysis of InGaAs/InAs/GaAs(1 1 1)A interfaces by in situ synchrotron X-ray reciprocal space mapping2019

    • Author(s)
      Takuo Sasaki and Masamitu Takahasi
    • Journal Title

      Journal of Crystal Growth

      Volume: 512 Pages: 33-36

    • DOI

      10.1016/j.jcrysgro.2019.02.007

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed
  • [Journal Article] 放射光その場X線逆格子マッピングによる化合物半導体の結晶成長ダイナミクス2018

    • Author(s)
      佐々木 拓生, 高橋 正光
    • Journal Title

      応用物理

      Volume: 87 Pages: 409-415

    • NAID

      130007715777

    • Related Report
      2018 Annual Research Report
  • [Journal Article] その場X線回折による窒化物半導体薄膜の結晶成長観察2017

    • Author(s)
      佐々木 拓生, 高橋 正光
    • Journal Title

      SPring-8/SACLA利用者情報

      Volume: 22 Pages: 306-309

    • Related Report
      2017 Research-status Report
    • Open Access
  • [Journal Article] Nitride-MBE system for in situ synchrotron X-ray measurements2016

    • Author(s)
      Takuo Sasaki, Fumitaro Ishikawa, Tomohiro Yamaguchi, and Masamitu Takahasi
    • Journal Title

      Japanese Journal of Applied Physics

      Volume: 55 Issue: 5S Pages: 05FB05-05FB05

    • DOI

      10.7567/jjap.55.05fb05

    • NAID

      210000146496

    • Related Report
      2016 Research-status Report
    • Peer Reviewed / Acknowledgement Compliant
  • [Presentation] N極性GaN上の液体Ga層のその場X線構造解析2019

    • Author(s)
      佐々木 拓生, 高橋 正光
    • Organizer
      第66回応用物理学会春季学術講演会
    • Related Report
      2018 Annual Research Report
  • [Presentation] 窒化物半導体成長のその場X線回折測定2018

    • Author(s)
      高橋 正光, 佐々木 拓生, 山口 智広
    • Organizer
      第47回結晶成長国内会議(JCCG-47)
    • Related Report
      2018 Annual Research Report
    • Invited
  • [Presentation] Real-time structural analysis of InGaAs/InAs/GaAs(111)A interfaces by in situ synchrotron X-ray reciprocal space mapping2018

    • Author(s)
      佐々木 拓生, 高橋 正光
    • Organizer
      The 20th International Conference on Molecular Beam Epitaxy (ICMBE 2018)
    • Related Report
      2018 Annual Research Report
    • Int'l Joint Research
  • [Presentation] GaN表面上Ga吸着層の構造解析2018

    • Author(s)
      佐々木 拓生, 岩田 卓也, 高橋 正光
    • Organizer
      第10回ナノ構造・エピタキシャル成長講演会
    • Related Report
      2018 Annual Research Report
  • [Presentation] MBE成長GaNナノワイヤにおけるイエロールミネッセンスの抑制2018

    • Author(s)
      上杉 智洋, 佐々木 拓生, 高橋 正光
    • Organizer
      第79回応用物理学会秋季学術講演会
    • Related Report
      2018 Annual Research Report
  • [Presentation] GaN表面上Ga吸着層の構造解析2018

    • Author(s)
      佐々木 拓生, 岩田 卓也, 高橋 正光
    • Organizer
      第79回応用物理学会秋季学術講演会
    • Related Report
      2018 Annual Research Report
  • [Presentation] GaN表面上Ga吸着層の秩序構造2018

    • Author(s)
      佐々木 拓生, 岩田 卓也, 高橋 正光
    • Organizer
      第65回応用物理学会春季学術講演会
    • Related Report
      2017 Research-status Report
  • [Presentation] GaN表面のX線CTR散乱測定2018

    • Author(s)
      佐々木 拓生, 岩田 卓也, 高橋 正光
    • Organizer
      第31回日本放射光学会年会・放射光科学合同シンポジウム
    • Related Report
      2017 Research-status Report
  • [Presentation] Ga-bilayer/GaN表面の X線CTR散乱測定2017

    • Author(s)
      佐々木 拓生, 高橋 正光
    • Organizer
      第78回応用物理学会秋季学術講演会
    • Related Report
      2017 Research-status Report
  • [Presentation] 窒化ガリウム結晶成長表面のCTR散乱測定2017

    • Author(s)
      佐々木 拓生, 高橋 正光
    • Organizer
      第9回ナノ構造・エピタキシャル成長講演会
    • Related Report
      2017 Research-status Report
  • [Presentation] GaN 上およびInN 上GaInN 成長における成長初期過程の観察2017

    • Author(s)
      山口 智広, 佐々木 拓生, 高橋 正光, 尾沼 猛儀, 本田 徹, 荒木 努, 名西やすし
    • Organizer
      第78回応用物理学会秋季学術講演会
    • Related Report
      2017 Research-status Report
  • [Presentation] Strain Relaxation Analysis Using In-situ X-ray Reciprocal Space Mapping Measurements in RF-MBE Growth of GaInN2016

    • Author(s)
      T. Yamaguchi, T. Sasaki, M. Takahasi, T. Honda, T. Onuma, Y. Nanishi
    • Organizer
      The 18th International Conference on Crystal Growth and Epitaxy (ICCGE-18)
    • Place of Presentation
      Nagoya Congress Center
    • Year and Date
      2016-08-09
    • Related Report
      2016 Research-status Report
    • Int'l Joint Research / Invited

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Published: 2016-04-21   Modified: 2020-03-30  

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