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research of prevention of low-temperature degradation of ful-countour zirconia prostheses

Research Project

Project/Area Number 16K20481
Research Category

Grant-in-Aid for Young Scientists (B)

Allocation TypeMulti-year Fund
Research Field Prosthodontics/ Dental materials science and
Research InstitutionTohoku University

Principal Investigator

Harada Akio  東北大学, 歯学研究科, 助教 (40757267)

Research Collaborator Egusa Hiroshi  
Nakamura Keisuke  
Nakazawa Kosuke  
Project Period (FY) 2016-04-01 – 2019-03-31
Project Status Completed (Fiscal Year 2018)
Budget Amount *help
¥3,900,000 (Direct Cost: ¥3,000,000、Indirect Cost: ¥900,000)
Fiscal Year 2018: ¥1,430,000 (Direct Cost: ¥1,100,000、Indirect Cost: ¥330,000)
Fiscal Year 2017: ¥1,170,000 (Direct Cost: ¥900,000、Indirect Cost: ¥270,000)
Fiscal Year 2016: ¥1,300,000 (Direct Cost: ¥1,000,000、Indirect Cost: ¥300,000)
Keywordsジルコニア / 低温劣化 / 歯科材料 / 表面処理 / 破折強度
Outline of Final Research Achievements

The purpose of this study was to evaluate the influence of ultrasonic scaling and low-temperature degradation (LTD) on surface properties of zirconia. Yttria-stabilized tetragonal zirconia polycrystals (3Y-TZP) were aged by autoclaving at 135℃ and 0.2 MPa for 100 hours comparable to 5 years intraoral aging, subsequently treated by ultrasonic scaler tips made of PEEK or stainless steel. X-ray diffraction analysis showed that LTD induced phase transformation whereas ultrasonic scaling did not generate monoclinic phase. Ultrasonic scaling significantly increased Sa (P <0.0001), especially when LTD-induced 3Y-TZP was subjected to ultrasonic scaling using stainless steel tip.

Academic Significance and Societal Importance of the Research Achievements

CAD/CAM技術の進歩により近年では歯冠修復材料としてジルコニアが多く用いられ、最近では前装材料を用いないフルカントゥア・ジルコニアが多く使用されている。一方で、前装材料を使用しないことにより、水分に曝露することで脆い結晶構造に変化する低温劣化という現象も知られており、口腔内における長期間の水分曝露による影響も無視できない。
本研究では低温劣化したジルコニア表面にメインテナンスで使用する器具におけるジルコニアの表面性状を評価し、ステンレススチールチップでは粗造な表面を形成したものの、臨床的には問題のない範囲であること、PEEK製チップではその影響はより小さなものであることを示した。

Report

(4 results)
  • 2018 Annual Research Report   Final Research Report ( PDF )
  • 2017 Research-status Report
  • 2016 Research-status Report
  • Research Products

    (1 results)

All 2018

All Journal Article (1 results) (of which Int'l Joint Research: 1 results,  Peer Reviewed: 1 results,  Open Access: 1 results)

  • [Journal Article] Surface properties of dental zirconia ceramics affected by ultrasonic scaling and low-temperature degradation2018

    • Author(s)
      Nakazawa K, Nakamura K, Harada A, Shirato M, Inagaki R, Ortengren U, Kanno T, Niwano Y, Egusa H.
    • Journal Title

      PLoS One

      Volume: 13 Issue: 9 Pages: e0203849-e0203849

    • DOI

      10.1371/journal.pone.0203849

    • Related Report
      2018 Annual Research Report
    • Peer Reviewed / Open Access / Int'l Joint Research

URL: 

Published: 2016-04-21   Modified: 2020-03-30  

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